← Back to Patent Explorer
US5896870A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of removing slurry particles

Assignee: International Business Machines Corp
•
Filing: 1997-03-11
•
Granted: 1999-04-27
•
Expires: 2017-03-11
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract Disclosed is a method and apparatus for polishing a semiconductor wafer. This invention describes a novel in situ method for eliminating residual slurry and slurry abrasive particles on the wafer. A reactant is added to the slurry during the end of the Chemical Mechanical Polish (CMP) process to dissolve the slurry and etch the abrasive particles.

Inventors

  • 👤 Cuc K. Huynh
  • 👤 Harold G. Linde
  • 👤 Patricia E. Marmillion
  • 👤 Anthony M. Palagonia
  • 👤 Bernadette A. Pierson
  • 👤 Matthew J. Rutten

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 13:57
CPC Classifications
B; B24; B24B; B24B55/00; B24B55/12; H; H10; H10P; H10P95/00; B24B37/00; B24B37/04; C; C09; C09K; C09K3/00; C09K3/14; C09K3/1454; C09K3/1463; H10P95/06; H10P95/062

Claims Analysis

Total Claims: 32
Claim 1
Independent Claim 42 words
A method for in situ reduction in size of abrasive particles in a slurry during a polishing process for planarization of a wafer, comprising: adding a reagent to the slurry during the polishing process to reduce the size of the abrasive particles.
Claim 2
Independent Claim 42 words
A method for in situ reduction in size of abrasive particles in a slurry during a polishing process for planarization of a wafer, comprising: adding a reagent to the slurry during the polishing process to reduce the size of the abrasive particles.
Claim 3
Dependent Claim 18 words
The method of claim 1, wherein the abrasive particles comprise cerium oxide and the reagent comprises nitric acid.
Claim 4
Dependent Claim 15 words
The method of claim 1, wherein the abrasive particles comprise silica, silicon, alumina, or tungsten.
Claim 5
Dependent Claim 30 words
The method of claim 1, wherein the abrasive particles comprise silica or silicon and the reagent is selected from the group consisting of aqueous KOH, alcoholic KOH, and aqueous TMAH.
Claim 6
Dependent Claim 24 words
The method of claim 1, wherein the abrasive particles comprise alumina and the reagent comprises a mixture of methanol, hydrochloric acid, and hydrofluoric acid.
Claim 7
Dependent Claim 19 words
The method of claim 1, wherein the abrasive particles comprises a tungsten and the reagent comprises a sodium hypochlorite.
Claim 8
Dependent Claim 19 words
The method of claim 1, wherein the abrasive particles comprise an alumina and the reagent comprises a phosphoric acid.
Claim 9
Independent Claim 46 words
A method for in situ reduction in size of agglomerations of abrasive particles in a slurry during a polishing process for planarization of a wafer, comprising: adding a reagent to the slurry during the polishing process to reduce the size of the agglomerations of abrasive particles.
Claim 10
Independent Claim 46 words
A method for in situ reduction in size of agglomerations of abrasive particles in a slurry during a polishing process for planarization of a wafer, comprising: adding a reagent to the slurry during the polishing process to reduce the size of the agglomerations of abrasive particles.
Claim 11
Independent Claim 37 words
A method for in situ removal of abrasive particles in a slurry during a polishing process for planarization of a wafer, comprising: exposing the slurry to a reagent during the polishing process to dissolve the abrasive particles.
Claim 12
Independent Claim 37 words
A method for in situ removal of abrasive particles in a slurry during a polishing process for planarization of a wafer, comprising: exposing the slurry to a reagent during the polishing process to dissolve the abrasive particles.
Claim 13
Independent Claim 61 words
A method for in situ reduction in size of abrasive particles in a slurry during a polishing process for planarization of a wafer, comprising: placing the wafer against a rotating polishing pad; applying the slurry to the polishing pad; and applying a reagent to one of the slurry and the pad during the polishing process to reduce the abrasive particle size.
Claim 14
Independent Claim 61 words
A method for in situ reduction in size of abrasive particles in a slurry during a polishing process for planarization of a wafer, comprising: placing the wafer against a rotating polishing pad; applying the slurry to the polishing pad; and applying a reagent to one of the slurry and the pad during the polishing process to reduce the abrasive particle size.
Claim 15
Dependent Claim 18 words
The method of claim 10, wherein the abrasive particles comprise cerium oxide and the reagent comprises nitric acid.
Claim 16
Dependent Claim 15 words
The method of claim 10, wherein the abrasive particles comprise silica, silicon, alumina, or tungsten.
Claim 17
Dependent Claim 30 words
The method of claim 10, wherein the abrasive particles comprise silica or silicon and the reagent is selected from the group consisting of aqueous KOH, alcoholic KOH, and aqueous TMAH.
Claim 18
Dependent Claim 24 words
The method of claim 10, wherein the abrasive particles comprise alumina and the reagent comprises a mixture of methanol, hydrochloric acid, and hydrofluoric acid.
Claim 19
Dependent Claim 19 words
The method of claim 10, wherein the abrasive particles comprises a tungsten and the reagent comprises a sodium hypochlorite.
Claim 20
Dependent Claim 19 words
The method of claim 10, wherein the abrasive particles comprise an alumina and the reagent comprises a phosphoric acid.
Claim 21
Independent Claim 52 words
A method for in situ reduction in size of abrasive particles in a slurry during a polishing process for planarization of a wafer, comprising: dispensing a CMP slurry; planarizing a semiconductor thin film using the slurry; reducing the slurry dispense; dispensing a reagent during a polishing process; and rinsing with DI water.
Claim 22
Independent Claim 52 words
A method for in situ reduction in size of abrasive particles in a slurry during a polishing process for planarization of a wafer, comprising: dispensing a CMP slurry; planarizing a semiconductor thin film using the slurry; reducing the slurry dispense; dispensing a reagent during a polishing process; and rinsing with DI water.
Claim 23
Dependent Claim 21 words
The method of claim 17, wherein the application of the reagent is controlled to reduce the size of the abrasive particles.
Claim 24
Dependent Claim 23 words
The method of claim 17, wherein the application of the reagent is controlled to reduce the size of agglomerations of the abrasive particles.
Claim 25
Dependent Claim 18 words
The method of claim 17, wherein the application of the reagent is controlled to dissolve the abrasive particles.
Claim 26
Dependent Claim 25 words
The method of claim 17, wherein the step of dispensing the reagent is for a time sufficient to reduce the size of the abrasive particles.
Claim 27
Dependent Claim 18 words
The method of claim 17, wherein the abrasive particles comprise cerium oxide and the reagent comprises nitric acid.
Claim 28
Dependent Claim 15 words
The method of claim 17, wherein the abrasive particles comprise silica, silicon, alumina, or tungsten.
Claim 29
Dependent Claim 30 words
The method of claim 17, wherein the abrasive particles comprise silica or silicon and the reagent is selected from the group consisting of aqueous KOH, alcoholic KOH, and aqueous TMAH.
Claim 30
Dependent Claim 24 words
The method of claim 17, wherein the abrasive particles comprise alumina and the reagent comprises a mixture of methanol, hydrochloric acid, and hydrofluoric acid.
Claim 31
Dependent Claim 18 words
The method of claim 17, wherein the abrasive particles comprise tungsten and the reagent comprises a sodium hypochlorite.
Claim 32
Dependent Claim 18 words
The method of claim 17, wherein the abrasive particles comprise alumina and the reagent comprises a phosphoric acid.

References Cited (Backward Citations)

US3728154A Cited
US4050954A Cited
US4932168A Cited
US4968381A Cited
US5176756A Cited
JPH04158613A Cited
US5320706A Cited
US5391511A Cited
US5389194A Cited
US5456758A Cited
US5478436A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 2002-04-26 2002-10-26 2003-04-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2006-04-26 2006-10-26 2007-04-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2010-04-26 2010-10-26 2011-04-27 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag