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US5356756A Expired / Lapsed US ⏱️ 0.0 years remaining

Application of microsubstrates for materials processing

Assignee: United States Department of Commerce
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Filing: 1992-10-26
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Granted: 1994-10-18
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Expires: 2012-10-26
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Abstract

Abstract Arrays of microfabricated hotplates have been used as substrate arrays for materials processing on a microscopic scale. Properties of individual elements (pixels) of the array, such as temperature and voltage bias, are controlled by addressing a given pixel with appropriate signals. Materials are deposited onto pixels with individually controlled deposition conditions (pixel temperature, bias). Pixels are also addressed to control properties during post-deposition processing steps such as heating in vacuum or various gases to alter stoichiometry of a single material, or to alloy multiple composition materials. The addressable heating characteristics may also be used for a maskless lithography on pixel elements. The result is an array of separately, but simultaneously, processed films. Properties of film elements may be measured using electrical contact pads. The array of processed films may be used for sensors, electronic devices, greatly accelerated materials development processes, and solid state physics, biology and chemistry studies.

Inventors

  • 👤 Richard Cavicchi
  • 👤 Stephen Semancik
  • 👤 John S. Suehle
  • 👤 Michael Gaitan

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 18:36
CPC Classifications
G; G01; G01N; G01N27/00; G01N27/02; G01N27/04; G01N27/14; G01N27/18; H; H05; H05B; H05B3/00; H05B3/10; H05B3/12; H05B3/14; H05B3/148; H05B2203/00; H05B2203/002; H05B2203/003

Claims Analysis

Total Claims: 22
Claim 1
Independent Claim 65 words
A method of preparing a plurality of micro-samples of materials for investigation which comprises: providing a substrate having a plurality of micro-hotplates, wherein each of said plurality of micro-hotplates can be individually temperature controlled; and depositing a material film on said plurality of micro-hotplates while thermally cycling selected ones of said plurality of micro-hotplates to form a micro-sample on each of said plurality of micro-hotplates.
Claim 2
Independent Claim 65 words
A method of preparing a plurality of micro-samples of materials for investigation which comprises: providing a substrate having a plurality of micro-hotplates, wherein each of said plurality of micro-hotplates can be individually temperature controlled; and depositing a material film on said plurality of micro-hotplates while thermally cycling selected ones of said plurality of micro-hotplates to form a micro-sample on each of said plurality of micro-hotplates.
Claim 3
Dependent Claim 39 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 1, wherein said step of thermally cycling selected ones of said micro-hotplates comprises heating all of said plurality of micro-hotplates to a common temperature.
Claim 4
Dependent Claim 40 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 1, wherein selected ones of said micro-samples are subjected to a post-deposition annealing treatment by heating selected ones of said micro-hotplates after said deposition step.
Claim 5
Dependent Claim 40 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 2, wherein selected ones of said micro-samples are subjected to a post-deposition annealing treatment by heating selected ones of said micro-hotplates after said deposition step.
Claim 6
Dependent Claim 34 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 1, further comprising performing a lithography process for isolating selected ones of said micro-hotplates prior to said deposition step.
Claim 7
Dependent Claim 46 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 5, wherein said lithography process involves applying a resist material to said substrate, irradiating portions of said resist material utilizing a mask and removing said irradiated portions of said resist material.
Claim 8
Dependent Claim 24 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 5, wherein said lithography process comprises a maskless-lithography process.
Claim 9
Dependent Claim 47 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 7, wherein said maskless-lithography process involves applying a resist material to said substrate and heating selected ones of said plurality of micro-hotplates to volatilize and thereby remove portions of said resist material.
Claim 10
Dependent Claim 25 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 1, wherein said step of depositing involves a sputtering process.
Claim 11
Dependent Claim 27 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 1, wherein said step of depositing involves a chemical vapor deposition process.
Claim 12
Dependent Claim 25 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 1, wherein said step of depositing involves an evaporation process.
Claim 13
Dependent Claim 28 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 1, wherein electrical properties of said material film are measured during said deposition.
Claim 14
Dependent Claim 28 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 3, wherein electrical properties of said material film are measured during said annealing.
Claim 15
Dependent Claim 28 words
A method of preparing a plurality of micro-samples of materials for investigation according to claim 4, wherein electrical properties of said material film are measured during said annealing.
Claim 16
Independent Claim 64 words
A method of characterizing material properties which comprises: providing a substrate having a plurality of micro-hotplates, wherein each of said plurality of micro-hotplates can be individually temperature controlled; depositing a material film on said plurality of micro-hotplates while thermally cycling selected ones of said plurality of micro-hotplates to form a micro-sample on each of said plurality of micro-hotplates; and characterizing properties of said micro-samples.
Claim 17
Independent Claim 64 words
A method of characterizing material properties which comprises: providing a substrate having a plurality of micro-hotplates, wherein each of said plurality of micro-hotplates can be individually temperature controlled; depositing a material film on said plurality of micro-hotplates while thermally cycling selected ones of said plurality of micro-hotplates to form a micro-sample on each of said plurality of micro-hotplates; and characterizing properties of said micro-samples.
Claim 18
Dependent Claim 35 words
A method of characterizing material properties according to claim 15, wherein said properties of said micro-samples which are characterized are selected from the group consisting of electrical properties, chemical properties, physical properties and combinations thereof.
Claim 19
Dependent Claim 19 words
A method of characterizing material properties according to claim 15, wherein said characterization is performed during said deposition step.
Claim 20
Dependent Claim 28 words
A method of characterizing material properties according to claim 15, wherein said characterization is performed by scanning electron microscopy, scanning tunneling microscopy, atomic force microscopy or x-ray analysis.
Claim 21
Dependent Claim 34 words
A method of characterizing material properties according to claim 15, wherein selected ones of said micro-samples are subjected to a post-deposition annealing treatment by heating selected ones of said micro-hotplates after said deposition step.
Claim 22
Dependent Claim 33 words
A method of characterizing material properties according to claim 15, wherein said step of thermally cycling selected ones of said micro-hotplates comprises heating all of said plurality of micro-hotplates to a common temperature.

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3.5 Years (Year 4) 1997-10-17 1998-04-18 1998-10-18 $2000.00 Window Closed / Lapsed
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