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US5439877A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for depositing high temperature superconducting oxide thin films

Assignee: EIDP Inc
•
Filing: 1994-03-24
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Granted: 1995-08-08
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Expires: 2014-03-24
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Abstract

Abstract In-situ process are provided for 1) depositing on a substrate a crystalline thin film of a high temperature superconducting oxide by exposing the back surface of the substrate, i.e., the surface of the substrate opposite the surface on which the thin film is deposited, to radiation from a direct radiant heat source, thereby heating the substrate to the desired growth temperature, and maintaining the radiation and thereby the desired growth temperature during the deposition of the thin film, and 2) depositing a crystalline thin film of high temperature superconducting oxides onto both the front and back surfaces of a substrate.

Inventors

  • 👤 Dean W. Face

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 03:22
CPC Classifications
H; H10; H10N; H10N60/00; H10N60/01; H10N60/0268; H10N60/0296; H10N60/0408; Y; Y10; Y10S; Y10S505/00; Y10S505/725; Y10S505/73; Y10S505/731

Claims Analysis

Total Claims: 18
Claim 1
Independent Claim 104 words
A process for in-situ depositing a uniform crystalline thin..film of a high temperature superconducting oxide onto a surface of a single crystal substrate having a front surface and a back surface comprising exposing said back surface to direct radiation from a radiant heat source to heat the substrate to a growth temperature of said superconducting oxide, and, while maintaining the radiation, sputtering the thin film onto the front surface, wherein the area of said film simultaneously deposited exceeds 6 cm 2 and the variation in T c from the average T c is plus or minus 2 K over the area of said film.
Claim 2
Dependent Claim 104 words
A process for in-situ depositing a uniform crystalline thin..film of a high temperature superconducting oxide onto a surface of a single crystal substrate having a front surface and a back surface comprising exposing said back surface to direct radiation from a radiant heat source to heat the substrate to a growth temperature of said superconducting oxide, and, while maintaining the radiation, sputtering the thin film onto the front surface, wherein the area of said film simultaneously deposited exceeds 6 cm 2 and the variation in T c from the average T c is plus or minus 2 K over the area of said film.
Claim 3
Dependent Claim 17 words
The process of claim 1 wherein said growth temperature is about 500° C. to about 900° C.
Claim 4
Dependent Claim 36 words
The process of claim 2 wherein said high temperature superconducting oxide is MBa 2 Cu 3 O 7-x , wherein M is Y or a rare earth metal and x is from about 0 to 0.3.
Claim 5
Dependent Claim 27 words
The process of claim 1 wherein said back surface of the substrate is coated with a layer of material to absorb said radiation prior to said exposure.
Claim 6
Dependent Claim 17 words
The process of claim 4 wherein said growth temperature is about 500° C. to about 900° C.
Claim 7
Dependent Claim 36 words
The process of claim 5 wherein said high temperature superconducting oxide is MBa 2 Cu 3 O 7-x , wherein M is Y or a rare earth metal and x is from about 0 to 0.3.
Claim 8
Dependent Claim 18 words
The process of claim 6 wherein said substrate is comprised of a single crystal of LaAlO 3 .
Claim 9
Dependent Claim 175 words
A process for in-situ depositing a first uniform crystalline thin film onto a back surface of a single crystal substrate, and a second uniform thin film onto a front surface of said substrate, said crystalline thin films being the same or different and comprised of high temperature superconducting oxides, said process comprising the steps of (a) forming a crystalline thin film of a first superconducting oxide on the back surface of the substrate, and (b) exposing said thin film formed in (a) on the back surface of the substrate to direct radiation from a radiant heat source thereby heating the substrate to the growth temperature of a second superconducting oxide, and, while maintaining said radiation, depositing by sputtering a second thin film of said second superconducting oxide on the front surface of the substrate, wherein the area of said film deposited on the front surface exceeds 6 cm 2 and the variation in T c from the average T c is a maximum of plus or minus 2 K over the area of said film.
Claim 10
Dependent Claim 175 words
A process for in-situ depositing a first uniform crystalline thin film onto a back surface of a single crystal substrate, and a second uniform thin film onto a front surface of said substrate, said crystalline thin films being the same or different and comprised of high temperature superconducting oxides, said process comprising the steps of (a) forming a crystalline thin film of a first superconducting oxide on the back surface of the substrate, and (b) exposing said thin film formed in (a) on the back surface of the substrate to direct radiation from a radiant heat source thereby heating the substrate to the growth temperature of a second superconducting oxide, and, while maintaining said radiation, depositing by sputtering a second thin film of said second superconducting oxide on the front surface of the substrate, wherein the area of said film deposited on the front surface exceeds 6 cm 2 and the variation in T c from the average T c is a maximum of plus or minus 2 K over the area of said film.
Claim 11
Dependent Claim 23 words
The process of claim 8 wherein the substrate is planar and said thin films are deposited on opposite sides of said planar substrate.
Claim 12
Dependent Claim 17 words
The process of claim 8 wherein said growth temperature is about 500° C. to about 900° C.
Claim 13
Dependent Claim 21 words
The process of claim 10 wherein said first and second high temperature superconducting oxides are the same high temperature superconducting oxide.
Claim 14
Dependent Claim 36 words
The process of claim 11 wherein said high temperature superconducting oxide is MBa 2 Cu 3 O 7-x , wherein M is Y or a rare earth metal and x is from about 0 to 0.3.
Claim 15
Dependent Claim 18 words
The process of claim 12 wherein said substrate is comprised of a single crystal of LaAlO 3 .
Claim 16
Dependent Claim 84 words
The process of claim 8 wherein said crystalline film of the first superconducting oxide is formed on said back surface of the substrate by exposing the front surface of the substrate to direct radiation from a radiant heat source to heat the substrate to a predetermined growth temperature of the first superconducting oxide, and, while maintaining the radiation, sputtering said first superconducting oxide onto said back surface to form in-situ crystalline film, wherein the area of said crystalline film exceeds 6 cm 2 .
Claim 17
Dependent Claim 19 words
The process of claim 14 wherein both said high temperature superconducting oxides are the same high temperature superconducting oxide.
Claim 18
Dependent Claim 35 words
The process of claim 15 wherein said high temperature superconducting oxide is MBa 2 Cu 3 O 7-x wherein M is Y or a rare earth metal and x is from about 0 to 0.3.

References Cited (Backward Citations)

US4598039A Cited
US4940842A Cited
US4913790A Cited
EP0359411A2 Cited
JPH02247384A Cited
US5206216A Cited
JPH0397870A Cited
EP0435765A2 Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1998-08-07 1999-02-06 1999-08-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2002-08-07 2003-02-06 2003-08-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2006-08-07 2007-02-06 2007-08-08 $7700.00 Window Closed / Lapsed

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