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US4460416A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for fabricating in-situ doped polysilicon employing overdamped gradually increasing gas flow rates with constant flow rate ratio

Assignee: Unisys Corp
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Filing: 1982-12-15
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Granted: 1984-07-17
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Expires: 2002-12-15
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Abstract

Abstract A method of fabricating a film of in-situ doped polycrystalline silicon having a surface that is free of microscopic hillocks includes the steps of providing a deposition chamber and a wafer therein on which the film is to be fabricated and introducing one gas containing silicon atoms and another gas containing dopant atoms into said chamber with respective flow rates; wherein the respective flow rates are gradually increased in an overdamped fashion over a start-up time interval of at least one minute from zero to respective steady state values while simultaneously the ratio of the respective flow rates is kept within 25% of the ratio of said steady state values.

Inventors

  • 👤 Casimir J. Wonsowicz

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 09:02
CPC Classifications
H; H10; H10P; H10P14/00; H10P14/40; H10P14/416; C; C23; C23C; C23C16/00; C23C16/22; C23C16/24; C23C16/44; H10P14/20; H10P14/24; H10P14/34; H10P14/3402; H10P14/3404; H10P14/3411; H10P14/3438; H10P14/3441; H10P14/3442

Claims Analysis

Total Claims: 18
Claim 1
Independent Claim 112 words
A method of fabricating a film of in-situ doped polycrystalline silicon having a surface that is free of microscopic hillocks, said method including the steps of: providing a deposition chamber and a wafer therein on which said film is to be fabricated; and introducing one gas containing silicon atoms and another gas containing dopant atoms into said chamber with respective flow rates; wherein said respective flow rates are gradually increased in an overdamped fashion over a start-up time interval of at least one minute from zero to respective steady state values while simultaneously the ratio of said respective flow rates is kept within 25% of the ratio of said steady state values.
Claim 2
Independent Claim 112 words
A method of fabricating a film of in-situ doped polycrystalline silicon having a surface that is free of microscopic hillocks, said method including the steps of: providing a deposition chamber and a wafer therein on which said film is to be fabricated; and introducing one gas containing silicon atoms and another gas containing dopant atoms into said chamber with respective flow rates; wherein said respective flow rates are gradually increased in an overdamped fashion over a start-up time interval of at least one minute from zero to respective steady state values while simultaneously the ratio of said respective flow rates is kept within 25% of the ratio of said steady state values.
Claim 3
Dependent Claim 21 words
A method according to claim 1 wherein the inside of said chamber is maintained at a temperature of 675° C.-725° C.
Claim 4
Dependent Claim 25 words
A method according to claim 2 wherein said respective flow rates are increased from zero to their respective steady state values in an exponential fashion.
Claim 5
Dependent Claim 21 words
A method according to claim 3 wherein said one gas is SiH 4 and said another gas is PH 3 .
Claim 6
Dependent Claim 29 words
A method according to claim 4 wherein said steady state flow rate of SiH 4 is at least ten times said steady state flow rate of PH 3 .
Claim 7
Dependent Claim 30 words
A method according to claim 5 wherein the inside of said chamber is maintained at a pressure of less than one torr while said gases are being introduced into it.
Claim 8
Independent Claim 115 words
A method of fabricating a film of in-situ doped polycrystalline material having a surface that is free of microscopic hillocks, said method including the steps of: providing a deposition chamber and a wafer therein on which said film is to be fabricated; and introducing one gas into said chamber which contains atoms of said polycrystalline material and simultaneously introducing another gas into said chamber which contains dopant atoms for said polycrystalline material; wherein said gases are introduced at respective flow rates which increase in a gradual fashion over a start-up time interval from zero to respective steady state values such that the ratio of said flow rates varies by no more than a predetermined fraction.
Claim 9
Independent Claim 115 words
A method of fabricating a film of in-situ doped polycrystalline material having a surface that is free of microscopic hillocks, said method including the steps of: providing a deposition chamber and a wafer therein on which said film is to be fabricated; and introducing one gas into said chamber which contains atoms of said polycrystalline material and simultaneously introducing another gas into said chamber which contains dopant atoms for said polycrystalline material; wherein said gases are introduced at respective flow rates which increase in a gradual fashion over a start-up time interval from zero to respective steady state values such that the ratio of said flow rates varies by no more than a predetermined fraction.
Claim 10
Dependent Claim 21 words
A method according to claim 7 wherein the inside of said chamber is maintained at a temperature of 675° C.-725° C.
Claim 11
Dependent Claim 29 words
A method according to claim 7 wherein said respective flow rates are limited during said start-up time interval to not overshoot said steady state values by more than 25%.
Claim 12
Dependent Claim 25 words
A method according to claim 7 wherein said respective flow rates are increased from zero to their respective steady state values in an exponential fashion.
Claim 13
Dependent Claim 16 words
A method according to claim 9 wherein said start-up time interval is at least one minute.
Claim 14
Dependent Claim 21 words
A method according to claim 7 wherein said one gas is SiH 4 and said another gas is PH 3 .
Claim 15
Dependent Claim 29 words
A method according to claim 7 wherein said steady state flow rate of SiH 4 is at least ten times said steady state flow rate of PH 3 .
Claim 16
Dependent Claim 30 words
A method according to claim 7 wherein the inside of said chamber is maintained at a pressure of less than one torr while said gases are being introduced into it.
Claim 17
Independent Claim 109 words
A method of fabricating a film of material having a surface that is free of microscopic hillocks, said method including the steps of: providing a deposition chamber and a wafer therein on which said film is to be fabricated; and introducing one gas into said chamber which contains atoms of one type and simultaneously introducing another gas into said chamber which contains atoms of another type; wherein said gases are introduced at respective flow rates which increase from zero to respective steady state values in an overdamped fashion while the ratio of said flow rates is confined to stay within 25% of the ratio of said steady state values.
Claim 18
Independent Claim 109 words
A method of fabricating a film of material having a surface that is free of microscopic hillocks, said method including the steps of: providing a deposition chamber and a wafer therein on which said film is to be fabricated; and introducing one gas into said chamber which contains atoms of one type and simultaneously introducing another gas into said chamber which contains atoms of another type; wherein said gases are introduced at respective flow rates which increase from zero to respective steady state values in an overdamped fashion while the ratio of said flow rates is confined to stay within 25% of the ratio of said steady state values.

References Cited (Backward Citations)

US4087571A Cited
US3945864A Cited
US3930908A Cited
US4100310A Cited
US4217375A Cited
US4313253A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-07-17 1988-01-16 1988-07-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-07-17 1992-01-16 1992-07-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-07-17 1996-01-16 1996-07-17 $7700.00 Window Closed / Lapsed

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