Patent US4144099A successfully refreshed from Google Patents.
US4144099A
Expired / Lapsed
US
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High performance silicon wafer and fabrication process
Assignee: International Business Machines Corp
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Filing: 1977-10-31
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Granted: 1979-03-13
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Expires: 1997-10-31
Abstract
Abstract Gettered semiconductor wafers for integrated circuit device manufacture are prepared by grinding a layer of damage into the back face of the wafer to a depth of about 8-35 microns, heating the wafer to a temperature of about 800 DEG -1150 DEG C. for about 1 to 3 hours and quickly cooling the wafer to a temperature below about 600 DEG C., and polishing both sides of the wafer to form a polished, substantially damage-free front face and a smooth back face which has a residual layer of crystallographic damage to provide additional gettering during device manufacture.
Inventors
- 👤 Harold D. Edmonds
- 👤 Gary Markovits
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-27 23:31
CPC Classifications
H; H10; H10P; H10P90/00; H10P90/12; B; B24; B24B; B24B7/00; B24B7/20; B24B7/22; B24B7/228; H10P36/00; H10P36/03; Y; Y10; Y10S; Y10S148/00; Y10S148/017; Y10S148/024; Y10S148/051; Y10S148/06; Y10S148/061; Y10S148/138; Y10S438/00; Y10S438/974
Claims Analysis
Total Claims: 15
Claim 1
Independent Claim
112 words
A process for preparing a gettered semiconductor wafer comprising: (1) shaping the wafer to form two flat parallel faces and removing damage resulting from said shaping, (2) grinding a layer of damage having a depth of about 8-35 microns in a first face with a rotating abrasive means, (3) heating the wafer in an inert atmosphere for a time and temperature sufficient to getter impurities and to relieve stresses caused by said grinding and quenching said wafer after heating and, (4) polishing said faces to form a smooth surface on the first face, while retaining a layer of crystallographic damage adjacent said face, and to form a polished substantially damage-free second face.
Claim 2
Dependent Claim
112 words
A process for preparing a gettered semiconductor wafer comprising: (1) shaping the wafer to form two flat parallel faces and removing damage resulting from said shaping, (2) grinding a layer of damage having a depth of about 8-35 microns in a first face with a rotating abrasive means, (3) heating the wafer in an inert atmosphere for a time and temperature sufficient to getter impurities and to relieve stresses caused by said grinding and quenching said wafer after heating and, (4) polishing said faces to form a smooth surface on the first face, while retaining a layer of crystallographic damage adjacent said face, and to form a polished substantially damage-free second face.
Claim 3
Dependent Claim
10 words
The process of claim 1 wherein the semiconductor is silicon.
Claim 4
Dependent Claim
21 words
The process of claim 1 wherein the abrasive means is diamond having a grit size ranging from about 100 to 1200.
Claim 5
Dependent Claim
15 words
The process of claim 1 wherein the heating step occurs after grinding and before polishing.
Claim 6
Dependent Claim
61 words
The process of claim 1 wherein the heating step is in a furnace at a temperature of about 800° to 1150° C. for a time of about 1 to 4 hours in a nitrogen atmosphere and the wafer is quenched by removing the wafer to a lower temperature so that it cools to below about 600° C. prior to further processing.
Claim 7
Dependent Claim
13 words
The process of claim 1 wherein the polishing is free polishing with silica.
Claim 8
Dependent Claim
55 words
The process of claim 1 wherein the layer of crystallographic damage consists of a network of substantially linear dislocations terminating upon one another having a defect density of from about 1 × 10 8 to 1 × 10 10 per cm 2 with the network being confined to a plane parallel to the first face.
Claim 9
Dependent Claim
58 words
The process of claim 6 wherein the polishing is performed in two stages in which the second face is single side polished to form a polished, substantially defect surface and then the first and second faces are simultaneously polished such that the second face has a residual layer of crystallographic damage having a depth of about 10-12 microns.
Claim 10
Dependent Claim
14 words
The process of claim 1 wherein the heating step occurs after grinding and polishing.
Claim 11
Dependent Claim
138 words
A process for making a high performance silicon semiconductor wafer with built in gettering prior to device fabrication comprising the steps of: (1) shaping the wafer to form two flat parallel surfaces, (2) chemically treating the wafer to remove damage resulting from said shaping, (3) grinding a layer of damage having a depth of about 8-35 microns in only one of said surfaces with a rotating abrasive means, (4) heating the wafer, after grinding in an inert atmosphere from a time and temperature sufficient to getter impurities and relieve stresses caused by said grinding and quenching said wafer after heating, (5) polishing only the other surface after said heating and quenching and (6) simultaneously free polishing both surfaces to remove cavities from the damaged surface while retaining a residual layer of crystallographic damage for gettering during device fabrication.
Claim 12
Dependent Claim
138 words
A process for making a high performance silicon semiconductor wafer with built in gettering prior to device fabrication comprising the steps of: (1) shaping the wafer to form two flat parallel surfaces, (2) chemically treating the wafer to remove damage resulting from said shaping, (3) grinding a layer of damage having a depth of about 8-35 microns in only one of said surfaces with a rotating abrasive means, (4) heating the wafer, after grinding in an inert atmosphere from a time and temperature sufficient to getter impurities and relieve stresses caused by said grinding and quenching said wafer after heating, (5) polishing only the other surface after said heating and quenching and (6) simultaneously free polishing both surfaces to remove cavities from the damaged surface while retaining a residual layer of crystallographic damage for gettering during device fabrication.
Claim 13
Dependent Claim
45 words
The process of claim 10 wherein the rotating abrasive means is a 400 grit diamond wheel and the heating is in a nitrogen atmosphere at about 1000° C. for about 3 hours and the residual layer damage depth is from about 10 to 12 microns.
Claim 14
Dependent Claim
82 words
A gettered semiconductor wafer having a polished substantially damage-free front surface and a smooth back surface which has a layer of mechanically produced crystallographic damage adjacent to the back surface for gettering during device processing wherein said damage consists of a network of substantially linear dislocations terminating upon one another having a defect density of from about 1 × 10 8 to 1 × 10 10 per cm 2 with the network being confined to a plane parallel to the back surface.
Claim 15
Dependent Claim
82 words
A gettered semiconductor wafer having a polished substantially damage-free front surface and a smooth back surface which has a layer of mechanically produced crystallographic damage adjacent to the back surface for gettering during device processing wherein said damage consists of a network of substantially linear dislocations terminating upon one another having a defect density of from about 1 × 10 8 to 1 × 10 10 per cm 2 with the network being confined to a plane parallel to the back surface.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-03-12 | 1982-09-11 | 1983-03-13 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-03-12 | 1986-09-11 | 1987-03-13 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-03-12 | 1990-09-11 | 1991-03-13 | $7700.00 | Window Closed / Lapsed |