Patent US1362243A successfully refreshed from Google Patents.
Patent US5766697A successfully refreshed from Google Patents.
US5766697A
Expired / Lapsed
US
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Method of making ferrolectric thin film composites
Assignee: United States Department of the Army
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Filing: 1996-11-05
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Granted: 1998-06-16
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Expires: 2016-11-05
Abstract
Abstract A method of making ferroelectric thin film composites includes the step of providing a barium strontium titanate material with an additive magnesia-based and forming a thin film ferroelectric composite using pulsed laser deposition. The method forms a thin film composite having enhanced electronic properties.
Inventors
- 👤 Somnath Sengupta
- 👤 Louise Sengupta
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 15:34
CPC Classifications
C; C23; C23C; C23C14/00; C23C14/22; C23C14/24; C23C14/28; C23C14/06; C23C14/08; C23C14/088
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
183 words
A method of making a thin film of a ferroelectric composite material having a composition comprising: barium strontium titanate, said barium strontium titanate represented as Ba 1-x Sr x TiO 3 , wherein x is greater than 0.0 but less than or equal to 0.75, and an additive selected from the group consisting of mangesia, alumina, silica, a low dielectric oxide, zirconia, and combinations thereof; wherein said barium strontium titanate and said additive are present in effective amounts to provide a composite having a low dielectric constant, low loss tangibles, and high tunability. the method comprising the steps of: a) providing at least one ceramic disc of said composition as an abalation target; b) providing a substrate at a temperature of between 400-700 degrees centigrade, and at a distance between the substrate and target of 25-50 mm; c) depositing a thin file of said composition on said substrate using a krypton exciminer pulsed laser utilizing a laser wavelength of 193-248 nm, a laser pulse energy of 226-350 m/J pulse, a pulse width of 10-20 ns and a pulse repetition rate of 5-25 Hz.
Claim 2
Independent Claim
183 words
A method of making a thin film of a ferroelectric composite material having a composition comprising: barium strontium titanate, said barium strontium titanate represented as Ba 1-x Sr x TiO 3 , wherein x is greater than 0.0 but less than or equal to 0.75, and an additive selected from the group consisting of mangesia, alumina, silica, a low dielectric oxide, zirconia, and combinations thereof; wherein said barium strontium titanate and said additive are present in effective amounts to provide a composite having a low dielectric constant, low loss tangibles, and high tunability. the method comprising the steps of: a) providing at least one ceramic disc of said composition as an abalation target; b) providing a substrate at a temperature of between 400-700 degrees centigrade, and at a distance between the substrate and target of 25-50 mm; c) depositing a thin file of said composition on said substrate using a krypton exciminer pulsed laser utilizing a laser wavelength of 193-248 nm, a laser pulse energy of 226-350 m/J pulse, a pulse width of 10-20 ns and a pulse repetition rate of 5-25 Hz.
Claim 3
Dependent Claim
26 words
The thin film ferroelectric composite material of claim 1, wherein said barium strontium titanate is Ba 1-x Sr x TiO 3 , wherein x=0.35 to 0.40.
Claim 4
Dependent Claim
32 words
The thin film ferroelectric composite material of claim 2, wherein the weight ratio of said barium strontium titanate to said additive ranges from approximately 99%-50% barium strontium titanate to approximately 1%-60% additive.
Claim 5
Dependent Claim
13 words
The thin film ferroelectric composite of claim 1 wherein said additive is magnesia.
Claim 6
Dependent Claim
14 words
The thin film ferroelectric composite of claim 4 wherein said magnesia is about 1%.
Claim 7
Dependent Claim
13 words
The thin film ferroelectric composite of claim 1 wherein said additive is alumina.
Claim 8
Dependent Claim
14 words
The thin film ferroelectric composite of claim 6 wherein said alumina is about 1%.
Claim 9
Dependent Claim
13 words
The thin film ferroelectric composite of claim 1 wherein said additive is zirconia.
Claim 10
Dependent Claim
14 words
The thin film ferroelectric composite of claim 8 wherein said zirconia is about 1%.
Claim 11
Dependent Claim
21 words
The method of claim 1 wherein a plurality of ceramic discs are used, said plurality making up said composition in total.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 2001-06-15 | 2001-12-15 | 2002-06-16 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2005-06-15 | 2005-12-15 | 2006-06-16 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2009-06-15 | 2009-12-15 | 2010-06-16 | $7700.00 | Window Closed / Lapsed |