Patent US5553395A successfully refreshed from Google Patents.
← Back to Patent Explorer
US5553395A Expired / Lapsed US ⏱️ 0.0 years remaining

Bubbler for solid metal organic source material and method of producing saturated carrying gas

Assignee: Raytheon Co
•
Filing: 1995-05-31
•
Granted: 1996-09-10
•
Expires: 2015-05-31
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A cone-shaped bubbler for use with solid metal organic source material used in metal organic chemical vapor phase deposition systems, and a method of producing carrying gas saturated with source material that is injected into such systems. The bubbler comprises a sealed container having a slanted wall with an inverted cone-shaped cross section. Solid metal organic source material is disposed in the container. A heat bath surrounds the sealed container. A carrying gas inlet is disposed adjacent the top of the container. Carrying gas is injected in a tangential direction relative to the source material, and a whirlpool effect is generated by the tangential gas flow that imparts a centrifugal force to gas molecules, pushing the source material against the wall to promote heat flow from the heat bath to sustain high rate sublimation. A gas outlet is disposed adjacent the bottom of the container. Once source material lining the slanted inner wall is removed, gravitational forces cause source material to refill the empty space, reducing channel formation and preventing thermal isolation of the source material at the center of the bubbler. The method comprises providing a sealed container with a slanted wall having an inverted cone-shaped cross section, disposing solid metal organic source material in the container, heating the sealed container, injecting a carrying gas adjacent the top of the container so that carrying gas is injected in a tangential direction relative to the solid source material, and removing saturated carrying gas from a gas outlet disposed adjacent the bottom of the container.

Inventors

  • 👤 Cheng P. Wen
  • 👤 Randy K. Rolph
  • 👤 Timothy T. Zielinski

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 06:04
CPC Classifications
C; C23; C23C; C23C16/00; C23C16/44; C23C16/448; C23C16/4481

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 170 words
A bubbler for use in a metal organic chemical vapor phase deposition system, said bubbler comprising: a sealed container comprising a slanted wall having an inverted cone-shaped cross section; solid metal organic source material disposed in the sealed container; a heat bath surrounding the sealed container; a carrying gas inlet disposed adjacent the top of the inverted cone-shaped container disposed so that carrying gas is injected in a tangential direction relative to the solid source material, and wherein a whirlpool effect is generated by the tangential gas flow that imparts a centrifugal force to gas molecules thereof, pushing the source material against the wall of the bubbler to promote heat flow from the heat bath to sustain high rate sublimation; and a gas outlet disposed adjacent the bottom of the inverted cone-shaped container; whereby once source material lining the slanted wall is removed, gravitational forces cause the source material to refill empty spaces, reducing channel formation and preventing thermal isolation of the source material at the center of the bubbler.
Claim 2
Dependent Claim 170 words
A bubbler for use in a metal organic chemical vapor phase deposition system, said bubbler comprising: a sealed container comprising a slanted wall having an inverted cone-shaped cross section; solid metal organic source material disposed in the sealed container; a heat bath surrounding the sealed container; a carrying gas inlet disposed adjacent the top of the inverted cone-shaped container disposed so that carrying gas is injected in a tangential direction relative to the solid source material, and wherein a whirlpool effect is generated by the tangential gas flow that imparts a centrifugal force to gas molecules thereof, pushing the source material against the wall of the bubbler to promote heat flow from the heat bath to sustain high rate sublimation; and a gas outlet disposed adjacent the bottom of the inverted cone-shaped container; whereby once source material lining the slanted wall is removed, gravitational forces cause the source material to refill empty spaces, reducing channel formation and preventing thermal isolation of the source material at the center of the bubbler.
Claim 3
Dependent Claim 21 words
The bubbler of claim 1 wherein the inverted cone-shaped container has a base angle of from approximately ten to forty-five degrees.
Claim 4
Dependent Claim 13 words
The bubbler of claim 1 wherein the solid source material comprises trimethyl indium.
Claim 5
Dependent Claim 11 words
The bubbler of claim 1 wherein the carrying gas comprises hydrogen.
Claim 6
Independent Claim 172 words
A method of producing a carrying gas saturated with source material that is injected into an epitaxial reactor, said method comprising the steps of: providing a sealed container comprising a slanted side wall having an inverted cone-shaped cross section; disposing solid metal organic source material in the sealed container; heating the sealed container; injecting a carrying gas into the inverted cone-shaped container adjacent the top thereof so that carrying gas is injected in a tangential direction relative to the solid source material, and wherein a whirlpool effect is generated by the tangential gas flow that imparts a centrifugal force to gas molecules thereof, pushing the source material against the wall of the bubbler to promote heat flow from the heat bath to sustain high rate sublimation; and removing saturated carrying gas from a gas outlet disposed adjacent the bottom of the inverted cone-shaped container; whereby gravitational forces cause source material to refill empty spaces, thus reducing channel formation and preventing thermal isolation of the source material at the center of the bubbler.
Claim 7
Independent Claim 172 words
A method of producing a carrying gas saturated with source material that is injected into an epitaxial reactor, said method comprising the steps of: providing a sealed container comprising a slanted side wall having an inverted cone-shaped cross section; disposing solid metal organic source material in the sealed container; heating the sealed container; injecting a carrying gas into the inverted cone-shaped container adjacent the top thereof so that carrying gas is injected in a tangential direction relative to the solid source material, and wherein a whirlpool effect is generated by the tangential gas flow that imparts a centrifugal force to gas molecules thereof, pushing the source material against the wall of the bubbler to promote heat flow from the heat bath to sustain high rate sublimation; and removing saturated carrying gas from a gas outlet disposed adjacent the bottom of the inverted cone-shaped container; whereby gravitational forces cause source material to refill empty spaces, thus reducing channel formation and preventing thermal isolation of the source material at the center of the bubbler.
Claim 8
Dependent Claim 32 words
The method of claim 5 wherein the step of providing a sealed container comprises the step of providing a sealed container having a base angle of from approximately ten to forty-five degrees.
Claim 9
Dependent Claim 30 words
The method of claim 5 wherein the step of disposing solid metal organic source material in the sealed container comprises the step of disposing trimethyl indium in the sealed container.
Claim 10
Dependent Claim 27 words
The method of claim 5 wherein the step of injecting a carrying gas into the inverted cone-shaped container comprises the step of injecting hydrogen into the container.

References Cited (Backward Citations)

US4101263A Cited
US5243767A Cited
US5381605A Cited
US5489166A Cited
US5377429A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1999-09-10 2000-03-11 2000-09-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2003-09-10 2004-03-11 2004-09-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2007-09-10 2008-03-11 2008-09-10 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag