US5547708A
Expired / Lapsed
US
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Chemical vapor deposition method for forming a deposited film with the use of liquid raw material
Assignee: Canon Inc
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Filing: 1994-11-14
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Granted: 1996-08-20
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Expires: 2014-11-14
Abstract
Abstract A chemical vapor deposition method for forming a deposited film on a substrate using a film-forming liquid raw material. The film-forming liquid is pulverized into liquid fine particles which are heated together with a gas to produce a film-forming raw material gas. The film-forming raw material gas is introduced into a reaction chamber where it chemically reacts with a surface of a substrate which is present in the reaction chamber.
Inventors
- 👤 Tetsuo Asaba
- 👤 Kenji Makino
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 12:02
CPC Classifications
C; C23; C23C; C23C16/00; C23C16/22; C23C16/30; C23C16/40; C23C16/401; C23C16/402; C23C16/06; C23C16/18; C23C16/44; C23C16/448; C23C16/4486
Claims Analysis
Total Claims: 14
Claim 1
Independent Claim
192 words
A chemical vapor deposition method for forming a deposited film on a substrate using a film-forming liquid raw material, said chemical vapor deposition method comprises: supplying said film-forming liquid raw material while regulating the amount of said film-forming liquid raw material into a liquid gasifying system comprising a liquid atomizing mechanism and a liquid gasifying mechanism provided with a plurality of plate-like shaped heating members respectively having a plurality of perforations; simultaneously supplying a gas into said liquid gasifying system while controlling the flow rate of said gas, wherein said film-forming liquid raw material is atomized into liquid fine particles which are heated together with said gas while being passed through said perforations of said plurality of plate-like shaped heating members while controlling the temperature of the heating members to produce a film-forming raw material gas; introducing said film-forming raw material gas from said gasifying system into a reaction chamber; and chemically reacting said film-forming raw material gas with a surface of a substrate disposed in said reaction chamber, said substrate being maintained at a temperature, sufficient to thereby cause the formation of a deposited film on said surface of said substrate.
Claim 2
Dependent Claim
192 words
A chemical vapor deposition method for forming a deposited film on a substrate using a film-forming liquid raw material, said chemical vapor deposition method comprises: supplying said film-forming liquid raw material while regulating the amount of said film-forming liquid raw material into a liquid gasifying system comprising a liquid atomizing mechanism and a liquid gasifying mechanism provided with a plurality of plate-like shaped heating members respectively having a plurality of perforations; simultaneously supplying a gas into said liquid gasifying system while controlling the flow rate of said gas, wherein said film-forming liquid raw material is atomized into liquid fine particles which are heated together with said gas while being passed through said perforations of said plurality of plate-like shaped heating members while controlling the temperature of the heating members to produce a film-forming raw material gas; introducing said film-forming raw material gas from said gasifying system into a reaction chamber; and chemically reacting said film-forming raw material gas with a surface of a substrate disposed in said reaction chamber, said substrate being maintained at a temperature, sufficient to thereby cause the formation of a deposited film on said surface of said substrate.
Claim 3
Dependent Claim
26 words
A chemical vapor deposition method according to claim 1, wherein at least one of the plurality of heating members is provided with a heat generating resistor.
Claim 4
Dependent Claim
76 words
A chemical vapor deposition method according to claim 1, wherein said chemical vapor deposition method is conducted so as to satisfy the equation: T 1 <T 2 <T 3 , with T 1 being a temperature of the film-forming liquid raw material upon supplying into the liquid gasifying system, T 2 being a temperature of the heating member upon gasifying the liquid fine particles, and T 3 being a temperature of the substrate upon film formation.
Claim 5
Dependent Claim
27 words
A chemical vapor deposition method according to claim 1, wherein the film-forming raw material is one or more members selected from the group consisting of organometallic compounds.
Claim 6
Dependent Claim
16 words
A chemical vapor deposition method according to claim 4, wherein the organometallic compounds are alkylaluminum hydrides.
Claim 7
Dependent Claim
16 words
A chemical vapor deposition method according to claim 4, wherein the gas is H 2 gas.
Claim 8
Dependent Claim
27 words
A chemical vapor deposition method according to claim 6, wherein the deposited film formed on the substrate is a deposited film containing aluminum as the main constituent.
Claim 9
Dependent Claim
29 words
A chemical vapor deposition method according to claim 1, wherein the film-forming raw material gas is one or more members selected from the group consisting of organic silane compounds.
Claim 10
Dependent Claim
16 words
A chemical vapor deposition method according to claim 8, wherein the gas is O 3 gas.
Claim 11
Dependent Claim
22 words
A chemical vapor deposition method according to claim 9, wherein the deposited film formed on the substrate is a silicon oxide film.
Claim 12
Dependent Claim
211 words
A chemical vapor deposition method for forming a deposited film on a substrate, said chemical vapor deposition method comprises: (a) supplying a film-forming raw material in the liquid state into a gasifying system integrally provided with a plurality of plate-like shaped heating members respectively having a plurality of perforations, a plurality of heat regulators regulating the amount of said film-forming raw material and thermodetectors; (b) supplying a gas reactive with said film-forming raw material into said gasifying system while regulating the flow rate of said gas; (c) introducing said film-forming raw material and said gas from said gasifying system into a reaction chamber having a substrate disposed therein while heating said film-forming raw material and said gas by passing said film-forming raw material and said gas through said perforations of said plurality of plate-like shaped heating members while controlling the temperature of said film-forming raw material and said gas at a desired value by means of said heat regulators and said thermo detectors and while gasifying said film-forming raw material into a gaseous state; and (d) chemically reacting said gasified film-forming raw material and said gas introduced into said reaction chamber to cause the formation of a deposited film on said substrate maintained at a reaction temperature in said reaction chamber.
Claim 13
Dependent Claim
211 words
A chemical vapor deposition method for forming a deposited film on a substrate, said chemical vapor deposition method comprises: (a) supplying a film-forming raw material in the liquid state into a gasifying system integrally provided with a plurality of plate-like shaped heating members respectively having a plurality of perforations, a plurality of heat regulators regulating the amount of said film-forming raw material and thermodetectors; (b) supplying a gas reactive with said film-forming raw material into said gasifying system while regulating the flow rate of said gas; (c) introducing said film-forming raw material and said gas from said gasifying system into a reaction chamber having a substrate disposed therein while heating said film-forming raw material and said gas by passing said film-forming raw material and said gas through said perforations of said plurality of plate-like shaped heating members while controlling the temperature of said film-forming raw material and said gas at a desired value by means of said heat regulators and said thermo detectors and while gasifying said film-forming raw material into a gaseous state; and (d) chemically reacting said gasified film-forming raw material and said gas introduced into said reaction chamber to cause the formation of a deposited film on said substrate maintained at a reaction temperature in said reaction chamber.
Claim 14
Dependent Claim
34 words
A chemical vapor deposition method according to claim 11, wherein the film-forming raw material is one or more members selected from the group consisting of alkylaluminum hydrides and the gas is H 2 gas.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1999-08-20 | 2000-02-19 | 2000-08-20 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2003-08-20 | 2004-02-19 | 2004-08-20 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2007-08-20 | 2008-02-19 | 2008-08-20 | $7700.00 | Window Closed / Lapsed |