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US5397429A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of manufacturing photoluminescing porous silicon using spark erosion

Assignee: University of Florida
•
Filing: 1993-09-14
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Granted: 1995-03-14
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Expires: 2013-09-14
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Abstract

Abstract A high frequency, high voltage spark generator is used to create a large number of sparks to erode the surface of a silicon wafer to a depth of up to 100 microns. After a sufficient amount of erosion has occurred, but prior to any macro-scale removal of material, the surface layer of the silicon wafer becomes porous and photoluminescing. The method can be performed in ambient atmosphere and temperature, or in specific gas atmospheres and at different temperatures. The method produces photoluminescing porous silicon layers on p-type, n-type, low-doped, high-doped or undoped silicon wafers.

Inventors

  • 👤 Rolf E. Hummel
  • 👤 Sung-Sik Chang

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 08:38
CPC Classifications
H; H10; H10H; H10H20/00; H10H20/80; H10H20/81; H10H20/822; H10H20/826; H10H20/8264

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 85 words
A method for the manufacture of a photoluminescing porous silicon layer on a silicon wafer substrate comprising the steps of: (A) providing a high voltage, high frequency spark generator capable of delivering a high number of sparks to the surface of a silicon wafer substrate; (B) eroding a portion of the surface of a silicon wafer substrate to a depth of less than 100 microns by the application of a high number of sparks to said silicon wafer surface to create a porous surface layer.
Claim 2
Independent Claim 85 words
A method for the manufacture of a photoluminescing porous silicon layer on a silicon wafer substrate comprising the steps of: (A) providing a high voltage, high frequency spark generator capable of delivering a high number of sparks to the surface of a silicon wafer substrate; (B) eroding a portion of the surface of a silicon wafer substrate to a depth of less than 100 microns by the application of a high number of sparks to said silicon wafer surface to create a porous surface layer.
Claim 3
Dependent Claim 15 words
The method of claim 1, where said spark generator produces at least approximately 1000 volts.
Claim 4
Dependent Claim 14 words
The method of claim 1, where said spark generator produces at least 10,000 volts.
Claim 5
Dependent Claim 17 words
The method of claim 1, where said spark generator operates at frequencies of at least one kilohertz.
Claim 6
Dependent Claim 13 words
The method of claim 1, where said eroding is performed at room temperature.
Claim 7
Dependent Claim 13 words
The method of claim 1, where said eroding is performed in ambient atmosphere.
Claim 8
Dependent Claim 15 words
The method of claim 1, where said eroding is performed in a specific gas atmosphere.
Claim 9
Dependent Claim 28 words
The method of claim 1, where said porous surface layer comprises particles ranging from 3 to 125 nanometers in diameter and pores ranging from 10 to 2000 nanometers.
Claim 10
Dependent Claim 13 words
The method of claim 1, where said spark generator comprises a metal electrode.
Claim 11
Dependent Claim 13 words
The method of claim 1, where said spark generator comprises a silicon electrode.

References Cited (Backward Citations)

US5279737A Cited
US5272355A Cited
US5318676A Cited
US5301204A Cited
US5256339A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1998-03-13 1998-09-12 1999-03-14 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2002-03-13 2002-09-12 2003-03-14 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2006-03-13 2006-09-12 2007-03-14 $7700.00 Window Closed / Lapsed

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