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US5125574A Expired / Lapsed US ⏱️ 0.0 years remaining

Atomizing nozzle and process

Assignee: Iowa State University Research Foundation Inc
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Filing: 1990-10-09
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Granted: 1992-06-30
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Expires: 2010-10-09
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Abstract

Abstract High pressure atomizing nozzle includes a high pressure gas manifold having a divergent expansion chamber between a gas inlet and arcuate manifold segment to minimize standing shock wave patterns in the manifold and thereby improve filling of the manifold with high pressure gas for improved melt atomization. The atomizing nozzle is especially useful in atomizing rare earth-transition metal alloys to form fine powder particles wherein a majority of the powder particles exhibit particle sizes having near-optimum magnetic properties.

Inventors

  • 👤 Iver E. Anderson
  • 👤 Richard S. Figliola
  • 👤 Holly M. Molnar

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 17:02
CPC Classifications
B; B22; B22F; B22F9/00; B22F9/02; B22F9/06; B22F9/08; B22F9/082

Claims Analysis

Total Claims: 30
Claim 1
Independent Claim 108 words
A high pressure gas atomizing nozzle for atomizing a melt, comprising: a) a melt supply member, b) a gas manifold for receiving high pressure gas, said manifold comprising a gas inlet in communication with a source of high pressure gas, a divergent first manifold chamber in communication with the gas inlet, and a second manifold chamber in communication with said divergent manifold chamber, said first manifold chamber diverging from the gas inlet toward the second manifold chamber, and c) a plurality of discrete gas discharge orifices disposed around the melt supply member and in communication with the manifold for discharging high pressure gas streams to atomize said melt.
Claim 2
Dependent Claim 108 words
A high pressure gas atomizing nozzle for atomizing a melt, comprising: a) a melt supply member, b) a gas manifold for receiving high pressure gas, said manifold comprising a gas inlet in communication with a source of high pressure gas, a divergent first manifold chamber in communication with the gas inlet, and a second manifold chamber in communication with said divergent manifold chamber, said first manifold chamber diverging from the gas inlet toward the second manifold chamber, and c) a plurality of discrete gas discharge orifices disposed around the melt supply member and in communication with the manifold for discharging high pressure gas streams to atomize said melt.
Claim 3
Dependent Claim 17 words
The nozzle of claim 1 wherein said second manifold chamber comprises a constant cross-section, arcuate manifold chamber.
Claim 4
Dependent Claim 54 words
The nozzle of claim 2 wherein the arcuate manifold chamber has an inner radius r 0 and an outer radius r 1 relative to a central axis of said manifold, and said expansion chamber has a dimension r 2 relative to said central axis wherein r 2 -r 0 ≧2(r 1 -r 0 ).
Claim 5
Dependent Claim 15 words
The nozzle of claim 3 wherein r 2 -r 0 δ2.5(r 1 -r 0 ).
Claim 6
Dependent Claim 24 words
The nozzle of claim 1 wherein the gas manifold is disposed in a nozzle body having a bore that receives said melt supply member.
Claim 7
Dependent Claim 22 words
The nozzle of claim 5 wherein the gas discharge orifices each intersect the bore at a tangency thereto not exceeding 0.002 inch.
Claim 8
Dependent Claim 17 words
The nozzle of claim 6 wherein the tangency of said discharge orifices does not exceed 0.001 inch.
Claim 9
Dependent Claim 20 words
The nozzle of claim 1 wherein the expansion chamber diverges at an included angle of about 40° to about 90°.
Claim 10
Dependent Claim 13 words
The nozzle of claim 8 wherein the included angle is about 64 degrees.
Claim 11
Dependent Claim 116 words
In a method of atomizing a rare earth-transition metal alloy melt by supplying high pressure gas to a gas manifold communicating to a plurality of discrete gas discharge orifices disposed around a melt supply member, the improvement comprising supplying the high pressure gas to a gas manifold having a divergent first manifold chamber disposed between a manifold gas inlet and a second manifold chamber communicating to said orifices, said first manifold chamber diverging from said gas inlet toward said second manifold chamber so as to reduce standing shock wave patterns in said manifold and thereby improve filling of said manifold with the high pressure gas that is discharged from the discharge orifices for atomizing the melt.
Claim 12
Dependent Claim 116 words
In a method of atomizing a rare earth-transition metal alloy melt by supplying high pressure gas to a gas manifold communicating to a plurality of discrete gas discharge orifices disposed around a melt supply member, the improvement comprising supplying the high pressure gas to a gas manifold having a divergent first manifold chamber disposed between a manifold gas inlet and a second manifold chamber communicating to said orifices, said first manifold chamber diverging from said gas inlet toward said second manifold chamber so as to reduce standing shock wave patterns in said manifold and thereby improve filling of said manifold with the high pressure gas that is discharged from the discharge orifices for atomizing the melt.
Claim 13
Dependent Claim 32 words
The method of claim 10 wherein the high pressure gas is supplied to gas discharge orifices that each intersect a melt supply member-receiving bore at a tangency thereto not exceeding 0.002 inch.
Claim 14
Dependent Claim 17 words
The method of claim 11 wherein the tangency of said discharge orifices does not exceed 0.001 inch.
Claim 15
Dependent Claim 67 words
The method of claim 10 wherein the high pressure gas is supplied form the divergent manifold chamber to the second manifold chamber having an inner radius r 0 and an outer radius r 1 relative to a central axis of said manifold via said divergent manifold chamber having a dimension r 2 relative to said central axis wherein r 2 -r 0 ≧2(r 1 -r 0 ).
Claim 16
Dependent Claim 15 words
The method of claim 13 wherein r 2 -r 0 δ2.5(r 1 -r 0 ).
Claim 17
Dependent Claim 24 words
The method of claim 10 wherein the divergent manifold chamber is formed to diverge at an included angle of about 40° to about 90°.
Claim 18
Dependent Claim 13 words
The method of claim 15 wherein the included angle is about 64 degrees.
Claim 19
Independent Claim 88 words
A method of making an improved high pressure gas atomizing nozzle having a bore for receiving a melt supply member, comprising the steps of: a) forming said bore to an initial, undersized, lateral dimension, b) forming a plurality of discrete gas discharge orifices about said bore and intersecting therewith at a given angle, and c) forming the bore to a final, lateral dimension larger than said undersized dimension such that the gas discharge orifices are each at a tangency to said final-dimensioned bore not exceeding about 0.002 inch.
Claim 20
Independent Claim 88 words
A method of making an improved high pressure gas atomizing nozzle having a bore for receiving a melt supply member, comprising the steps of: a) forming said bore to an initial, undersized, lateral dimension, b) forming a plurality of discrete gas discharge orifices about said bore and intersecting therewith at a given angle, and c) forming the bore to a final, lateral dimension larger than said undersized dimension such that the gas discharge orifices are each at a tangency to said final-dimensioned bore not exceeding about 0.002 inch.
Claim 21
Dependent Claim 24 words
The method of claim 17 wherein the said discharge orifices are formed at a tangency to said final-dimensioned bore not exceeding about 0.001 inch.
Claim 22
Dependent Claim 60 words
In a high pressure gas atomizing nozzle having a melt supply member for supplying a melt for atomization, the improvement wherein the melt supply member comprises an inner refractory tubular member having a melt supply orifice, and an outer metallic tubular member spaced from the inner refractory body to form a thermal insulating space between the inner and outer members.
Claim 23
Dependent Claim 60 words
In a high pressure gas atomizing nozzle having a melt supply member for supplying a melt for atomization, the improvement wherein the melt supply member comprises an inner refractory tubular member having a melt supply orifice, and an outer metallic tubular member spaced from the inner refractory body to form a thermal insulating space between the inner and outer members.
Claim 24
Dependent Claim 28 words
The combination of claim 19 wherein the inner member includes a lateral, annular flange disposed on an annular shoulder of the outer member proximate an upper end thereof.
Claim 25
Dependent Claim 144 words
A high pressure gas atomizing nozzle for atomizing a melt, comprising: a) a melt supply member, b) a gas manifold for receiving high pressure gas, said manifold comprising a gas inlet in communication with a source of high pressure gas, a divergent first manifold chamber in communication with the gas inlet, and a second manifold chamber in communication with said divergent manifold chamber, said arcuate manifold chamber having an inner radius r 0 and an outer radius r 1 relative to a central axis of said manifold and said divergent first manifold chamber having a dimension r 2 relative to said central axis wherein r 2 -r 0 ≧2(r 1 -r 0 ), and c) a plurality of discrete gas discharge orifices disposed around the melt supply member and in communication with the manifold for discharging high pressure gas streams to atomize said melt.
Claim 26
Dependent Claim 144 words
A high pressure gas atomizing nozzle for atomizing a melt, comprising: a) a melt supply member, b) a gas manifold for receiving high pressure gas, said manifold comprising a gas inlet in communication with a source of high pressure gas, a divergent first manifold chamber in communication with the gas inlet, and a second manifold chamber in communication with said divergent manifold chamber, said arcuate manifold chamber having an inner radius r 0 and an outer radius r 1 relative to a central axis of said manifold and said divergent first manifold chamber having a dimension r 2 relative to said central axis wherein r 2 -r 0 ≧2(r 1 -r 0 ), and c) a plurality of discrete gas discharge orifices disposed around the melt supply member and in communication with the manifold for discharging high pressure gas streams to atomize said melt.
Claim 27
Dependent Claim 15 words
The nozzle of claim 23 wherein r 2 -r 0 δ2.5(r 1 -r 0 ).
Claim 28
Dependent Claim 146 words
In a method of atomizing a rare earth-transition metal alloy melt by supplying high pressure gas to a gas manifold communicating to a plurality of discrete gas discharge orifices disposed about a melt supply member, the improvement comprising supplying the high pressure gas to a gas manifold having a divergent first manifold chamber disposed between a manifold gas inlet and a second manifold chamber communicating to said orifices and having an inner radius r 0 and an outer radius r 1 relative to a central axis of said manifold, said first manifold chamber having a dimension r 2 relative to said central axis wherein r 2 -r 0 ≧2(r 1 -r 0 ) so as to reduce standing shock wave patterns in said manifold and thereby improve filling of said manifold with the high pressure gas that is discharged from the orifices for atomizing the melt.
Claim 29
Dependent Claim 146 words
In a method of atomizing a rare earth-transition metal alloy melt by supplying high pressure gas to a gas manifold communicating to a plurality of discrete gas discharge orifices disposed about a melt supply member, the improvement comprising supplying the high pressure gas to a gas manifold having a divergent first manifold chamber disposed between a manifold gas inlet and a second manifold chamber communicating to said orifices and having an inner radius r 0 and an outer radius r 1 relative to a central axis of said manifold, said first manifold chamber having a dimension r 2 relative to said central axis wherein r 2 -r 0 ≧2(r 1 -r 0 ) so as to reduce standing shock wave patterns in said manifold and thereby improve filling of said manifold with the high pressure gas that is discharged from the orifices for atomizing the melt.
Claim 30
Dependent Claim 15 words
The method of claim 23 wherein r 2 -r 0 δ2.5(r 1 -r 0 ).

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1995-06-30 1995-12-30 1996-06-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1999-06-30 1999-12-30 2000-06-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2003-06-30 2003-12-30 2004-06-30 $7700.00 Window Closed / Lapsed

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