Patent US4970038A successfully refreshed from Google Patents.
US4970038A
Expired / Lapsed
US
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Process of preparing polyester yarn
Assignee: BASF Corp
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Filing: 1988-11-29
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Granted: 1990-11-13
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Expires: 2008-11-29
Abstract
Abstract A yarn comprising polyester fibers having an improved balance of properties (tenacity and boiling water shrinkage) is produced within predetermined limits. The polyester yarn is prepared by cold drawing a partially oriented feeder yarn, partially annealing the drawn yarn, and subsequently annealing the partially annealed cold drawn yarn at controlled tensions.
Inventors
- 👤 Wayne S. Stanko
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 20:55
CPC Classifications
D; D02; D02J; D02J1/00; D02J1/22; D02J1/229; D01; D01F; D01F6/00; D01F6/58; D01F6/62
Claims Analysis
Total Claims: 18
Claim 1
Independent Claim
127 words
A process of preparing polyester yarn having predetermined limits with respect to tenacity and boiling water shrinkage comprising: (a) drawing at ambient temperature a partially oriented feeder yarn comprising polyester filaments having a birefringence of at least 0.0175 at a draw ratio in the range of from about 1.75 to about 260; (b) partially annealing the drawn feeder yarn of step (a) at a temperature in the range of from about 70° C. to about 110° C., said drawing and said partial annealing occurring substantially sequentially; and, (c) annealing the partially annealed feeder yarn of step (b) at a tension in the range of from about at least 0.001 grams to about 50 grams and at a temperature of from about 110° C. to about 160° C.
Claim 2
Dependent Claim
127 words
A process of preparing polyester yarn having predetermined limits with respect to tenacity and boiling water shrinkage comprising: (a) drawing at ambient temperature a partially oriented feeder yarn comprising polyester filaments having a birefringence of at least 0.0175 at a draw ratio in the range of from about 1.75 to about 260; (b) partially annealing the drawn feeder yarn of step (a) at a temperature in the range of from about 70° C. to about 110° C., said drawing and said partial annealing occurring substantially sequentially; and, (c) annealing the partially annealed feeder yarn of step (b) at a tension in the range of from about at least 0.001 grams to about 50 grams and at a temperature of from about 110° C. to about 160° C.
Claim 3
Dependent Claim
37 words
The process recited in claim 1 wherein said polyester yarn has a tenacity in the range of from about 4.5 to about 7.0 g/denier and a boiling water shrinkage of from about 2 to about 10 percent.
Claim 4
Dependent Claim
14 words
The process recited in claim 2 wherein said polyester is a linear terephthalate polyester.
Claim 5
Dependent Claim
14 words
The process recited in claim 3 wherein said linear terephthalate polyester is poly(ethylene terephthalate).
Claim 6
Dependent Claim
24 words
The process recited in claim 4 wherein said birefringence of said feeder yarn is in the range of from about 0.020 to about 0.037.
Claim 7
Dependent Claim
78 words
The process recited in claim 5 wherein the preparation of said feeder yarn comprises: (i) extruding molten poly(ethylene terephthalate) having an intrinsic viscosity in the range of from about 0.4 to about 0.8 through a spinneret to form one or more filaments; (ii) quenching said filaments; (iii) applying an aqueous lubricating finish to said quenched filaments; and, (iv) taking up said filaments at a speed in the range of from about 2,200 to about 3,000 meters per minute.
Claim 8
Dependent Claim
21 words
The process recited in claim 6 wherein said fibers are taken up at a speed of about 2,750 meters per minute.
Claim 9
Dependent Claim
20 words
The process recited in claim 7 wherein said draw ratio of step (a) is from about 2.00 to about 2.50.
Claim 10
Dependent Claim
25 words
The process recited in claim 8 wherein said annealing temperature of step (b) is in the range of from about 90° to about 110° C.
Claim 11
Dependent Claim
26 words
The process recited in claim 9 wherein said tension of step (c) is an amount in the range of from about 20 to about 50 grams.
Claim 12
Dependent Claim
26 words
The process recited in claim 9 wherein said tension of step (c) is an amount in the range of from about 0.001 to about 10 grams.
Claim 13
Dependent Claim
158 words
A process of preparing polyester yarn having a tenacity in the range of from about 6.0 to about 7.5 grams per denier, a boiling water shrinkage in the range of from about 5 to about 10%, and an elongation in the range of from about 12 to about 15%, comprising: (a) drawing at ambient temperature a partially oriented feeder yarn comprising polyester filaments having a birefringence of at least 0.0175 at a draw ratio in the range of from about 2.20 to about 2.60; (b) partially annealing the feeder yarn of step (a) at a temperature in the range of from about 90° C. to about 110° C., said drawing and said partial annealing occurring substantially sequentially; and, (c) annealing the partially annealed feeder yarn of step (b) at a tension in the range of from about at least 20 grams to about 50 grams and at a temperature of from about 130° C. to about 160° C.
Claim 14
Dependent Claim
158 words
A process of preparing polyester yarn having a tenacity in the range of from about 6.0 to about 7.5 grams per denier, a boiling water shrinkage in the range of from about 5 to about 10%, and an elongation in the range of from about 12 to about 15%, comprising: (a) drawing at ambient temperature a partially oriented feeder yarn comprising polyester filaments having a birefringence of at least 0.0175 at a draw ratio in the range of from about 2.20 to about 2.60; (b) partially annealing the feeder yarn of step (a) at a temperature in the range of from about 90° C. to about 110° C., said drawing and said partial annealing occurring substantially sequentially; and, (c) annealing the partially annealed feeder yarn of step (b) at a tension in the range of from about at least 20 grams to about 50 grams and at a temperature of from about 130° C. to about 160° C.
Claim 15
Dependent Claim
12 words
The process recited in claim 12 wherein said polyester is poly(ethylene terephthalate).
Claim 16
Dependent Claim
159 words
A process of preparing polyester yarn having a tenacity in the range of from about 4.5 to about 5.5 grams per denier, a boiling water shrinkage in the range of from about 2 to about 3%, and an elongation in the range of from about 25 to about 35% comprising: (a) drawing at ambient temperature a partially oriented feeder yarn comprising polyester filaments having a birefringence of at least 0.0175 at a draw ratio in the range of from about 1.95 to about 2.05: (b) partially annealing the drawn feeder yarn of step (a) at a temperature in the range of from about 80° C. to about 100° C., said drawing and said partial annealing occurring substantially sequentially; and, (c) annealing the partially annealed feeder yarn of step (b) at a tension in the range of from about at least 0.001 grams to about 5 grams and at a temperature of from about 140° C. to about 160° C.
Claim 17
Dependent Claim
159 words
A process of preparing polyester yarn having a tenacity in the range of from about 4.5 to about 5.5 grams per denier, a boiling water shrinkage in the range of from about 2 to about 3%, and an elongation in the range of from about 25 to about 35% comprising: (a) drawing at ambient temperature a partially oriented feeder yarn comprising polyester filaments having a birefringence of at least 0.0175 at a draw ratio in the range of from about 1.95 to about 2.05: (b) partially annealing the drawn feeder yarn of step (a) at a temperature in the range of from about 80° C. to about 100° C., said drawing and said partial annealing occurring substantially sequentially; and, (c) annealing the partially annealed feeder yarn of step (b) at a tension in the range of from about at least 0.001 grams to about 5 grams and at a temperature of from about 140° C. to about 160° C.
Claim 18
Dependent Claim
12 words
The process recited in claim 14 wherein said polyester is poly(ethylene terephthalate).
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
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| 3.5 Years (Year 4) | 1993-11-12 | 1994-05-14 | 1994-11-13 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1997-11-12 | 1998-05-14 | 1998-11-13 | $3760.00 | Window Closed / Lapsed |
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