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Patent US4623356A successfully refreshed from Google Patents.
US4623356A
Expired / Lapsed
US
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Oxidative afterwash treatment for non-formaldehyde durable press finishing process
Assignee: Springs Industries Inc
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Filing: 1984-11-06
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Granted: 1986-11-18
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Expires: 2004-11-06
Abstract
Abstract A method for preventing discoloration of durable press fabrics containing cellulosic fibers that have been previously finished using a non-formaldehyde finishing agent such as glyoxal in which the fabric is treated with an oxidative afterwash solution at elevated temperature followed by neutralization, rinsing and drying. The oxidative afterwash treatment may be performed in a continuous process as part of or immediately following the durable press finishing operation, or at a later time in a totally separate process.
Inventors
- 👤 James E. Hendrix
- 👤 Kimberley J. Lane
- 👤 John Y. Daniels
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 11:28
CPC Classifications
D; D06; D06C; D06C3/00; D06C3/02; D06L; D06L4/00; D06L4/20; D06L4/22; D06L4/23; D06L4/24
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
125 words
In a method of obtaining a durable press textile fabric containing cellulosic fibers, wherein said textile fabric has been treated with a non-formaldehyde finishing agent taken from the group consisting essentially of glyoxal, non-formaldehyde polymers of glyoxal and aldehydes, the improvement characterized in that said textile fabric is subjected to an oxidative afterwash treatment following treatment with said non-formaldehyde finishing agent to prevent yellowing of said fabric upon storage, said afterwash treatment comprising the steps of: washing said fabric a first time in an oxidative solution containing an oxidate, a stabilizer compound, a base, and a surfactant; washing said fabric a second time in a neutralizing solution to thereby neutralize said oxidant; rinsing said textile fabric in an aqueous solution; and drying said textile fabric.
Claim 2
Dependent Claim
125 words
In a method of obtaining a durable press textile fabric containing cellulosic fibers, wherein said textile fabric has been treated with a non-formaldehyde finishing agent taken from the group consisting essentially of glyoxal, non-formaldehyde polymers of glyoxal and aldehydes, the improvement characterized in that said textile fabric is subjected to an oxidative afterwash treatment following treatment with said non-formaldehyde finishing agent to prevent yellowing of said fabric upon storage, said afterwash treatment comprising the steps of: washing said fabric a first time in an oxidative solution containing an oxidate, a stabilizer compound, a base, and a surfactant; washing said fabric a second time in a neutralizing solution to thereby neutralize said oxidant; rinsing said textile fabric in an aqueous solution; and drying said textile fabric.
Claim 3
Dependent Claim
34 words
A method according to claim 1, wherein said oxidant is taken from the group consisting essentially of sodium peroxide, sodium perborate, sodium percarbonate, hydrogen peroxide, sodium perchlorate potassium periodate, peroxyphosphates, peroxysulfates and organic peracids.
Claim 4
Dependent Claim
32 words
A method according to claim 1 wherein said stabilizer comprises one or more compounds taken from the group consisting essentially of sodium silicate, phosphate esters, magnesium salts, phenols, amines, amides, and phosphates.
Claim 5
Dependent Claim
15 words
A method according to claim 1, wherein said oxidative solution further comprises a chelating agent.
Claim 6
Dependent Claim
15 words
A method according to claim 1, wherein said neutralizing solution contains a dilute organic acid.
Claim 7
Dependent Claim
36 words
A method according to claim 1, wherein said textile fabric is exposed to said oxidative solution for a period of time between 5 seconds and 5 minutes and at a temperature between 40° and 200° F.
Claim 8
Dependent Claim
35 words
A method according to claim 1, wherein said textile fabric is exposed to said oxidative solution for a period of time between 5 and 90 seconds and at a temperature between 160° and 180° F.
Claim 9
Dependent Claim
23 words
A method according to claim 1, wherein said textile fabric is subjected to said oxidative afterwash treatment simultaneously with said non-formaldehyde finishing agent.
Claim 10
Dependent Claim
36 words
A method according to claim 1, wherein the concentration of said oxidant in said oxidative solution is maintained at a level equal to or less than 1% based on the total weight of said oxidative solution.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1989-11-17 | 1990-05-19 | 1990-11-18 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1993-11-17 | 1994-05-19 | 1994-11-18 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1997-11-17 | 1998-05-19 | 1998-11-18 | $7700.00 | Window Closed / Lapsed |