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US4600514A Expired / Lapsed US ⏱️ 0.0 years remaining

Controlled gel time for solidification of multi-phased wastes

Assignee: Chem-Technics Inc
•
Filing: 1983-09-15
•
Granted: 1986-07-15
•
Expires: 2003-09-15
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Abstract

Abstract A method of controlling the gelling time during the solidification of multi-phased liquid and semi-liquid wastes comprising admixing the waste with cement, a powdered alkali metal silicate and a liquid alkali metal silicate.

Inventors

  • 👤 Jesse R. Conner

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 11:15
CPC Classifications
C; C02; C02F; C02F11/00; C02F11/008; C04; C04B; C04B28/00; C04B28/24; C04B28/26; Y; Y02; Y02W; Y02W30/00; Y02W30/50; Y02W30/91

Claims Analysis

Total Claims: 16
Claim 1
Independent Claim 89 words
A method of controlling the gelling time during the solidification of liquid and semi-liquid wastes, comprising the steps of: admixing the waste with cement, a powdered alkali metal silicate, and a liquid alkali metal silicate in relative quantities sufficient to cause the admixture to gell and set to a sedentary mass, the relative proportion of said powdered alkali metal silicate to said liquid alkali metal silicate being selected to cause the admixture to gel within a predetermined time; and thereafter allowing the admixture to set to a sedentary mass.
Claim 2
Independent Claim 89 words
A method of controlling the gelling time during the solidification of liquid and semi-liquid wastes, comprising the steps of: admixing the waste with cement, a powdered alkali metal silicate, and a liquid alkali metal silicate in relative quantities sufficient to cause the admixture to gell and set to a sedentary mass, the relative proportion of said powdered alkali metal silicate to said liquid alkali metal silicate being selected to cause the admixture to gel within a predetermined time; and thereafter allowing the admixture to set to a sedentary mass.
Claim 3
Dependent Claim 25 words
The method of claim 1, further comprising the step of admixing a dry water absorbent material having fine particles, said particles having high surface area.
Claim 4
Dependent Claim 34 words
The method of claim 2, wherein said water absorbent material is selected from the group consisting of clay, diatomaceous earth, calcium silicate, fumed silica, acrylic polymers, styrene polymers, natural gums, organo-aluminum compounds, and cellulosics.
Claim 5
Dependent Claim 11 words
The method of claim 1, wherein said cement comprises Portland cement.
Claim 6
Dependent Claim 14 words
The method of claim 1, wherein said powdered alkali metal silicate comprises sodium metasilicate.
Claim 7
Dependent Claim 16 words
The method of claim 1, wherein said liquid alkali metal silicate comprises a sodium silicate solution.
Claim 8
Dependent Claim 23 words
The method of claim 6, wherein said sodium silicate solution is between about 1% to about 45% sodium silicate by weight in water.
Claim 9
Dependent Claim 26 words
The method of claim 1, wherein the amount of said liquid alkali metal silicate added to the waste is between about 0.1% and 10% by volume.
Claim 10
Dependent Claim 35 words
The method of claim 1, wherein the amount of said powdered alkali metal silicate added to the waste is between about 0.01 pound per gallon of waste and about 1 pound per gallon of waste.
Claim 11
Dependent Claim 29 words
The method of claim 1, wherein the gel time of the admixture is increased by increasing the proportion of powdered alkali metal silicate to the liquid alkali metal silicate.
Claim 12
Dependent Claim 29 words
The method of claim 1, wherein the gel time of the admixture is decreased by decreasing the relative proportion of powdered alkli metal silicate to liquid alkali metal silicate.
Claim 13
Dependent Claim 10 words
The method of claim 1, wherein the waste is aqueous.
Claim 14
Dependent Claim 15 words
The method of claim 12, wherein the waste is multi-phased, whereby phase separation is prevented.
Claim 15
Dependent Claim 35 words
The method of claim 1, wherein the waste is non-aqueous, and further comprising the step of admixing with the waste water in an amount sufficient to cause the admixture to set to a sedentary mass.
Claim 16
Dependent Claim 24 words
The method of claim 1, wherein the powdered alkali metal silicate and the liquid alkali metal silicate are added to the waste substantially simultaneously.

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-07-14 1990-01-13 1990-07-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-07-14 1994-01-13 1994-07-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-07-14 1998-01-13 1998-07-15 $7700.00 Window Closed / Lapsed

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