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Patent US4147598A successfully refreshed from Google Patents.
US4147598A
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Method for producing colored anodic oxide films on aluminum based alloy materials
Assignee: Riken Keikinzoku Kogyo KK
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Filing: 1977-09-22
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Granted: 1979-04-03
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Expires: 1997-09-22
Abstract
Abstract Method for producing colored anodic oxide films on aluminum-based alloy materials comprising steps of subjecting the material having an oxide film thereon to a coloring electrolytic treatment in a bath of electrolyte containing water soluble nickel salt and boric acid. The material is applied with alternating voltage pulses having negative pulse duration which is the same as or greater than duration of positive voltage pulse.
Inventors
- 👤 Fumio Shigeta
- 👤 Kazuyoshi Kaneda
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 05:52
CPC Classifications
C; C25; C25D; C25D11/00; C25D11/02; C25D11/04; C25D11/18; C25D11/20; C25D11/22; Y; Y10; Y10S; Y10S204/00; Y10S204/09
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
157 words
A method for producing coloured oxide films comprising subjecting an aluminum based material to an anodizing treatment to produce an oxide film thereon, dipping the material in an electrolyte bath containing from about 70 to about 150 grams of water-soluble nickel salt per liter of water and from about 20 to about 50 grams of boric acid per liter of water, wherein the bath is maintained at a temperature between about 20° and about 22° C., and applying alternating voltage pulses to the aluminum based material, the alternating voltage pulses including more than one negative voltage pulse and more than one positive voltage pulse, and wherein the negative voltage puses have a duration which is at least the same as that of the positive voltage pulses, the negative voltage pulses have a range of from about 12.5 to about 15 volts, and the positive voltage pulses have a range of from about 5.5 to about 13 volts.
Claim 2
Independent Claim
157 words
A method for producing coloured oxide films comprising subjecting an aluminum based material to an anodizing treatment to produce an oxide film thereon, dipping the material in an electrolyte bath containing from about 70 to about 150 grams of water-soluble nickel salt per liter of water and from about 20 to about 50 grams of boric acid per liter of water, wherein the bath is maintained at a temperature between about 20° and about 22° C., and applying alternating voltage pulses to the aluminum based material, the alternating voltage pulses including more than one negative voltage pulse and more than one positive voltage pulse, and wherein the negative voltage puses have a duration which is at least the same as that of the positive voltage pulses, the negative voltage pulses have a range of from about 12.5 to about 15 volts, and the positive voltage pulses have a range of from about 5.5 to about 13 volts.
Claim 3
Dependent Claim
26 words
The method in accordance with claim 1 wherein the water-soluble nickel salt is selected from the group consisting of nickel acetate, nickel sulfate and nickel chloride.
Claim 4
Dependent Claim
15 words
The method in accordance with claim 2 wherein the water-soluble nickel salt is nickel sulfate.
Claim 5
Dependent Claim
25 words
The method in accordance with claim 1 wherein the bath contains from about 100 to about 150 grams of nickel salt per liter of water.
Claim 6
Dependent Claim
24 words
The method in accordance with claim 1 wherein the positive voltage pulses are applied in durations of from about 1 to about 3 seconds.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-04-02 | 1982-10-02 | 1983-04-03 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-04-02 | 1986-10-02 | 1987-04-03 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-04-02 | 1990-10-02 | 1991-04-03 | $7700.00 | Window Closed / Lapsed |