← Back to Patent Explorer
USRE31355E Expired / Lapsed US ⏱️ 0.0 years remaining

Method for hot consolidating powder

Assignee: Dow Chemical Co
•
Filing: 1981-02-23
•
Granted: 1983-08-23
•
Expires: 2001-02-23
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A .[.container.]. .Iadd.method .Iaddend.for hot consolidating powder of metallic and non-metallic composition and combinations thereof by the application of heat and pressure .[.wherein the.]. .Iadd.to a thick-walled and regularly shaped .Iaddend.container .[.includes.]. .Iadd.having .Iaddend.a mass of container material which is substantially fully dense and incompressible and is capable of plastic flow at .[.pressing.]. .Iadd.conventinal compaction .Iaddend.temperatures, a cavity of .[.a predetermined.]. .Iadd.an irregular .Iaddend.shape formed within the mass for receiving a quantity of powder, the mass including walls around the cavity of sufficient thickness so that the exterior surface thereof does not closely follow the contour of the cavity whereby, upon the application of heat and pressure to the container, the mass acts like a fluid to apply hydrostatic pressure to the powder contained in the cavity.

Inventors

  • 👤 Walter J. Rozmus

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 21:40
CPC Classifications
B; B22; B22F; B22F3/00; B22F3/12; B22F3/14; B22F3/15; B22F3/156; B22F3/1208; B22F2998/00

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 207 words
A method for hot consolidating powder of metallic and non-metallic composition and combinations thereof to form a densified .Iadd.and irregularly shaped .Iaddend.compact, said method comprising the steps of: (a) providing a container by forming a cavity having the general .Iadd.irregular .Iaddend.shape of the compact to be produced in a mass of container material which is substantially fully dense and incompressible and is capable of plastic flow at elevated temperatures, the volume of said mass being sufficiently large with respect to the volume of said cavity to form walls entirely surrounding said cavity of sufficient thickness so that the exterior surface of the walls .Iadd.are regularly shaped and .Iaddend.do not closely follow the contour of said cavity, (b) filling said cavity with a powder to be compacted, (c) hermetically sealing said container, (d) .Iadd.applying conventional compaction temperatures and pressures by .Iaddend.heating said container and powder to a temperature at which said mass is capable of plastic flow and the powder is susceptible to compaction and applying external pressure to the entire exterior surface of said container to apply a hydrostatic pressure to the powder in said cavity to densify said powder into a compact, and (e) cooling said container and compact and removing said container from said compact.
Claim 2
Independent Claim 207 words
A method for hot consolidating powder of metallic and non-metallic composition and combinations thereof to form a densified .Iadd.and irregularly shaped .Iaddend.compact, said method comprising the steps of: (a) providing a container by forming a cavity having the general .Iadd.irregular .Iaddend.shape of the compact to be produced in a mass of container material which is substantially fully dense and incompressible and is capable of plastic flow at elevated temperatures, the volume of said mass being sufficiently large with respect to the volume of said cavity to form walls entirely surrounding said cavity of sufficient thickness so that the exterior surface of the walls .Iadd.are regularly shaped and .Iaddend.do not closely follow the contour of said cavity, (b) filling said cavity with a powder to be compacted, (c) hermetically sealing said container, (d) .Iadd.applying conventional compaction temperatures and pressures by .Iaddend.heating said container and powder to a temperature at which said mass is capable of plastic flow and the powder is susceptible to compaction and applying external pressure to the entire exterior surface of said container to apply a hydrostatic pressure to the powder in said cavity to densify said powder into a compact, and (e) cooling said container and compact and removing said container from said compact.
Claim 3
Independent Claim 147 words
A method for hot consolidating powder of metallic and non-metallic composition and combinations thereof to form a densified powder compact comprising the steps of (a) encapsulating a quantity of powder .Iadd.in an irregularly shaped cavity .Iaddend.in a thick-walled metal container wherein the walls of the container .Iadd.are regularly shaped and .Iaddend.entirely surround the powder and are substantially fully dense and incompressible and are capable of plastic flow at predetermined temperatures and pressures, (b) heating the container and powder to a .Iadd.conventional compaction .Iaddend.temperature at which the powder will densify and (c) applying .Iadd.a conventional compaction .Iaddend.pressure to the entire exterior surface of the heated container by pressing the container between the dies of a press while restraining the container the applied pressure being of sufficient magnitude to cause plastic flow at the container walls thereby subjecting the powder to a hydrostatic pressure which causes it to densify.
Claim 4
Independent Claim 147 words
A method for hot consolidating powder of metallic and non-metallic composition and combinations thereof to form a densified powder compact comprising the steps of (a) encapsulating a quantity of powder .Iadd.in an irregularly shaped cavity .Iaddend.in a thick-walled metal container wherein the walls of the container .Iadd.are regularly shaped and .Iaddend.entirely surround the powder and are substantially fully dense and incompressible and are capable of plastic flow at predetermined temperatures and pressures, (b) heating the container and powder to a .Iadd.conventional compaction .Iaddend.temperature at which the powder will densify and (c) applying .Iadd.a conventional compaction .Iaddend.pressure to the entire exterior surface of the heated container by pressing the container between the dies of a press while restraining the container the applied pressure being of sufficient magnitude to cause plastic flow at the container walls thereby subjecting the powder to a hydrostatic pressure which causes it to densify.
Claim 5
Dependent Claim 35 words
The method set forth in claim 2 including the step of permitting controlled escape of container metal from between the press dies when the pressure exceeds a desired maximum to prevent damage to the press.
Claim 6
Independent Claim 134 words
A method for hot consolidating powder to form .[.a.]. .Iadd.an irregularly shaped and .Iaddend.densified powder compact comprising the steps of (a) encapsulating a quantity of powder in a thick-walled low carbon steel container wherein the walls of the container .Iadd.are regularly shaped and .Iaddend.entirely surround the powder and are substantially fully dense and incompressible and are capable of plastic flow at temperatures above 1,000° F. and a pressure exceeding 5,000 psi, (b) preheating the container and powder to a temperature above 1,000° F. and (c) applying a pressure above 5,000 psi to the entire exterior surface of the container by pressing the container between the dies of a press while restraining the container thereby causing plastic flow of the container walls to subject the powder to a hydrostatic pressure which causes it to densify.
Claim 7
Independent Claim 134 words
A method for hot consolidating powder to form .[.a.]. .Iadd.an irregularly shaped and .Iaddend.densified powder compact comprising the steps of (a) encapsulating a quantity of powder in a thick-walled low carbon steel container wherein the walls of the container .Iadd.are regularly shaped and .Iaddend.entirely surround the powder and are substantially fully dense and incompressible and are capable of plastic flow at temperatures above 1,000° F. and a pressure exceeding 5,000 psi, (b) preheating the container and powder to a temperature above 1,000° F. and (c) applying a pressure above 5,000 psi to the entire exterior surface of the container by pressing the container between the dies of a press while restraining the container thereby causing plastic flow of the container walls to subject the powder to a hydrostatic pressure which causes it to densify.
Claim 8
Dependent Claim 35 words
The method set forth in claim 4 including the step of permitting controlled escape of container metal from between the press dies when the pressure exceeds a desired maximum to prevent damage to the press.
Claim 9
Dependent Claim 34 words
The method as set forth in claim 1 wherein the step of applying external pressure to the entire exterior surface of said container is further defined as applying gas pressure in a gas autoclave.
Claim 10
Dependent Claim 487 words
The method as set forth in claim 1 wherein the step of applying external pressure to the entire external surface of said container is further defined as pressing the container between the dies of a press while restraining the container to cause plastic flow of the container walls. .Iadd. 8. A method for hot consolidating material of metallic and nonmetallic composition and combination thereof to form a fully densified compact comprising the steps of: encapsulating a quantity of less than fully dense material in a cavity of irregular shape in a thick-walled container having a regular shape and walls entirely surrounding the cavity and of sufficient thickness so as not to follow the contour of the cavity and of a material which is substantially fully dense and incompressible and capable of plastic flow at elevated temperatures, heating the container and material to a conventional compaction temperature at which the container is capable of plastic flow and the material is susceptible to compaction and will densify and applying conventional pressure to the entire exterior surface of the container thereby causing plastic flow of the container walls to transmit pressure to the material to cause full densification at hydrostatic pressre applied by the container. .Iaddend. .Iadd. 9. A method as set forth in claim 8 further defined as encapsulating the material in the cavity by hermetically sealing the container. .Iaddend..Iadd. 10. A method as set forth in claim 8 further defined as forming the container of a gross volume of wall material which is greater than the volume of the cavity surrounded by the container wall material. .Iaddend..Iadd. 11. A method as set forth in claim 8 further defined as forming the container of a gross volume of wall material which is greater than the volume of the cavity surrounded by the wall material and decreasing the volume of the cavity during densification of the compact as the volume of the wall material remains constant. .Iaddend..Iadd. 12. A method as set forth in claim 8 further defined as removing the container from the compact. .Iaddend..Iadd. 13. A method as set forth in claim 8 including cooling the container and compact and removing the container from the compact. .Iaddend. .Iadd. 14. A method as set forth in claim 8 further defined as forming the container by mating at least two metal container sections together by welding. .Iaddend..Iadd. 15. A method as set forth in claim 8 wherein the step of applying external pressure to the entire exterior surface of the container is further defined as applying gas pressure in an autoclave. .Iaddend. .Iadd. 16. A method as set forth in claim 8 wherein the step of applying external pressure to the entire exterior surface of the container is further defined as applying force to a portion of the container while restraining the remainder of the container to cause the hydrostatic pressure and plastic flow of the container for densification. .Iaddend.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-08-22 1987-02-21 1987-08-23 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-08-22 1991-02-21 1991-08-23 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-08-22 1995-02-21 1995-08-23 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag