US5849355A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Electroless copper plating
Assignee: Honeywell International Inc
•
Filing: 1996-09-18
•
Granted: 1998-12-15
•
Expires: 2016-09-18
Abstract
Abstract An optimized electroless copper plating technique suitable for plating electroless copper upon ceramics.
Inventors
- 👤 Michael R. McHenry
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 16:42
CPC Classifications
H; H05; H05K; H05K1/00; H05K1/16; H01; H01F; H01F41/00; H01F41/02; H01F41/04; H01F41/041; H01F41/042; H03; H03H; H03H3/00; Y; Y10; Y10T; Y10T29/00; Y10T29/49; Y10T29/49002; Y10T29/4902
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
89 words
A process for electroless copper coating on a substrate, comprising the steps of: cleaning the substrate alkaline cleaning and conditioning for a dwell time of about 4.5 to 5.5 minutes; rinsing with Reverse Osmosis water; preconditioning said substrate in a stannous chloride solution from about 0.75 to about 1.5 minutes; treating with a tin-palladium colloid; postactivating with a solution to remove tin from the tin-palladium colloid from about 2.75 to about 3.25 minutes; and applying electroless copper in solution, which solution has been used less than about one week.
Claim 2
Dependent Claim
89 words
A process for electroless copper coating on a substrate, comprising the steps of: cleaning the substrate alkaline cleaning and conditioning for a dwell time of about 4.5 to 5.5 minutes; rinsing with Reverse Osmosis water; preconditioning said substrate in a stannous chloride solution from about 0.75 to about 1.5 minutes; treating with a tin-palladium colloid; postactivating with a solution to remove tin from the tin-palladium colloid from about 2.75 to about 3.25 minutes; and applying electroless copper in solution, which solution has been used less than about one week.
Claim 3
Dependent Claim
42 words
The process as claimed in claim 1 comprising the additional step of: microetching from about 55 to about 65 seconds subsequent to the step of rinsing with reverse osmosis water and prior to the step of preconditioning in a stannous chloride solution.
Claim 4
Dependent Claim
185 words
A process for optimizing an electroless copper coating process so as to maximize overall adhesion and coverage of the electroless copper onto a substrate, wherein the electroless copper coating process comprises the steps of: initial abrasive cleaning the substrate, alcohol rinsing the substrate, immersing the substrate in an alkaline cleaning and conditioning solution, rinsing the substrate with reverse osmosis water, immersing the substrate in a preconditioning solution of stannous chloride, treating the substrate with a tin-palladium colloid, immersing the substrate in a postactivating solution to remove tin from the tin-palladium colloid, and applying electroless copper in solution; the optimizing process comprising the steps of: adjusting the time in which the substrate is in the alkaline cleaning and conditioning solution so as to maximize adhesion and coverage of the resulting electroless copper on a substrate; adjusting the time in which the substrate is in the postactivating solution so as to maximize adhesion and coverage of the resulting electroless copper on a substrate; and adjusting the age of the electroless copper bath so as to maximize adhesion and coverage of the resulting electroless copper on a substrate.
Claim 5
Dependent Claim
185 words
A process for optimizing an electroless copper coating process so as to maximize overall adhesion and coverage of the electroless copper onto a substrate, wherein the electroless copper coating process comprises the steps of: initial abrasive cleaning the substrate, alcohol rinsing the substrate, immersing the substrate in an alkaline cleaning and conditioning solution, rinsing the substrate with reverse osmosis water, immersing the substrate in a preconditioning solution of stannous chloride, treating the substrate with a tin-palladium colloid, immersing the substrate in a postactivating solution to remove tin from the tin-palladium colloid, and applying electroless copper in solution; the optimizing process comprising the steps of: adjusting the time in which the substrate is in the alkaline cleaning and conditioning solution so as to maximize adhesion and coverage of the resulting electroless copper on a substrate; adjusting the time in which the substrate is in the postactivating solution so as to maximize adhesion and coverage of the resulting electroless copper on a substrate; and adjusting the age of the electroless copper bath so as to maximize adhesion and coverage of the resulting electroless copper on a substrate.
References Cited (Backward Citations)
US3833872A
Cited
US3765082A
Cited
US4310821A
Cited
US4313152A
Cited
US4641114A
Cited
US4543553A
Cited
US4613843A
Cited
US4730095A
Cited
EP0209816A1
Cited
US4626816A
Cited
US4959631A
Cited
US4914260A
Cited
US4918418A
Cited
US4926292A
Cited
EP0433176A2
Cited
US5225969A
Cited
US5358907A
Cited
US4999597A
Cited
US5298687A
Cited
US5363080A
Cited
US5398400A
Cited
US5532667A
Cited
US5380451A
Cited
US5416356A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 2001-12-14 | 2002-06-15 | 2002-12-15 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2005-12-14 | 2006-06-15 | 2006-12-15 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2009-12-14 | 2010-06-15 | 2010-12-15 | $7700.00 | Window Closed / Lapsed |