US5620524A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Apparatus for fluid delivery in chemical vapor deposition systems
Assignee: IPPRIME Inc
•
Filing: 1995-02-27
•
Granted: 1997-04-15
•
Expires: 2015-02-27
Abstract
Abstract Described herein is an apparatus and method for delivering fluid components for semiconductor processes such as chemical vapor deposition (CVD) and chemical etch processes. Any prescribed mixture of separate fluid reagents can be delivered with extreme accuracy and precision using the apparatus we describe here. The unique embodiment of a precision fluid pumping system utilizing internal pressure and temperature transducers, capacity volume and restrictive elements that comprise a continuous pulse-free system for use in CVD applications. This system has superior performance characteristics in the areas of: accuracy, precision, repeatability of the fluid mixture delivery and continuous repeatable delivery without intermittent pulsation. We describe a novel fluid pump whose design is integrated using a closed loop feedback system composed of temperature and pressure sensors. This allows the entire system to perform to in either an isobaric-isothermal mode or an isocratic-isothermal mode. The construction of this system is separated into three principle areas (Fluid Pump Hardware), (Fluid phase change hardware) and (Control algorithms), the complete embodiment constitutes a novel invention in the field of chemical delivery as pertaining to the fabrication of semiconductor devices.
Inventors
- 👤 Chiko Fan
- 👤 Anthony Pearson
- 👤 J. James Chen
- 👤 James L. White, Jr.
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 16:05
CPC Classifications
B; B01; B01J; B01J4/00; C; C23; C23C; C23C16/00; C23C16/44; C23C16/448; C23C16/4481
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
309 words
A step gradient positive displacement dual plunger system for continuous and pulse-free delivery of reagents for semiconductor processing, said system comprising: a plurality of reagent sources; a buffer gas source; a primary liquid delivery chamber and a secondary liquid delivery chamber; wherein said primary and secondary liquid chamber are comprised of a high pressure chamber with an inlet and an outlet, a plunger connected to a motor assembly, fluoropolymer high pressure seals, and a washing chamber; said motor assembly comprising a ball screw spindle, a counter rotating shaft and bearing, a direct or gear drive motor with an attached optical encoder that provides closed loop motion control; said plurality of reagent sources and said buffer gas source are connected by solenoid valves to a manifold, said manifold is connected to the inlet of said primary liquid delivery chamber via a solenoid valve; a pressure transducer is connected to the outlet of said primary liquid delivery chamber via a check valve, and the inlet of said secondary liquid delivery chamber; a device to minimize the pressure pulsation associated with the plunger operation; wherein said device comprise a capillary tube before and in series with a volume element, said volume element is connected in series to another capillary tube, and a heating or cooling means for heating or cooling the reagents in the volume elements; a heating gas mixing block comprising a reagent inlet, a buffer gas inlet, a heating means for heating the heating gas mixing block, and an outlet to a reaction chamber; wherein said reagent is flashed vaporized and mixed with a buffer gas; and the outlet of said secondary liquid delivery chamber is connected before and in series with said device via said capillary tubing, said device is connected before and in series with the reagent inlet of said heating gas mixing block via said capillary tubing.
Claim 2
Dependent Claim
309 words
A step gradient positive displacement dual plunger system for continuous and pulse-free delivery of reagents for semiconductor processing, said system comprising: a plurality of reagent sources; a buffer gas source; a primary liquid delivery chamber and a secondary liquid delivery chamber; wherein said primary and secondary liquid chamber are comprised of a high pressure chamber with an inlet and an outlet, a plunger connected to a motor assembly, fluoropolymer high pressure seals, and a washing chamber; said motor assembly comprising a ball screw spindle, a counter rotating shaft and bearing, a direct or gear drive motor with an attached optical encoder that provides closed loop motion control; said plurality of reagent sources and said buffer gas source are connected by solenoid valves to a manifold, said manifold is connected to the inlet of said primary liquid delivery chamber via a solenoid valve; a pressure transducer is connected to the outlet of said primary liquid delivery chamber via a check valve, and the inlet of said secondary liquid delivery chamber; a device to minimize the pressure pulsation associated with the plunger operation; wherein said device comprise a capillary tube before and in series with a volume element, said volume element is connected in series to another capillary tube, and a heating or cooling means for heating or cooling the reagents in the volume elements; a heating gas mixing block comprising a reagent inlet, a buffer gas inlet, a heating means for heating the heating gas mixing block, and an outlet to a reaction chamber; wherein said reagent is flashed vaporized and mixed with a buffer gas; and the outlet of said secondary liquid delivery chamber is connected before and in series with said device via said capillary tubing, said device is connected before and in series with the reagent inlet of said heating gas mixing block via said capillary tubing.
Claim 3
Dependent Claim
20 words
The system as claimed in claim 1, wherein said capillary tubing is manufactured of a material compatible to said reagent.
Claim 4
Dependent Claim
22 words
The system as claimed in claim 2, wherein said capillary tubing is formed of fused silica, stainless steel, polymer or titanium tubing.
Claim 5
Dependent Claim
20 words
The system as claimed in claim 1, wherein said volume element is manufactured of a material compatible to said reagent.
Claim 6
Dependent Claim
20 words
The system as claimed in claim 4, wherein said volume element is formed of stainless steel, polymer or titanium tubing.
Claim 7
Dependent Claim
330 words
A continuous gradient positive displacement dual plunger system for continuous and pulse-free delivery of reagents for semiconductor processing, said system comprising; a plurality of reagent supply means for supplying a liquid reagent to a heating gas mixing block; wherein said reagent supply means comprises: a reagent source; a buffer gas source; a primary liquid delivery chamber and secondary liquid delivery chambers; wherein said primary and secondary liquid delivery chambers are comprised of a high pressure chamber with an inlet and an outlet, a plunger connected to a motor assembly, fluoropolymer high pressure seals, and a washing chamber; said motor assembly comprising a ball screw spindle, a counter rotating shaft and bearing, a direct or gear drive motor with an attached optical encoder that provides closed loop motion control; said reagent source and said buffer gas source are connected by solenoid valves to a manifold, said manifold is connected to the inlet of said primary liquid delivery chamber via a solenoid valve; a pressure transducer is connected to the outlet of said primary liquid delivery chamber via a check valve, and the inlet of said secondary liquid delivery chamber; a device to minimize the pressure pulsation associated with the plunger operation; wherein said device comprises a capillary tube before and in series with a volume element, said volume element is connected in series to another capillary tube, and a heating or cooling means for heating or cooling the reagents in the volume element; the outlet of said secondary liquid delivery chamber is connected before and in series with said device via said capillary tubing, said device is connected before and in series with the reagent inlet of said heating gas mixing block via said capillary tubing; and a heating gas mixing block comprising a plurality of reagent inlets, a buffer gas inlet, a heating means for heating the heating gas mixing block, and an outlet to a reaction chamber; wherein said reagents are flashed vaporized and mixed with a buffer gas.
Claim 8
Dependent Claim
330 words
A continuous gradient positive displacement dual plunger system for continuous and pulse-free delivery of reagents for semiconductor processing, said system comprising; a plurality of reagent supply means for supplying a liquid reagent to a heating gas mixing block; wherein said reagent supply means comprises: a reagent source; a buffer gas source; a primary liquid delivery chamber and secondary liquid delivery chambers; wherein said primary and secondary liquid delivery chambers are comprised of a high pressure chamber with an inlet and an outlet, a plunger connected to a motor assembly, fluoropolymer high pressure seals, and a washing chamber; said motor assembly comprising a ball screw spindle, a counter rotating shaft and bearing, a direct or gear drive motor with an attached optical encoder that provides closed loop motion control; said reagent source and said buffer gas source are connected by solenoid valves to a manifold, said manifold is connected to the inlet of said primary liquid delivery chamber via a solenoid valve; a pressure transducer is connected to the outlet of said primary liquid delivery chamber via a check valve, and the inlet of said secondary liquid delivery chamber; a device to minimize the pressure pulsation associated with the plunger operation; wherein said device comprises a capillary tube before and in series with a volume element, said volume element is connected in series to another capillary tube, and a heating or cooling means for heating or cooling the reagents in the volume element; the outlet of said secondary liquid delivery chamber is connected before and in series with said device via said capillary tubing, said device is connected before and in series with the reagent inlet of said heating gas mixing block via said capillary tubing; and a heating gas mixing block comprising a plurality of reagent inlets, a buffer gas inlet, a heating means for heating the heating gas mixing block, and an outlet to a reaction chamber; wherein said reagents are flashed vaporized and mixed with a buffer gas.
References Cited (Backward Citations)
US3223040A
Cited
US3818805A
Cited
US3818807A
Cited
US3869963A
Cited
US3943717A
Cited
US3985021A
Cited
US3985019A
Cited
US4045343A
Cited
US4234427A
Cited
US4321014A
Cited
US4352636A
Cited
US4556367A
Cited
US4600365A
Cited
US4808092A
Cited
US4714545A
Cited
US4911405A
Cited
US4947889A
Cited
US5201851A
Cited
US5160542A
Cited
US5129418A
Cited
US5098741A
Cited
US5204314A
Cited
US5078922A
Cited
US5440887A
Cited
US5259731A
Cited
US5243821A
Cited
US5253981A
Cited
US5534069A
Cited
US5470390A
Cited
US5450743A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 2000-04-14 | 2000-10-14 | 2001-04-15 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2004-04-14 | 2004-10-14 | 2005-04-15 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2008-04-14 | 2008-10-14 | 2009-04-15 | $7700.00 | Window Closed / Lapsed |