US5482697A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method of making V6 O13+x [0<X≦2.0]
Assignee: Valence Technology Inc
•
Filing: 1994-01-19
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Granted: 1996-01-09
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Expires: 2014-01-19
Abstract
Abstract A method of making non-stoichiometric vanadium oxides V6O13+X by treatment with H2O2.
Inventors
- 👤 M. Yazid Saidi
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 17:00
CPC Classifications
H; H01; H01M; H01M4/00; H01M4/02; H01M4/36; H01M4/48; H01M4/485; C; C01; C01G; C01G31/00; C01G31/02; C01P; C01P2002/00; C01P2002/70; C01P2002/72; C01P2004/00; C01P2004/01; C01P2004/03; H01M4/13; H01M4/131; H01M4/64; H01M4/66; H01M4/661; Y; Y02; Y02E; Y02E60/00; Y02E60/10
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
54 words
A method of making V 6 O 13+x wherein 0<x<2.0 comprising the steps of: in a stirred aqueous medium contained in a reaction vessel, slowly contacting V 6 O 13 with at least a nominal stoichiometric amount of hydrogen peroxide to form the product V 6 O 13+x wherein 0<x<2.0; and drying said product.
Claim 2
Independent Claim
54 words
A method of making V 6 O 13+x wherein 0<x<2.0 comprising the steps of: in a stirred aqueous medium contained in a reaction vessel, slowly contacting V 6 O 13 with at least a nominal stoichiometric amount of hydrogen peroxide to form the product V 6 O 13+x wherein 0<x<2.0; and drying said product.
Claim 3
Dependent Claim
37 words
The method of claim 1 wherein an aqueous solution of H 2 O 2 is added slowly to said stirred aqueous medium containing V 6 O 13 over a period of about 4 to about 12 hours.
Claim 4
Dependent Claim
20 words
The method of claim 2 further comprising the step of applying a stream of oxygen to said stirred aqueous medium.
Claim 5
Dependent Claim
15 words
The method of claim 3 wherein the product produced is V 6 O 13 .8.
Claim 6
Dependent Claim
15 words
The method of claim 3 wherein the product produced is V 6 O 14 .2.
Claim 7
Dependent Claim
17 words
The method of claim 1 wherein a stream of oxygen is added to said stirred aqueous medium.
Claim 8
Dependent Claim
21 words
The method of claim 1 wherein said reaction vessel is maintained at temperature of about 0° C. to about 45° C.
Claim 9
Dependent Claim
17 words
The method of claim 1 wherein said reaction vessel is sealed to maintain a constant volume reaction.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1999-01-08 | 1999-07-10 | 2000-01-09 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2003-01-08 | 2003-07-10 | 2004-01-09 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2007-01-08 | 2007-07-10 | 2008-01-09 | $7700.00 | Window Closed / Lapsed |