Patent US5333994A successfully refreshed from Google Patents.
← Back to Patent Explorer
US5333994A Expired / Lapsed US ⏱️ 0.0 years remaining

High temperature NMR sample spinner

Assignee: Doty Scientific Inc
•
Filing: 1992-09-22
•
Granted: 1994-08-02
•
Expires: 2012-09-22
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A high-strength, thin-wall ceramic cylinder partially closed at one end, with radial-inflow turbine blades ground into the partially closed end thereof, provides the rotational drive, surface protection, and burst strength necessary to contain and spin a low strength, disposable soft ceramic capsule, loaded with a sample for NMR experiments, at high rotational speeds inside an NMR receiver/transmitter coil. An improved radial inflow turbine design results in higher efficiency for micro-turbines. A cylindrical air journal bearing at both ends provides radial stability and support. An axial thrust air bearing is formed at the end opposite the turbine blades between the sacrificial bottom of the soft capsule and a thrust ring. The high-strength ceramic is typically of a partially stabilized zirconia or hot pressed silicon nitride. The disposable capsule is typically of hexagonal boron nitride.

Inventors

  • 👤 F. David Doty
  • 👤 Jonathan B. Spitzmesser
  • 👤 David G. Wilson

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 12:27
CPC Classifications
G; G01; G01R; G01R33/00; G01R33/20; G01R33/28; G01R33/30; G01R33/307

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 43 words
A ceramic thin-walled cylindrical rotor shell for NMR having radial inflow turbine blades ground into a partially closed drive end wherein said rotor shell comprises a high strength ceramic chosen from the set consisting of partially stabilized zirconia and hot pressed silicon nitride.
Claim 2
Dependent Claim 43 words
A ceramic thin-walled cylindrical rotor shell for NMR having radial inflow turbine blades ground into a partially closed drive end wherein said rotor shell comprises a high strength ceramic chosen from the set consisting of partially stabilized zirconia and hot pressed silicon nitride.
Claim 3
Dependent Claim 26 words
A ceramic thin-walled cylindrical rotor shell having radial inflow turbine blades ground into a partially closed drive end wherein said rotor shell comprises partially stabilized zirconia.
Claim 4
Dependent Claim 26 words
A ceramic thin-walled cylindrical rotor shell having radial inflow turbine blades ground into a partially closed drive end wherein said rotor shell comprises partially stabilized zirconia.
Claim 5
Dependent Claim 29 words
A ceramic thin-walled cylindrical rotor shell for NMR having radial inflow turbine blades ground into a partially closed drive end wherein said rotor shell comprises hot pressed silicon nitride.
Claim 6
Dependent Claim 29 words
A ceramic thin-walled cylindrical rotor shell for NMR having radial inflow turbine blades ground into a partially closed drive end wherein said rotor shell comprises hot pressed silicon nitride.
Claim 7
Dependent Claim 27 words
A ceramic thin-walled cylindrical rotor shell for NMR having radial inflow turbine blades ground into a partially closed drive end wherein said rotor shell comprises silicon nitride.
Claim 8
Dependent Claim 27 words
A ceramic thin-walled cylindrical rotor shell for NMR having radial inflow turbine blades ground into a partially closed drive end wherein said rotor shell comprises silicon nitride.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1997-08-01 1998-01-31 1998-08-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2001-08-01 2002-01-31 2002-08-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2005-08-01 2006-01-31 2006-08-02 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag