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US5200029A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of making a planar optical amplifier

Assignee: Nokia Bell Labs
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Filing: 1991-12-04
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Granted: 1993-04-06
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Expires: 2011-12-04
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Abstract

Abstract An active optical device comprises a glass, waveguiding structure disposed on a substantially planar principal surface of a substrate. The structure includes a silica-based, erbium-doped active core. The active core has an erbium-to-silicon atomic ratio of at least about 0.01, an absolute erbium concentration of at least about 1.4×10 20 atoms per cubic centimeter, and a radiative lifetime of the erbium lasing level of at least about 7 milliseconds. Also disclosed is a method for forming an active optical device, including the step of depositing an erbium-doped active core by sputtering.

Inventors

  • 👤 Allan J. Bruce
  • 👤 Joseph Shmulovich
  • 👤 Amy Wong
  • 👤 Yiu-Huen Wong

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 09:17
CPC Classifications
H; H01; H01S; H01S3/00; H01S3/05; H01S3/06; H01S3/063; H01S3/14; H01S3/16; H01S3/1601; H01S3/1603; H01S3/1608

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 232 words
A method for forming an optical device on a substrate having a substantially planar principal surface, comprising: a) forming a first layer of vitreous silicon dioxide on the principal surface; b) depositing a second layer of silica-based glass over the first layer by sputtering a target of silica-based glass such that the second layer has a higher refractive index than the first layer; c) annealing the second layer such that it is stabilized; d) removing a portion of the second layer by etching, such that an elongate core, extending along the longitudinal axis, is formed, the core being adapted, after completion of the device, to guide electromagnetic radiation of at least a signal wavelength and a pump wavelength; and e) depositing a third layer of phosphosilicate glass over the core such that the third layer has a smaller refractive index than the core; characterized in that f) the target further comprises sodium and erbium; and g) the target composition is selected such that the core has an erbium-to-silicon atomic ratio of at least about 0.01, a sodium-to-silicon atomic ratio in the approximate range 0.2-0.6, and an absolute erbium concentration of at least about 1.4×10 20 atoms per cubic centimeter, and the target composition is further selected such that a lasing level is associated with the erbium in the core, the lasing level having a radiative lifetime of at least about 7 ms.
Claim 2
Independent Claim 232 words
A method for forming an optical device on a substrate having a substantially planar principal surface, comprising: a) forming a first layer of vitreous silicon dioxide on the principal surface; b) depositing a second layer of silica-based glass over the first layer by sputtering a target of silica-based glass such that the second layer has a higher refractive index than the first layer; c) annealing the second layer such that it is stabilized; d) removing a portion of the second layer by etching, such that an elongate core, extending along the longitudinal axis, is formed, the core being adapted, after completion of the device, to guide electromagnetic radiation of at least a signal wavelength and a pump wavelength; and e) depositing a third layer of phosphosilicate glass over the core such that the third layer has a smaller refractive index than the core; characterized in that f) the target further comprises sodium and erbium; and g) the target composition is selected such that the core has an erbium-to-silicon atomic ratio of at least about 0.01, a sodium-to-silicon atomic ratio in the approximate range 0.2-0.6, and an absolute erbium concentration of at least about 1.4×10 20 atoms per cubic centimeter, and the target composition is further selected such that a lasing level is associated with the erbium in the core, the lasing level having a radiative lifetime of at least about 7 ms.
Claim 3
Dependent Claim 23 words
The method of claim 1, further comprising, after (d) and before (e), the step of forming a protective dielectric film over the core.
Claim 4
Dependent Claim 28 words
The method of claim 1, further comprising, after (d), the step of annealing the core such that roughness due to etching of the second layer is substantially removed.
Claim 5
Dependent Claim 37 words
The method of claim 1, further comprising, after (d), the step of annealing the core at a temperature of at least about 700° C. for a duration of at least about 1 hour in a reactive atmosphere.
Claim 6
Dependent Claim 13 words
The method of claim 4, wherein the reactive atmosphere comprises very dry oxtgen.
Claim 7
Independent Claim 367 words
A method for forming an optical device on a substrate having a substantially planar principal surface, comprising: a) forming a first layer of silicon dioxide on the principal surface; b) depositing a second layer of phosphosilicate glass over the first layer such that the second layer has a higher refractive index than the first layer, c) annealing the second layer such that it is at least partially densified; d) removing a portion of the second layer by etching, such that an elongate lower core having a longitudinal axis is formed, the lower core being adapted, after completion of the device, to guide electromagnetic radiation of at least a signal wavelength and a pump wavelength; e) annealing the lower core such that roughness due to etching of the second layer is substantially removed; f) depositing a third layer of silica-based glass over the lower core by sputtering a target of silica-based glass such that the third layer has a higher refractive index than the lower core; g) annealing the third layer such that it is stabilized; h) removing a portion of the third layer by etching, such that an elongate upper core, extending along the longitudinal axis, is formed, the upper core being adapted, after completion of the device, to guide electromagnetic radiation of the signal and pump wavelengths; i) annealing the upper core at a temperature of at least about 700° C. for a duration of at least about 1 hour in a reactive atmosphere; and j) depositing a fourth layer of phosphosilicate glass over the upper and lower cores such that the fourth layer has a smaller refractive index than the upper and lower cores; characterized in that k) the target further comprises sodium and erbium; and l) the target composition is selected such that the third layer has an erbium-to-silicon atomic ratio of at least about 0.01, a sodium-to-silicon atomic ratio in the approximate range 0.2-0.6, and an absolute erbium concentration of at least about 1.4×10 20 atoms per cubic centimeter, and the target composition is further selected such that a lasing level is associated with the erbium in the third layer, the lasing level having a radiative lifetime of at least about 7 ms.
Claim 8
Independent Claim 367 words
A method for forming an optical device on a substrate having a substantially planar principal surface, comprising: a) forming a first layer of silicon dioxide on the principal surface; b) depositing a second layer of phosphosilicate glass over the first layer such that the second layer has a higher refractive index than the first layer, c) annealing the second layer such that it is at least partially densified; d) removing a portion of the second layer by etching, such that an elongate lower core having a longitudinal axis is formed, the lower core being adapted, after completion of the device, to guide electromagnetic radiation of at least a signal wavelength and a pump wavelength; e) annealing the lower core such that roughness due to etching of the second layer is substantially removed; f) depositing a third layer of silica-based glass over the lower core by sputtering a target of silica-based glass such that the third layer has a higher refractive index than the lower core; g) annealing the third layer such that it is stabilized; h) removing a portion of the third layer by etching, such that an elongate upper core, extending along the longitudinal axis, is formed, the upper core being adapted, after completion of the device, to guide electromagnetic radiation of the signal and pump wavelengths; i) annealing the upper core at a temperature of at least about 700° C. for a duration of at least about 1 hour in a reactive atmosphere; and j) depositing a fourth layer of phosphosilicate glass over the upper and lower cores such that the fourth layer has a smaller refractive index than the upper and lower cores; characterized in that k) the target further comprises sodium and erbium; and l) the target composition is selected such that the third layer has an erbium-to-silicon atomic ratio of at least about 0.01, a sodium-to-silicon atomic ratio in the approximate range 0.2-0.6, and an absolute erbium concentration of at least about 1.4×10 20 atoms per cubic centimeter, and the target composition is further selected such that a lasing level is associated with the erbium in the third layer, the lasing level having a radiative lifetime of at least about 7 ms.
Claim 9
Dependent Claim 24 words
The method of claim 6, further comprising, after (i) and before (j), the step of forming a protective dielectric film over the active core.
Claim 10
Dependent Claim 13 words
The method of claim 6, wherein the reactive atmosphere comprises very dry oxygen.
Claim 11
Dependent Claim 29 words
The method of claim 6, further comprising, after (h), the step of annealing the upper core such that roughness due to etching of the third layer is substantially removed.

References Cited (Backward Citations)

US4586785A Cited
US4425146A Cited
US4826288A Cited
US4931077A Cited
US4962995A Cited
US5005175A Cited
US5027079A Cited
US5125946A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1996-04-05 1996-10-05 1997-04-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2000-04-05 2000-10-05 2001-04-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2004-04-05 2004-10-05 2005-04-06 $7700.00 Window Closed / Lapsed

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