US5144134A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method for determining the quality of a lubricant layer on a magnetic recording medium by detecting electrons at varying drawing angles
Assignee: Fuji Electric Co Ltd
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Filing: 1991-06-05
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Granted: 1992-09-01
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Expires: 2011-06-05
Abstract
Abstract The quality of a lubricant layer formed on a surface of a magnetic recording medium is determined by exposing the lubricant molecules of the lubricant layer to a radiation source for x-ray photoelectron spectroscopy while varying the photoelectron drawing angle. The number of emitted electrons is determined and, from this, the degree of orientation and the quality of the lubricant layer is found.
Inventors
- 👤 Katsumi Onodera
- 👤 Youichi Tei
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 05:20
CPC Classifications
G; G01; G01N; G01N23/00; G01N23/22; G01N23/227; G01N23/2273; G11; G11B; G11B5/00; G11B5/62; G11B5/72; G11B5/725; G11B5/7253; G11B5/7257
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
135 words
A method for determining the quality of a lubricant layer, formed from lubricant molecules having main chain and polar group portions, on a surface of a magnetic recording medium having a protective layer which comprises: (a) exposing the lubricant layer to a radiation source for X-ray photoelectron spectroscopy while varying the photoelectron drawing angle; (b) determining the numbers of emitted electrons at varying drawing angles corresponding to the main chain and polar group portions and the drawing angle which the number of emitted electrons corresponding to the main chain portions is at its maximum; and (c) assessing the degree of orientation of the polar group portion towards the protective layer from the information collected in step (b), wherein a high degree of orientation towards the protective layer is indicative of a high quality lubricant layer.
Claim 2
Independent Claim
135 words
A method for determining the quality of a lubricant layer, formed from lubricant molecules having main chain and polar group portions, on a surface of a magnetic recording medium having a protective layer which comprises: (a) exposing the lubricant layer to a radiation source for X-ray photoelectron spectroscopy while varying the photoelectron drawing angle; (b) determining the numbers of emitted electrons at varying drawing angles corresponding to the main chain and polar group portions and the drawing angle which the number of emitted electrons corresponding to the main chain portions is at its maximum; and (c) assessing the degree of orientation of the polar group portion towards the protective layer from the information collected in step (b), wherein a high degree of orientation towards the protective layer is indicative of a high quality lubricant layer.
Claim 3
Dependent Claim
23 words
A method according to claim 1, wherein the lubricant layer is formed on a magnetic layer which is formed on a nonmagnetic substrate.
Claim 4
Dependent Claim
25 words
A method according to claim 2, wherein the magnetic recording medium comprises a carbon protective layer disposed between the magnetic layer and the lubricant layer.
Claim 5
Dependent Claim
95 words
A method according to claim 3, wherein the number of electrons emitted corresponding to the polar group portion at a 16 degree drawing angle and at a 90 degree drawing angle are compared to the entire peak intensity of the group and wherein, a 16 degree peak intensity which is less than 12%, and a 90 degree peak intensity which is less are indicative of a high quality lubricant layer in which the polar groups of the lubricant molecules are oriented to the side of the lubricant layer in contact with the carbon protective layer.
Claim 6
Dependent Claim
82 words
A method according to claim 4, wherein the number of electrons emitted corresponding to the main chain portion at a 16 degree drawing angle is compared to the entire peak intensity of the group and wherein, a 16 degree peak intensity which is less than 14% of the entire peak intensity of the group is indicative of a high quality lubricant layer in which the main chain portions of the lubricant molecules are oriented to the surface side of the lubricant layer.
Claim 7
Dependent Claim
65 words
A method according to claim 5, wherein a determination that the drawing angle at which the number of electrons emitted from the main chain portion of the lubricant molecule is at a maximum at about 10 degrees is indicative of a high quality lubricant layer in which the main chain portions of the lubricant molecules are oriented to the surface side of the lubricant layer.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1995-09-01 | 1996-03-02 | 1996-09-01 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1999-09-01 | 2000-03-02 | 2000-09-01 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2003-09-01 | 2004-03-02 | 2004-09-01 | $7700.00 | Window Closed / Lapsed |