Patent US5094619A successfully refreshed from Google Patents.
US5094619A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Coloration of dental restorations
Assignee: Individual
•
Filing: 1989-11-27
•
Granted: 1992-03-10
•
Expires: 2009-11-27
Abstract
Abstract A method of coloring dental restorations which consists of incorporating within the dental restoration material prior to curing a coloration agent which upon the application of heat or other energy alters the color of the restoration. By applying the energy in steps it is possible to match closely the color of the restoration to adjacent teeth or that of the tooth on which the restoration is mounted.
Inventors
- 👤 Gerald G. McLaughlin
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 23:07
CPC Classifications
A; A61; A61C; A61C13/00; A61C13/08; A61C13/082; A61K; A61K6/00; A61K6/80; A61K6/884; A61K6/887
Claims Analysis
Total Claims: 28
Claim 1
Independent Claim
122 words
A method of effecting the coloration of a restoration to be mounted on a tooth comprising the steps of: (a) incorporating into a dental composite which comprises a material selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methyacrylate monomer a coloration agent whose color changes when subject to the application of heat; (b) manufacturing said restoration from said dental composite without the application of heat; and (c) subjecting to repeated successive exposures at least a portion of said restoration to heat in a plurality of steps while placing said restoration on said tooth between each successive exposure of heat until the color of said restoration matches accurately a pre-selected color, followed by mounting said restoration.
Claim 2
Independent Claim
122 words
A method of effecting the coloration of a restoration to be mounted on a tooth comprising the steps of: (a) incorporating into a dental composite which comprises a material selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methyacrylate monomer a coloration agent whose color changes when subject to the application of heat; (b) manufacturing said restoration from said dental composite without the application of heat; and (c) subjecting to repeated successive exposures at least a portion of said restoration to heat in a plurality of steps while placing said restoration on said tooth between each successive exposure of heat until the color of said restoration matches accurately a pre-selected color, followed by mounting said restoration.
Claim 3
Dependent Claim
18 words
The method of claim 1 wherein a trace amount of said coloration agent is added to said mixture.
Claim 4
Dependent Claim
15 words
The method of claim 1 wherein said coloration agent consists of a micro-pulverized crystalline sugar.
Claim 5
Dependent Claim
20 words
The method of claim 1 wherein said coloration agent comprises a mixture of micro-pulverized crystalline sugar and anhydrous copper sulfate.
Claim 6
Dependent Claim
13 words
The method of claim 1 wherein said coloration agent comprises yellow iron oxide.
Claim 7
Dependent Claim
13 words
The method of claim 1 wherein said coloration agent comprises black iron oxide.
Claim 8
Independent Claim
156 words
A method of effecting the coloration of a restoration to be mounted on a tooth comprising the steps of: a. incorporating into a polymerizable mixture from which the restoration is manufactured a coloration agent selected from the class of materials which change color upon the application of heat, said polymerizable mixture selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methacrylate monomer; b. shaping said mixture into said restoration without the application of heat; c. polymerizing without the application of heat said mixture using a polymerizing agent which does not affect the color of said coloration agent; and d. subjecting to repeated successive exposures at least a portion of said restoration to heat in a plurality of steps while placing said restoration on said tooth between each successive exposure of heat until the color of said restoration matches accurately a pre-selected color followed by mounting said restoration permanently in place.
Claim 9
Independent Claim
156 words
A method of effecting the coloration of a restoration to be mounted on a tooth comprising the steps of: a. incorporating into a polymerizable mixture from which the restoration is manufactured a coloration agent selected from the class of materials which change color upon the application of heat, said polymerizable mixture selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methacrylate monomer; b. shaping said mixture into said restoration without the application of heat; c. polymerizing without the application of heat said mixture using a polymerizing agent which does not affect the color of said coloration agent; and d. subjecting to repeated successive exposures at least a portion of said restoration to heat in a plurality of steps while placing said restoration on said tooth between each successive exposure of heat until the color of said restoration matches accurately a pre-selected color followed by mounting said restoration permanently in place.
Claim 10
Dependent Claim
13 words
The method of claim 7 wherein said coloration agent is yellow iron oxide.
Claim 11
Dependent Claim
13 words
The method of claim 7 wherein said coloration agent is black iron oxide.
Claim 12
Independent Claim
126 words
A method of effecting the coloration of a dental restoration comprising the steps of: (a) incorporating into a polymerizable mixture from which the restoration is manufactured a coloration agent consisting of micro-pulverized crystalline sugar in an amount sufficient to cause a change in color upon the application of heat, said polymerizable mixture selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methacrylate monomer; (b) shaping said mixture into said restoration; (c) polymerizing said mixture using a polymerizing agent which does not affect the color of said coloration agent; and (d) subjecting at least a portion of said restoration to sufficient heat for a sufficient length of time to change the color of said restoration to match accurately a pre-selected color.
Claim 13
Independent Claim
126 words
A method of effecting the coloration of a dental restoration comprising the steps of: (a) incorporating into a polymerizable mixture from which the restoration is manufactured a coloration agent consisting of micro-pulverized crystalline sugar in an amount sufficient to cause a change in color upon the application of heat, said polymerizable mixture selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methacrylate monomer; (b) shaping said mixture into said restoration; (c) polymerizing said mixture using a polymerizing agent which does not affect the color of said coloration agent; and (d) subjecting at least a portion of said restoration to sufficient heat for a sufficient length of time to change the color of said restoration to match accurately a pre-selected color.
Claim 14
Dependent Claim
38 words
The method of claim 10 wherein a trace amount of said sugar is incorporated into said mixture, the fineness of said sugar being sufficient to obtain a uniform visible color in said restoration upon application of said heat.
Claim 15
Independent Claim
141 words
A method of effecting the coloration of a dental restoration comprising the steps of: a. incorporating into a polymerizable mixture from which the restoration is manufactured a trace amount of a coloration agent which is sufficient to change color upon the application of heat, said coloration agent consisting of a mixture of micro pulverized crystalline sugar and anhydrous copper sulfate in about equal volumes, said polymerizable mixture selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methacrylate monomer; b. shaping said mixture into said restoration; c. polymerizing said mixture using a polymerizing agent which does not affect the color of said coloration agent; and d. subjecting at least a portion of said restoration to sufficient heat for a sufficient length of time to change the color of said restoration to match accurately a pre-selected color.
Claim 16
Independent Claim
141 words
A method of effecting the coloration of a dental restoration comprising the steps of: a. incorporating into a polymerizable mixture from which the restoration is manufactured a trace amount of a coloration agent which is sufficient to change color upon the application of heat, said coloration agent consisting of a mixture of micro pulverized crystalline sugar and anhydrous copper sulfate in about equal volumes, said polymerizable mixture selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methacrylate monomer; b. shaping said mixture into said restoration; c. polymerizing said mixture using a polymerizing agent which does not affect the color of said coloration agent; and d. subjecting at least a portion of said restoration to sufficient heat for a sufficient length of time to change the color of said restoration to match accurately a pre-selected color.
Claim 17
Independent Claim
132 words
The method of effecting the coloration of a restoration to be mounted on a tooth comprising the steps of: a. incorporating into a polymerizable mixture from which the restoration is manufactured a coloration agent consisting of micro-pulverized crystalline sugar, said polymerizable mixture selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methacrylate monomer; b. shaping said mixture into said restoration; c. polymerizing said mixture using a polymerizing agent which does not affect the color of said coloration agent; and d. subjecting at least a portion of said restoration to heat in a plurality of steps while placing said restoration on said tooth between each application of heat until the color of said restoration matches accurately a pre-selected color followed by mounting said restoration permanently in place.
Claim 18
Independent Claim
132 words
The method of effecting the coloration of a restoration to be mounted on a tooth comprising the steps of: a. incorporating into a polymerizable mixture from which the restoration is manufactured a coloration agent consisting of micro-pulverized crystalline sugar, said polymerizable mixture selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methacrylate monomer; b. shaping said mixture into said restoration; c. polymerizing said mixture using a polymerizing agent which does not affect the color of said coloration agent; and d. subjecting at least a portion of said restoration to heat in a plurality of steps while placing said restoration on said tooth between each application of heat until the color of said restoration matches accurately a pre-selected color followed by mounting said restoration permanently in place.
Claim 19
Dependent Claim
38 words
The method of claim 13 wherein a trace amount of said sugar is incorporated into said mixture, the fineness of said sugar being sufficient to obtain a uniform visible color in said restoration after application of said heat.
Claim 20
Independent Claim
148 words
The method of effecting the coloration of a restoration to be mounted on a tooth comprising the steps of: a. incorporating into a polymerizable mixture from which the restoration is manufactured a coloration agent consisting of a mixture of micro pulverized crystalline sugar and anhydrous copper sulfate in about equal volumes in a trace amount, said polymerizable mixture selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methacrylate monomer; b. shaping said mixture into said restoration; c. polymerizing said mixture using a polymerizing agent which does not affect the color of said coloration agent; and d. subjecting at least a portion of said restoration to heat in a plurality of steps while placing said restoration on said tooth between each application of heat until the color of said restoration matches accurately a pre-selected color followed by mounting said restoration permanently in place.
Claim 21
Independent Claim
148 words
The method of effecting the coloration of a restoration to be mounted on a tooth comprising the steps of: a. incorporating into a polymerizable mixture from which the restoration is manufactured a coloration agent consisting of a mixture of micro pulverized crystalline sugar and anhydrous copper sulfate in about equal volumes in a trace amount, said polymerizable mixture selected from the group consisting of dimethacrylate monomer, methyl methacrylate, and polyurethane mixed with a methacrylate monomer; b. shaping said mixture into said restoration; c. polymerizing said mixture using a polymerizing agent which does not affect the color of said coloration agent; and d. subjecting at least a portion of said restoration to heat in a plurality of steps while placing said restoration on said tooth between each application of heat until the color of said restoration matches accurately a pre-selected color followed by mounting said restoration permanently in place.
Claim 22
Independent Claim
137 words
The method of effecting the coloration of a polymerizable dental restoration to be mounted on a tooth comprising the steps of: a. incorporating into a dental composite comprising an unsaturated polymerizable monomer from which the restoration is manufactured a coloration agent selected from the class of materials which change color upon the application of heat; b. shaping said mixture into said restoration; c. polymerizing said mixture without the application of said heat using a polymerizing agent which does not affect the color of said coloration agent; and d. subjecting to repeated successive exposures at least a portion of said restoration to said heat in a plurality of steps while said restoration is on said tooth until the color of said restoration matches accurately the color of an adjacent tooth followed by mounting said restoration permanently in place.
Claim 23
Independent Claim
137 words
The method of effecting the coloration of a polymerizable dental restoration to be mounted on a tooth comprising the steps of: a. incorporating into a dental composite comprising an unsaturated polymerizable monomer from which the restoration is manufactured a coloration agent selected from the class of materials which change color upon the application of heat; b. shaping said mixture into said restoration; c. polymerizing said mixture without the application of said heat using a polymerizing agent which does not affect the color of said coloration agent; and d. subjecting to repeated successive exposures at least a portion of said restoration to said heat in a plurality of steps while said restoration is on said tooth until the color of said restoration matches accurately the color of an adjacent tooth followed by mounting said restoration permanently in place.
Claim 24
Independent Claim
120 words
The method of effecting the coloration of a dental restoration to be mounted on a tooth comprising the steps of: a. incorporating into a polymerizable dental restorative material containing an unsaturated polymerizable monomer from which the restoration is manufactured a coloration agent selected from the class of materials which change color upon the application of heat; b. shaping said mixture into said restoration; c. curing said mixture using an agent which does not affect the color of said coloration agent; d. subjecting said restoration after curing to repeated successive exposures of said heat in a plurality of steps until the color of said restoration matches accurately a preselected color; and e. mounting said restoration permanently in place on said tooth.
Claim 25
Independent Claim
120 words
The method of effecting the coloration of a dental restoration to be mounted on a tooth comprising the steps of: a. incorporating into a polymerizable dental restorative material containing an unsaturated polymerizable monomer from which the restoration is manufactured a coloration agent selected from the class of materials which change color upon the application of heat; b. shaping said mixture into said restoration; c. curing said mixture using an agent which does not affect the color of said coloration agent; d. subjecting said restoration after curing to repeated successive exposures of said heat in a plurality of steps until the color of said restoration matches accurately a preselected color; and e. mounting said restoration permanently in place on said tooth.
Claim 26
Dependent Claim
29 words
The method of claim 17 in which said restoration is removed for exposure to said heat and is mountable on said tooth between the successive exposures of said heat.
Claim 27
Dependent Claim
35 words
The method of claim 17 in which said restoration is mounted on said tooth during the successive exposures of said heat so that the color of said restoration is altered while said restoration is mounted.
Claim 28
Dependent Claim
38 words
The method of claim 17 in which said preselected color is the color of an adjacent tooth so that said successive exposures are continued until the color of said restoration approaches and matches that of said adjacent tooth.
References Cited (Backward Citations)
US3488846A
Cited
US3932938A
Cited
US4150485A
Cited
US4261879A
Cited
US4481227A
Cited
US4512743A
Cited
US4433959A
Cited
US4563153A
Cited
US4650418A
Cited
US4650418B1
Cited
US4743642A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1995-03-10 | 1995-09-09 | 1996-03-10 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1999-03-10 | 1999-09-09 | 2000-03-10 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2003-03-10 | 2003-09-09 | 2004-03-10 | $7700.00 | Window Closed / Lapsed |