Patent US5077053A successfully refreshed from Google Patents.
US5077053A
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US
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Zein as a moisture barrier for sugarless edible compositions and method for preparing same
Assignee: Warner Lambert Co LLC
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Filing: 1990-02-12
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Granted: 1991-12-31
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Expires: 2010-02-12
Abstract
Abstract The present invention pertains to an edible coated composition which comprises (a) a core material comprising sorbitol, (b) a primary coating layer comprising zein over the core material, and (c) a sugarless secondary coasting layer over the primary coating layer. The present invention also pertains to methods for preparing the edible coated compositions.
Inventors
- 👤 Thomas J. Kuncewitch
- 👤 Jose Silva
- 👤 Daniel A. Orlandi
- 👤 Michael Glass
- 👤 Jose F. Zamudio-Tena
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-02 23:25
CPC Classifications
A; A23; A23G; A23G3/00; A23G3/34; A23G3/36; A23G3/44; A23G3/02; A23G3/20; A23G3/26; A23G3/343; A23G3/42; A23G3/50; A23G3/54; A23P; A23P20/00; A23P20/10; A23G2200/00; A23G2200/10
Claims Analysis
Total Claims: 23
Claim 1
Independent Claim
68 words
An edible coated tablet composition which comprises: (a) a core material comprising sorbitol, (b) a primary coating layer consisting essentially of zein over the core material, and (c) a secondary coating layer over the primary layer, said secondary layer obtained by applying at least one aqueous solution comprising a saturated sorbitol solution, a crystalline sorbitol powder, one or more film-forming agents, and one or more crystallization retarding agents.
Claim 2
Dependent Claim
68 words
An edible coated tablet composition which comprises: (a) a core material comprising sorbitol, (b) a primary coating layer consisting essentially of zein over the core material, and (c) a secondary coating layer over the primary layer, said secondary layer obtained by applying at least one aqueous solution comprising a saturated sorbitol solution, a crystalline sorbitol powder, one or more film-forming agents, and one or more crystallization retarding agents.
Claim 3
Dependent Claim
50 words
The composition according to claim 1, wherein the core material comprises the following ingredients: ______________________________________
Ingredient Percentage by Weight
______________________________________
Sorbitol 84.00-98.00
Acidulant 0.50-3.00
Breath freshening agent
0.50-0.80
Intense sweetening agent
0.00-0.10
Flavoring agent 0.50-2.00
Lubricating agent
0.10-0.50
Vegetable oil 0.00-0.50
Emulsifying agent
0.00-0.20
Coloring agent 0.00-0.03
Fillers 0.00-15.00
______________________________________
Claim 4
Dependent Claim
13 words
The composition according to claim 1, wherein the secondary coating layer comprises sorbitol.
Claim 5
Dependent Claim
72 words
The composition according to claim 3, wherein the secondary coating layer comprises in percentages by weight: (a) from about 77% to about 83% of sorbitol solution comprising from about 65% to about 75% sorbitol, (b) from about 9.5% to about 12.5% crystalline sorbitol powder, (c) from about 0.25% to about 1.5% of at least one film-forming agent, and (d) from about 0.1% to about 5.0% of at least one crystallization retarding agent.
Claim 6
Dependent Claim
141 words
The composition according to claim 4, wherein the secondary coating layer comprises two coating layers wherein the first coating layer comprises in percentages by weight: (a) from about 77% to about 83% of sorbitol solution comprising from about 65% to about 75% sorbitol, (b) from about 9.5% to about 12.5% crystalline sorbitol powder, (c) from about 0.25% to about 1.5% of at least one film-forming agent, and (d) from about 0.1% to about 5.0% of at least one crystallization retarding agent, and the second coating layer comprises in percentages by weight: (a) about 82% to about 94% sorbitol solution comprising about 65% to about 75% sorbitol, (b) about 1.0% to about 3.5% crystalline sorbitol powder, (c) about 0.05% to about 2.0% of at least one film-forming agent, and (d) about 0.1% to about 0.3% of at least one crystallization retarding agent.
Claim 7
Dependent Claim
28 words
The composition according to claim 1, wherein the core material is present in an amount from about 40% to about 60%, by weight of the edible coated composition.
Claim 8
Dependent Claim
29 words
The composition according to claim 1, wherein the primary coating layer is present in an amount from about 0.1% to about 1.5%, by weight of the edible coated composition.
Claim 9
Dependent Claim
29 words
The composition according to claim 1, wherein the secondary coating layer is present in an amount from about 40% to about 60%, by weight of the edible coated composition.
Claim 10
Independent Claim
129 words
A method for preparing an edible coated tablet composition which comprises the steps of: (A) providing the following ingredients: (a) a solid core material composition which comprises sorbitol, (b) a solution of a primary coating layer composition consisting essentially of zein, (c) an aqueous secondary coating layer solution comprising a saturated sorbitol solution, a crystalline sorbitol powder, one or more film-forming agents, and one or more crystallization retarding agents; and (B) forming the core material composition into a suitable tablet shape, (C) coating the core material from step (B) with the primary coating layer solution, (D) drying the coated core material from step (C), (E) coating the coated core material from step (D) with the secondary coating layer solution, and (F) drying the coated core material from step (E).
Claim 11
Independent Claim
129 words
A method for preparing an edible coated tablet composition which comprises the steps of: (A) providing the following ingredients: (a) a solid core material composition which comprises sorbitol, (b) a solution of a primary coating layer composition consisting essentially of zein, (c) an aqueous secondary coating layer solution comprising a saturated sorbitol solution, a crystalline sorbitol powder, one or more film-forming agents, and one or more crystallization retarding agents; and (B) forming the core material composition into a suitable tablet shape, (C) coating the core material from step (B) with the primary coating layer solution, (D) drying the coated core material from step (C), (E) coating the coated core material from step (D) with the secondary coating layer solution, and (F) drying the coated core material from step (E).
Claim 12
Dependent Claim
50 words
The method according to claim 9, wherein the core material comprises the following ingredients: ______________________________________
Ingredient Percentage by Weight
______________________________________
Sorbitol 84.00-98.00
Acidulant 0.50-3.00
Breath freshening agent
0.50-0.80
Intense sweetening agent
0.00-0.10
Flavoring agent 0.50-2.00
Lubricating agent
0.10-0.50
Vegetable oil 0.00-0.50
Emulsifying agent
0.00-0.20
Coloring agent 0.00-0.03
Fillers 0.00-15.00
______________________________________
Claim 13
Dependent Claim
29 words
The method according to claim 9, wherein the solution of primary coating layer composition comprises a solution from about 10% to about 20% of zein in aqueous propylene glycol.
Claim 14
Dependent Claim
16 words
The method according to claim 9, wherein the solution of secondary coating layer composition comprises sorbitol.
Claim 15
Dependent Claim
75 words
The method according to claim 12, wherein the solution of secondary coating layer composition comprises in percentages by weight: (a) from about 77% to about 83% of sorbitol solution comprising from about 65% to about 75% sorbitol, (b) from about 9.5% to about 12.5% crystalline sorbitol powder, (c) from about 0.25% to about 1.5% of at least one film-forming agent, and (d) from about 0.1% to about 5.0% of at least one crystallization retarding agent.
Claim 16
Dependent Claim
153 words
The method according to claim 13, wherein the solution of secondary coating layer comprises two coating layers wherein the first coating layer comprises in percentages by weight: (a) from about 77% to about 83% of sorbitol solution comprising from about 65% to about 75% sorbitol, (b) from about 9.5% to about 12.5% crystalline sorbitol powder, (c) from about 0.25% to about 1.5% of at least one film-forming agent, and (d) from about 0.1% to about 5.0% of at least one crystallization retarding agent, and the second coating layer comprises in percentages by weight: (a) about 82% to about 94% by weight sorbitol solution comprising about 65% to about 75% by weight sorbitol, (b) about 1.0% to about 3.5% by weight crystalline sorbitol powder, (c) about 0.05% to about 2.0% by weight of at least one film-forming agent, and (d) about 0.1% to about 0.3% by weight of at least one crystallization retarding agent.
Claim 17
Dependent Claim
28 words
The method according to claim 9, wherein the core material is present in an amount from about 40% to about 60%, by weight of the edible coated composition.
Claim 18
Dependent Claim
29 words
The method according to claim 9, wherein the primary coating layer is present in an amount from about 0.1% to about 1.5%, by weight of the edible coated composition.
Claim 19
Dependent Claim
29 words
The method according to claim 9, wherein the secondary coating layer is present in an amount from about 40% to about 60%, by weight of the edible coated composition.
Claim 20
Independent Claim
131 words
A method for protecting a moisture-sensitive tablet core material comprising sorbitol which comprises the steps of: (A) providing the following ingredients: (a) a solid core material composition which comprises sorbitol, (b) a solution of a primary coating layer composition consisting essentially of zein, (c) an aqueous secondary coating layer solution comprising a saturated sorbitol solution, a crystalline sorbitol powder, one or more film-forming agents, and one or more crystallization retarding agents; and (B) forming the core material composition into a suitable tablet shape, (C) coating the core material from step (B) with the primary coating layer composition, (D) drying the coated core material from step (C), (E) coating the coated core material from step (D) with the secondary coating layer composition, and (F) drying the coated core material from step (E).
Claim 21
Independent Claim
131 words
A method for protecting a moisture-sensitive tablet core material comprising sorbitol which comprises the steps of: (A) providing the following ingredients: (a) a solid core material composition which comprises sorbitol, (b) a solution of a primary coating layer composition consisting essentially of zein, (c) an aqueous secondary coating layer solution comprising a saturated sorbitol solution, a crystalline sorbitol powder, one or more film-forming agents, and one or more crystallization retarding agents; and (B) forming the core material composition into a suitable tablet shape, (C) coating the core material from step (B) with the primary coating layer composition, (D) drying the coated core material from step (C), (E) coating the coated core material from step (D) with the secondary coating layer composition, and (F) drying the coated core material from step (E).
Claim 22
Independent Claim
145 words
A method for protecting the color of a sugarless coating layer in an edible tablet composition which comprises the steps of: (A) providing the following ingredients: (a) a solid core material composition which comprises sorbitol and an acidulant, (b) a solution of a primary coating layer composition consisting essentially of zein, (c) an aqueous secondary coating layer solution comprising a saturated sorbitol solution, a crystalline sorbitol powder, one or more film-forming agents, one or more crystallization retarding agents, a coloring agent, and a metal carbonate; and (B) forming the core material composition into a suitable tablet shape, (C) coating the core material from step (B) with the primary coating layer composition, (D) drying the coated core material from step (C), (E) coating the coated core material from step (D) with the secondary coating layer composition, and (F) drying the coated core material from step (E).
Claim 23
Independent Claim
145 words
A method for protecting the color of a sugarless coating layer in an edible tablet composition which comprises the steps of: (A) providing the following ingredients: (a) a solid core material composition which comprises sorbitol and an acidulant, (b) a solution of a primary coating layer composition consisting essentially of zein, (c) an aqueous secondary coating layer solution comprising a saturated sorbitol solution, a crystalline sorbitol powder, one or more film-forming agents, one or more crystallization retarding agents, a coloring agent, and a metal carbonate; and (B) forming the core material composition into a suitable tablet shape, (C) coating the core material from step (B) with the primary coating layer composition, (D) drying the coated core material from step (C), (E) coating the coated core material from step (D) with the secondary coating layer composition, and (F) drying the coated core material from step (E).
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1994-12-30 | 1995-07-01 | 1995-12-31 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1998-12-30 | 1999-07-01 | 1999-12-31 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2002-12-30 | 2003-07-01 | 2003-12-31 | $7700.00 | Window Closed / Lapsed |