Patent US5028367A successfully refreshed from Google Patents.
US5028367A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Two-stage fast debinding of injection molding powder compacts
Assignee: Rensselaer Polytechnic Institute
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Filing: 1989-12-08
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Granted: 1991-07-02
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Expires: 2009-12-08
Abstract
Abstract A process for making molded objects utilizes powder injection molding techniques. Powder is mixed with a binder and then cast into a compact. The compact is then subjected to a first debinding step in the presence of a wicking agent under gentle heating. In this first stage, at least 40% of the binder is removed. Additional binder is then removed in a subsequent higher temperature stage to produce a compact which is free of binder and free of cracks.
Inventors
- 👤 Tai-Shing Wei
- 👤 Randall M. German
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 22:31
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/622; C04B35/626; C04B35/63; C04B35/638; B; B22; B22F; B22F3/00; B22F3/10; B22F3/1017; B22F3/1021; B22F3/1025
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
263 words
A process for making a molded object, comprising: mixing a waxy binder with a powder including at least one of powdered metal, powdered ceramics, powdered cermets and powdered composites to form a mixture having about from 15% to 50% by volume binder and particles of up to 100 microns in size; compressing the mixture under heating and pressure to form a compact containing binder and having a powder portion with a pore size; supporting the compact in a wicking medium which can absorb melted binder by capillary action from the compact, the wicking medium comprising a freely deformable and porous wicking medium having a pore size which is smaller than the pore size of to powder portion of the compact; removing at least 40% of the binder from the compact in a first stage while the compact is in contact with the wicking medium, by heating the compact to a temperature above the melting point of the binder and below the vaporization and decomposition temperature of the binder, and at a rate of 5° C. to 10° C. per minute, the melted binder being received into the wicking medium from the compact by capillary action; removing remaining binder from the porous compact in a second steps by removing the compact from the wicking medium and thereafter exposing the porous compact to a temperature at least as high as the vaporization temperature of the binder to form a binder free compact, the second stage being conducted under isothermal conditions; and after the second stage, sintering the binder free compact to form the molded object.
Claim 2
Dependent Claim
263 words
A process for making a molded object, comprising: mixing a waxy binder with a powder including at least one of powdered metal, powdered ceramics, powdered cermets and powdered composites to form a mixture having about from 15% to 50% by volume binder and particles of up to 100 microns in size; compressing the mixture under heating and pressure to form a compact containing binder and having a powder portion with a pore size; supporting the compact in a wicking medium which can absorb melted binder by capillary action from the compact, the wicking medium comprising a freely deformable and porous wicking medium having a pore size which is smaller than the pore size of to powder portion of the compact; removing at least 40% of the binder from the compact in a first stage while the compact is in contact with the wicking medium, by heating the compact to a temperature above the melting point of the binder and below the vaporization and decomposition temperature of the binder, and at a rate of 5° C. to 10° C. per minute, the melted binder being received into the wicking medium from the compact by capillary action; removing remaining binder from the porous compact in a second steps by removing the compact from the wicking medium and thereafter exposing the porous compact to a temperature at least as high as the vaporization temperature of the binder to form a binder free compact, the second stage being conducted under isothermal conditions; and after the second stage, sintering the binder free compact to form the molded object.
Claim 3
Dependent Claim
15 words
A process according to claim 1 wherein the wicking medium is high temperature resistant powder.
Claim 4
Dependent Claim
17 words
A process according to claim 1 wherein the wicking medium is high temperature resistant cloth like material.
Claim 5
Dependent Claim
15 words
A process according to claim 2, wherein said high temperature resistant powder comprises alumina powder.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1994-07-01 | 1994-12-31 | 1995-07-02 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1998-07-01 | 1998-12-31 | 1999-07-02 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2002-07-01 | 2002-12-31 | 2003-07-02 | $7700.00 | Window Closed / Lapsed |