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US5028367A Expired / Lapsed US ⏱️ 0.0 years remaining

Two-stage fast debinding of injection molding powder compacts

Assignee: Rensselaer Polytechnic Institute
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Filing: 1989-12-08
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Granted: 1991-07-02
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Expires: 2009-12-08
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Abstract

Abstract A process for making molded objects utilizes powder injection molding techniques. Powder is mixed with a binder and then cast into a compact. The compact is then subjected to a first debinding step in the presence of a wicking agent under gentle heating. In this first stage, at least 40% of the binder is removed. Additional binder is then removed in a subsequent higher temperature stage to produce a compact which is free of binder and free of cracks.

Inventors

  • 👤 Tai-Shing Wei
  • 👤 Randall M. German

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 19:44
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/622; C04B35/626; C04B35/63; C04B35/638; B; B22; B22F; B22F3/00; B22F3/10; B22F3/1017; B22F3/1021; B22F3/1025

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 263 words
A process for making a molded object, comprising: mixing a waxy binder with a powder including at least one of powdered metal, powdered ceramics, powdered cermets and powdered composites to form a mixture having about from 15% to 50% by volume binder and particles of up to 100 microns in size; compressing the mixture under heating and pressure to form a compact containing binder and having a powder portion with a pore size; supporting the compact in a wicking medium which can absorb melted binder by capillary action from the compact, the wicking medium comprising a freely deformable and porous wicking medium having a pore size which is smaller than the pore size of to powder portion of the compact; removing at least 40% of the binder from the compact in a first stage while the compact is in contact with the wicking medium, by heating the compact to a temperature above the melting point of the binder and below the vaporization and decomposition temperature of the binder, and at a rate of 5° C. to 10° C. per minute, the melted binder being received into the wicking medium from the compact by capillary action; removing remaining binder from the porous compact in a second steps by removing the compact from the wicking medium and thereafter exposing the porous compact to a temperature at least as high as the vaporization temperature of the binder to form a binder free compact, the second stage being conducted under isothermal conditions; and after the second stage, sintering the binder free compact to form the molded object.
Claim 2
Dependent Claim 263 words
A process for making a molded object, comprising: mixing a waxy binder with a powder including at least one of powdered metal, powdered ceramics, powdered cermets and powdered composites to form a mixture having about from 15% to 50% by volume binder and particles of up to 100 microns in size; compressing the mixture under heating and pressure to form a compact containing binder and having a powder portion with a pore size; supporting the compact in a wicking medium which can absorb melted binder by capillary action from the compact, the wicking medium comprising a freely deformable and porous wicking medium having a pore size which is smaller than the pore size of to powder portion of the compact; removing at least 40% of the binder from the compact in a first stage while the compact is in contact with the wicking medium, by heating the compact to a temperature above the melting point of the binder and below the vaporization and decomposition temperature of the binder, and at a rate of 5° C. to 10° C. per minute, the melted binder being received into the wicking medium from the compact by capillary action; removing remaining binder from the porous compact in a second steps by removing the compact from the wicking medium and thereafter exposing the porous compact to a temperature at least as high as the vaporization temperature of the binder to form a binder free compact, the second stage being conducted under isothermal conditions; and after the second stage, sintering the binder free compact to form the molded object.
Claim 3
Dependent Claim 15 words
A process according to claim 1 wherein the wicking medium is high temperature resistant powder.
Claim 4
Dependent Claim 17 words
A process according to claim 1 wherein the wicking medium is high temperature resistant cloth like material.
Claim 5
Dependent Claim 15 words
A process according to claim 2, wherein said high temperature resistant powder comprises alumina powder.

References Cited (Backward Citations)

US4197118A Cited
US4113480A Cited
US4305756A Cited
US4404166A Cited
JPS60118664A Cited
US4713206A Cited
JPS6177671A Cited
US4704242A Cited
JPH01184204A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-07-01 1994-12-31 1995-07-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-07-01 1998-12-31 1999-07-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-07-01 2002-12-31 2003-07-02 $7700.00 Window Closed / Lapsed

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