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US5000771A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for manufacturing an article comprising a refractory dielectric body

Assignee: Furukawa Electric North America Inc
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Filing: 1989-12-29
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Granted: 1991-03-19
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Expires: 2009-12-29
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Abstract

Abstract To attain high strength optical glass fibers, the glass preforms, from which the fibers are drawn, must generally be free of surface imperfections such as bubbles, and air lines. It has been discovered that these imperfections can be removed quickly and cleanly by contacting the preform surface with a substantial portion of the electrically conducting plasma region (the plasma fireball) extending from a plasma torch. Significantly, the surface material is substantially removed by vaporization, due to the extremely high plasma temperature (>9000° C. at the plasma center) of the isothermal plasma torch. Though the temperatures in the tail of the plasma fireball are substantially less than at the plasma center, the temperatures are generally still several thousand degrees centigrade. These tail temperatures typically are sufficiently high to cause vaporization of most refractory dielectrics making the inventive method applicable to the fabrication of a wide variety of articles comprising refractory dielectric bodies. Advantageously, selective etching, according to one aspect of the inventive method, is used to remove fiber preform eccentricity and to fabricate optical fiber preforms with non-circular cross-sections for such applications as fiber sensors. Selective etching can result by controlling the plasma fireball location, the rotation of the silica preform, and/or the travel of the fireball across the preform. Significantly, the fireball location is controlled, among other ways, by injecting into the torch an additional gas that has a high ionization threshold or by inserting a probe along the axis of the torch. In either case, a substantial portion of the plasma fireball is advantageously "pushed" outside the torch for ease of contact with the silica preform surface, or any other refractory dielectric being processed.

Inventors

  • 👤 James W. Fleming, Jr.
  • 👤 Fred P. Partus

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 16:20
CPC Classifications
C; C03; C03B; C03B37/00; C03B37/01; C03B37/012; C03B37/014; C03B37/0148; C03B37/01205; C03B37/01225; C03B37/01228; C03B37/01237; C03B37/01257; C03B37/01446

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 105 words
Method for manufacturing an article comprising a refractory dielectric material, the method comprising: (a) providing a refractory dielectric body; (b) removing a portion of material from the refractory dielectric body; and (c) completing manufacturing the article; Characterized in that (d) step (b) comprises exposing the refractory dielectric body to a substantially localized heat source so that at least a substantial part of the portion of material is removed by vaporization, the heat source comprising a plasma fireball generated by a plasma torch, the plasma fireball being the electrically conducting portion of a plasma into which plasma sustaining electromagnetic energy is coupled by the plasma torch.
Claim 2
Dependent Claim 105 words
Method for manufacturing an article comprising a refractory dielectric material, the method comprising: (a) providing a refractory dielectric body; (b) removing a portion of material from the refractory dielectric body; and (c) completing manufacturing the article; Characterized in that (d) step (b) comprises exposing the refractory dielectric body to a substantially localized heat source so that at least a substantial part of the portion of material is removed by vaporization, the heat source comprising a plasma fireball generated by a plasma torch, the plasma fireball being the electrically conducting portion of a plasma into which plasma sustaining electromagnetic energy is coupled by the plasma torch.
Claim 3
Dependent Claim 44 words
Method of claim 1, wherein the heat source comprises contact with the plasma fireball generated by the plasma torch, the plasma generated from a first gas, associated with the first gas being an ionization threshold, and associated with the plasma torch being an axis.
Claim 4
Dependent Claim 18 words
Method of claim 2, wherein the refractory dielectric body is an optical fiber preform comprising a silica glass.
Claim 5
Dependent Claim 10 words
Method of claim 2, wherein the first gas comprises oxygen.
Claim 6
Dependent Claim 30 words
Method of claim 2, comprising introducing a second gas into the plasma torch, where the second gas has a ionization threshold that is higher than that of the first gas.
Claim 7
Dependent Claim 30 words
Method of claim 2, comprising positioning a substantial portion of the plasma fireball outside the plasma torch, the portion being in the range 0.01% to 50% of the fireball volume.
Claim 8
Dependent Claim 10 words
Method of claim 5, wherein the second gas is nitrogen.
Claim 9
Dependent Claim 25 words
Method of claim 2, wherein the plasma torch comprises an electrically insulated probe means extending into the plasma torch substantially along the plasma torch axis.
Claim 10
Dependent Claim 22 words
Method of claim 2, comprising moving the plasma fireball along the refractory dielectric body at a speed in the range 0.01-100 cm/sec.
Claim 11
Dependent Claim 39 words
Method of claim 2, comprising rotating the refractory dielectric body, at least during some interval while removing a portion of material from the refractory dielectric body, at varying rates in the range from 0.0 rpm to about 200 rpm.
Claim 12
Dependent Claim 11 words
Method of claim 3, wherein the article is an optical fiber.
Claim 13
Dependent Claim 13 words
Method of claim 3, wherein the preform further comprises a synthetic silica substrate.
Claim 14
Dependent Claim 12 words
Method of claim 2, wherein the article is an optical fiber sensor.

References Cited (Backward Citations)

US4718976A Cited
US4630890A Cited
US4491463A Cited
US4498917A Cited
US4698126A Cited
US4758304A Cited
US4793897A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-03-18 1994-09-17 1995-03-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-03-18 1998-09-17 1999-03-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-03-18 2002-09-17 2003-03-19 $7700.00 Window Closed / Lapsed

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