Patent US4861382A successfully refreshed from Google Patents.
US4861382A
Expired / Lapsed
US
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Sugar process
Assignee: Tate and Lyle PLC
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Filing: 1987-10-05
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Granted: 1989-08-29
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Expires: 2007-10-05
Abstract
Abstract A continuous process for the crystallization of fructose from an aqueous fructose syrup containing at least 90% by weight fructose on a dry solids basis, in which the syrup at a total solids content of at least 95% by weight is rapidly and thoroughly mixed with seed, at a temperature of 55 DEG -75 DEG e.g for up to 2.5 minutes; is then deposited onto a surface where it is allowed to crystallize under quiescent conditions at a temperature of about 50 DEG -70 DEG , until a solid cake is formed; and is the comminuted to provide a free-flowing granular product which can be further dried. The process provides a particulate product in the form of crystals in a glossy matrix, in which 95% of the crystals have a particle size of less than 20 microns, the overall degree of crystallinity is greater than 70%, the bulk density is less than 0.65 and which is completely free of organic solvent residues. Other food ingredients may be added simultaneously with the seed.
Inventors
- 👤 Brita C. Goodacre
- 👤 Alan Smithson
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 01:09
CPC Classifications
C; C13; C13K; C13K11/00
Claims Analysis
Total Claims: 14
Claim 1
Independent Claim
143 words
A continuous process for the total solidification of fructose comprising the steps of, in the absence of organic solvent, (a) rapidly and thoroughly mixing together aqueous fructose syrup containing at least 90% by weight fructose on a dry solids basis and a total solids content of at least 95% by weight with 5-30 weight % fructose seed crystals, in a screw extruder at a temperature of 55°-75° for up to 2.5 minutes to form a viscous flowable slurry having a degree of crystallinity not much more than provided by the seed; (b) depositing the viscous flowable slurry onto a surface and allowing it to solidify under quiescent conditions at a temperature of about 50°-70°, until a solid cake is formed; and (c) breaking up and comminuting the solid cake to provide a free-flowing granular product having a degree of crystallinity of over 50%.
Claim 2
Dependent Claim
143 words
A continuous process for the total solidification of fructose comprising the steps of, in the absence of organic solvent, (a) rapidly and thoroughly mixing together aqueous fructose syrup containing at least 90% by weight fructose on a dry solids basis and a total solids content of at least 95% by weight with 5-30 weight % fructose seed crystals, in a screw extruder at a temperature of 55°-75° for up to 2.5 minutes to form a viscous flowable slurry having a degree of crystallinity not much more than provided by the seed; (b) depositing the viscous flowable slurry onto a surface and allowing it to solidify under quiescent conditions at a temperature of about 50°-70°, until a solid cake is formed; and (c) breaking up and comminuting the solid cake to provide a free-flowing granular product having a degree of crystallinity of over 50%.
Claim 3
Dependent Claim
16 words
A process according to claim 1, in which the mixing time is up to 2 minutes.
Claim 4
Dependent Claim
18 words
A process according to claim 1, in which the syrup has a solids concentration of 95-98.5% by weight.
Claim 5
Dependent Claim
21 words
A process according to claim 1, in which the seed is added at a level in excess of 5% by weight.
Claim 6
Dependent Claim
21 words
A process according to claim 4, in which the seed is added at a level of 0 to 20% by weight.
Claim 7
Dependent Claim
22 words
A process according to claim 1, in which the seed has a particle size range within the range 75 to 355 microns.
Claim 8
Dependent Claim
17 words
A process according to claim 1, in which the product is further crystallised by a drying process.
Claim 9
Dependent Claim
158 words
A continuous process for the total solidification of fructose from an aqueous fructose syrup which consists essentially of the steps of, in the absence of organic solvent, rapidly and thoroughly mixing together for up to 2.5 minutes an aqueous fructose syrup containing at least 90% by weight fructose on a dry solids basis and a total solids content of at least 95% by weight with 5-30% by weight thereof of fructose seed crystals in a screw extruder at a temperature of 55° to 75° C., to form a viscous flowable slurry having a degree of crystallinity not much more than provided by the seed, depositing the slurry onto a surface and allowing the fructose to crystallize under quiescent conditions at a temperature of about 50° to 70° C. for up to 3 hours until a solid cake is formed, and comminuting the solid cake to provide a free-flowing granular product having a degree of crystallinity of over 50%.
Claim 10
Dependent Claim
158 words
A continuous process for the total solidification of fructose from an aqueous fructose syrup which consists essentially of the steps of, in the absence of organic solvent, rapidly and thoroughly mixing together for up to 2.5 minutes an aqueous fructose syrup containing at least 90% by weight fructose on a dry solids basis and a total solids content of at least 95% by weight with 5-30% by weight thereof of fructose seed crystals in a screw extruder at a temperature of 55° to 75° C., to form a viscous flowable slurry having a degree of crystallinity not much more than provided by the seed, depositing the slurry onto a surface and allowing the fructose to crystallize under quiescent conditions at a temperature of about 50° to 70° C. for up to 3 hours until a solid cake is formed, and comminuting the solid cake to provide a free-flowing granular product having a degree of crystallinity of over 50%.
Claim 11
Dependent Claim
41 words
The process of claim 8 in which the mixing time is up to 2 minutes, the syrup has a solid concentration of 95 to 98.5% by weight and the seed is added at a level of 10 to 20% by weight.
Claim 12
Dependent Claim
34 words
The process of claim 9 wherein the mixing is effected in said screw extruder operated at a rate of 100 to 300 rev.min -1 and the mixing time is about 30 to 90 seconds.
Claim 13
Dependent Claim
22 words
A process according to claim 10, in which the seed has a particle size range within the range 75 to 355 microns.
Claim 14
Dependent Claim
27 words
The process of claim 11, in which the freeflowing granular product is further crystallized by a drying process to a degree of crystallinity of at least 70%.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1992-08-28 | 1993-02-27 | 1993-08-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1996-08-28 | 1997-02-27 | 1997-08-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2000-08-28 | 2001-02-27 | 2001-08-29 | $7700.00 | Window Closed / Lapsed |