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US4814307A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing an electrode substrate which is uniform in physical properties

Assignee: Kureha Corp
•
Filing: 1987-06-30
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Granted: 1989-03-21
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Expires: 2007-06-30
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Abstract

Abstract Disclosed herein are a process for producing an electrode substrate, which process comprises the steps of kneading a raw material mixture comprising from 30 to 60% by weight of short carbon fibers, from 20 to 50% by weight of a phenol resin binder and from 20 to 50% by weight of a molding additive, extruding the thus kneaded raw material mixture and after press-molding the thus extruded material by rolling or stamping, calcining the thus press-molded material in an inert atmosphere and/or under a reduced pressure and the electrode substrate produced by the above-mentioned process.

Inventors

  • 👤 Masayuki Funabashi
  • 👤 Masayosi Sibuya

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 07:30
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/71; C04B35/78; C04B35/80; C04B35/83; H; H01; H01M; H01M4/00; H01M4/86; H01M4/96; Y; Y02; Y02E; Y02E60/00; Y02E60/30; Y02E60/50

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 193 words
A process for continuously producing an electrode substrate, which process comprises the steps of: (1) kneading, at a temperature of not higher than 110° C. a raw material mixture comprising from 30 to 60% by weight of short carbon fibers, from 20 to 50% by weight of a phenol resin binder, and from 20 to 50% by weight of a molding additive of an organic high polymer having a carbonizing yield of not more than 5% by weight, said organic high polymer being selected from a copolymer resin of ethylene and vinyl acetate, and a mixture of a copolymer resin of ethylene and vinyl acetate and a polyolefin; (2) extruding the thus kneaded raw material mixture through an extrusion die; (3) thereafter heating the thus extruded raw material to a temperature of from 130° to 180° C., and press-molding the thus heated material under a pressure of from 20 to 80 kgf/cm 2 by rolling or stamping, and then (4) calcining the thus press-molded material for about one hour at a temperature of from 800° to 3000° C. in an inert atmosphere and/or under a reduced pressure, whereby said electrode substrate is formed.
Claim 2
Dependent Claim 193 words
A process for continuously producing an electrode substrate, which process comprises the steps of: (1) kneading, at a temperature of not higher than 110° C. a raw material mixture comprising from 30 to 60% by weight of short carbon fibers, from 20 to 50% by weight of a phenol resin binder, and from 20 to 50% by weight of a molding additive of an organic high polymer having a carbonizing yield of not more than 5% by weight, said organic high polymer being selected from a copolymer resin of ethylene and vinyl acetate, and a mixture of a copolymer resin of ethylene and vinyl acetate and a polyolefin; (2) extruding the thus kneaded raw material mixture through an extrusion die; (3) thereafter heating the thus extruded raw material to a temperature of from 130° to 180° C., and press-molding the thus heated material under a pressure of from 20 to 80 kgf/cm 2 by rolling or stamping, and then (4) calcining the thus press-molded material for about one hour at a temperature of from 800° to 3000° C. in an inert atmosphere and/or under a reduced pressure, whereby said electrode substrate is formed.
Claim 3
Dependent Claim 20 words
A process according to claim 1, wherein the kneading of step (1) is practiced for not longer than 10 minutes.
Claim 4
Dependent Claim 62 words
A process according to claim 1, wherein said short carbon fibers have diameters of from 5 to 30 micrometers and lengths of from 0.05 to 2 mm, and wherein the carbonizing linear shrinkage of said short carbon fibers is not more than 3% when said short carbon fibers are calcined at 2000° C. in an inert atmosphere and/or under a reduced pressured.
Claim 5
Dependent Claim 22 words
A process according to claim 1, wherein the carbonizing yield of said phenol resin binder is from 30 to 75% by weight.
Claim 6
Dependent Claim 46 words
A process according to claim 1, wherein the mixture of a copolymer resin of ethylene and vinyl acetate and a polyolefin comprises 100 parts by weight of said copolymer resin of ethylene and vinyl acetate and not more than 100 parts by weight of said polyolefin.
Claim 7
Dependent Claim 12 words
A process according to claim 1, wherein said polyolefin is a polyethylene.
Claim 8
Dependent Claim 45 words
A process according to claim 1, wherein said raw material mixture comprises from 35 to 50% by weight of said short carbon fibers, from 25 to 40% by weight of said phenol resin binder and from 25 to 40% by weight of said molding additive.
Claim 9
Dependent Claim 30 words
A process according to claim 1, wherein step (3) is practiced so as to select a shape of the roll or stamp to produce a press-molded material of desired shape.
Claim 10
Dependent Claim 23 words
A process as in claim 1, wherein step (2) is practiced by extruding the kneaded raw material mixture through a T-shaped extrusion die.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-03-20 1992-09-19 1993-03-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-03-20 1996-09-19 1997-03-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-03-20 2000-09-19 2001-03-21 $7700.00 Window Closed / Lapsed

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