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US4774096A Expired / Lapsed US ⏱️ 0.0 years remaining

Novel fibrous product

Assignee: Ogilvie Mills Ltd
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Filing: 1986-07-23
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Granted: 1988-09-27
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Expires: 2006-07-23
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Abstract

Abstract A process for the preparation of a fibrous natural product comprising agitating an aqueous slurry of ground material from the outer seed coat of a legume, especially yellow or green field peas, to dissolve only water-soluble protein and sugar products, filtering the slurry and drying the solid product thus obtained to provide a novel fibrous natural product. The latter is useful as an additive for edible food products such as bread, muffins and pasta to increase the fibrous content thereof.

Inventors

  • 👤 Gary B. Nickel
  • 👤 George D. Richardson

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 09:04
CPC Classifications
A; A21; A21D; A21D13/00; A21D13/02; A23; A23L; A23L11/00; A23L11/05; A23L33/00; A23L33/20; A23L33/21

Claims Analysis

Total Claims: 45
Claim 1
Independent Claim 99 words
A process for the preparation of a novel improved fibrous natural product which comprises agitating an aqueous slurry of ground solid material from the outer seed coat of a legume for only a period of time required to dissolve water-soluble proteins and sugars present in the solid material while retaining in the solid material pectins or gums present in the solid material, filtering said slurry to remove solid product containing said pectins or gums from said slurry, and drying the solid product containing said pectins or gums to provide a novel fibrous natural product containing said pectins or gums.
Claim 2
Dependent Claim 99 words
A process for the preparation of a novel improved fibrous natural product which comprises agitating an aqueous slurry of ground solid material from the outer seed coat of a legume for only a period of time required to dissolve water-soluble proteins and sugars present in the solid material while retaining in the solid material pectins or gums present in the solid material, filtering said slurry to remove solid product containing said pectins or gums from said slurry, and drying the solid product containing said pectins or gums to provide a novel fibrous natural product containing said pectins or gums.
Claim 3
Dependent Claim 107 words
A process for the preparation of a novel improved fibrous natural product which comprises grinding solid material from the outer seed coat of a legume to a requisite particle size, forming an aqueous slurry of the ground material and agitating said slurry for only a period of time required to dissolve water-soluble proteins and sugars present in the solid material while retaining pectins or gums present in the solid material, filtering said slurry to remove solid product containing said pectins or gums from said slurry, and drying the solid product containing said pectins or gums to provide a novel fibrous natural product containing said pectins or gums.
Claim 4
Dependent Claim 107 words
A process for the preparation of a novel improved fibrous natural product which comprises grinding solid material from the outer seed coat of a legume to a requisite particle size, forming an aqueous slurry of the ground material and agitating said slurry for only a period of time required to dissolve water-soluble proteins and sugars present in the solid material while retaining pectins or gums present in the solid material, filtering said slurry to remove solid product containing said pectins or gums from said slurry, and drying the solid product containing said pectins or gums to provide a novel fibrous natural product containing said pectins or gums.
Claim 5
Dependent Claim 160 words
A process for the preparation of a novel improved fibrous natural product which comprises agitating an aqueous slurry of ground material from the outer seed coat of a legume for only a period of time required to dissolve water-soluble proteins and sugars present in the solid material while retaining in the solid material pectins or gums present in the solid material, filtering said slurry to remove solid material containing said pectins or gums from said slurry, suspending the solid material containing said pectins or gums in water to form a second aqueous slurry and treating said second slurry with an oxidizing or bleaching agent to oxidize or bleach the solid material while retaining in the solid material said pectins or gums, filtering said second slurry to remove solid product containing said pectins or gums from said second slurry, and drying the solid product containing said pectins or gums to provide a novel fibrous natural product containing said pectins or gums.
Claim 6
Dependent Claim 160 words
A process for the preparation of a novel improved fibrous natural product which comprises agitating an aqueous slurry of ground material from the outer seed coat of a legume for only a period of time required to dissolve water-soluble proteins and sugars present in the solid material while retaining in the solid material pectins or gums present in the solid material, filtering said slurry to remove solid material containing said pectins or gums from said slurry, suspending the solid material containing said pectins or gums in water to form a second aqueous slurry and treating said second slurry with an oxidizing or bleaching agent to oxidize or bleach the solid material while retaining in the solid material said pectins or gums, filtering said second slurry to remove solid product containing said pectins or gums from said second slurry, and drying the solid product containing said pectins or gums to provide a novel fibrous natural product containing said pectins or gums.
Claim 7
Dependent Claim 19 words
The process of claim 1, wherein the outer seed coat material is obtained from yellow or green field peas.
Claim 8
Dependent Claim 20 words
The process of claim 1, wherein the legume hull material is obtained from white beans, navy beans or soya beans.
Claim 9
Dependent Claim 33 words
The process of claim 1, wherein the outer seed coat material has a particle size which passes through a 30 to 60 mesh screen but does not pass through a 150 mesh screen.
Claim 10
Dependent Claim 31 words
The process of claim 1, wherein the outer seed coat material has a particle size which passes through a 40 mesh screen but does not pass through a 150 mesh screen.
Claim 11
Dependent Claim 31 words
The process of claim 1, wherein the outer seed coat material has a particle size which passes through a 60 mesh screen but does not pass through an 80 mesh screen.
Claim 12
Dependent Claim 19 words
The process of claim 1, wherein the slurry contains from about 2% to about 20% by weight of solid.
Claim 13
Dependent Claim 19 words
The process of claim 1, wherein the slurry contains from about 2% to about 10% by weight of solid.
Claim 14
Dependent Claim 15 words
The process of claim 1, wherein the slurry contains about 5% by weight of solid.
Claim 15
Dependent Claim 22 words
The process of claim 1, wherein the slurry is agitated at a temperature of from about 5° C. to about 40° C.
Claim 16
Dependent Claim 22 words
The process of claim 1, wherein the slurry is agitated at a temperature of from about 15° C. to about 25° C.
Claim 17
Dependent Claim 17 words
The process of claim 1, wherein the slurry is agitated at a temperature of about 20° C.
Claim 18
Dependent Claim 22 words
The process of claim 1, wherein the slurry is agitated for a period of from about 2 minutes to about 10 minutes.
Claim 19
Dependent Claim 22 words
The process of claim 1, wherein the slurry is agitated for a period of from about 6 minutes to about 8 minutes.
Claim 20
Dependent Claim 29 words
The process of claim 1, wherein the slurry is agitated at a temperature of about 20° C. for a period of from about 6 minutes to about 8 minutes.
Claim 21
Dependent Claim 20 words
The process of claim 1, wherein the slurry is maintained at a pH of from about 6.0 to about 6.5.
Claim 22
Dependent Claim 29 words
The process of claim 1, wherein the slurry is maintained at a pH of from about 6.0 to about 6.5 by the addition of citric acid or phosphoric acid.
Claim 23
Dependent Claim 20 words
The process of claim 3 wherein the second slurry contains from about 5% to about 20% by weight of solid.
Claim 24
Dependent Claim 16 words
The process of claim 3 wherein the second slurry contains about 10% by weight of solid.
Claim 25
Dependent Claim 25 words
The process of claim 3, wherein the oxidizing or bleaching agent is an alkali metal hypochlorite, an alkali metal sulphite or an alkali metal bisulphite.
Claim 26
Dependent Claim 19 words
The process of claim 3, wherein the oxidizing or bleaching agent is sodium hypochlorite, sodium sulphite or sodium bisulphite.
Claim 27
Dependent Claim 14 words
The process of claim 3, wherein the oxidizing or bleaching agent is sulphur dioxide.
Claim 28
Dependent Claim 14 words
The process of claim 3, wherein the oxidizing or bleaching agent is hydrogen peroxide.
Claim 29
Dependent Claim 28 words
The process of claim 3, wherein the oxidizing or bleaching agent is used at a concentration of from about 100 parts to about 200 parts per million (ppm).
Claim 30
Dependent Claim 20 words
The process of claim 3, wherein the oxidizing or bleaching agent is used at a concentration of about 100 ppm.
Claim 31
Dependent Claim 24 words
The process of claim 3, wherein the oxidizing or bleaching agent is hydrogen peroxide which is used at a concentration of about 100 ppm.
Claim 32
Dependent Claim 25 words
The process of claim 3, wherein the oxidizing or bleaching is carried out at a temperature of from about 15° C. to about 30° C.
Claim 33
Dependent Claim 25 words
The process of claim 3, wherein the oxidizing or bleaching is carried out at a temperature of from about 20° C. to about 25° C.
Claim 34
Dependent Claim 27 words
The process of claim 3, wherein the oxidizing or bleaching is carried out at a temperature of about 25° C. for a period of about 5 minutes.
Claim 35
Dependent Claim 21 words
The process of claim 1, wherein the fibrous natural product is dried by means of a flash type (forced air) drier.
Claim 36
Dependent Claim 37 words
The process of claim 1, wherein the fibrous natural product is ground to a powder having a particle size which passes through a 30 to 50 mesh screen but does not pass through a 150 mesh screen.
Claim 37
Dependent Claim 26 words
The process of claim 1, wherein the fibrous natural product is ground to a powder having a particle size which passes through an 80 mesh screen.
Claim 38
Dependent Claim 139 words
A process for the preparation of a novel improved fibrous natural product which comprises grinding material from the outer seed coat of a legume to a particle size which passes through a 20 mesh screen but does not pass through a 60 mesh screen, forming a 5% w/w aqueous slurry of the ground material and agitating said slurry at a temperature of about 20° C. for a period of from about 6 to about 8 minutes to dissolve water-soluble products, filtering said slurry through a 325 mesh screen, suspending the solid material in water to form a 10% w/w second slurry, treating said second slurry with 100 ppm of hydrogen peroxide at a temperature of about 25° C. for a period of about 5 minutes, filtering said second slurry and drying the solid product to provide a fibrous product.
Claim 39
Dependent Claim 139 words
A process for the preparation of a novel improved fibrous natural product which comprises grinding material from the outer seed coat of a legume to a particle size which passes through a 20 mesh screen but does not pass through a 60 mesh screen, forming a 5% w/w aqueous slurry of the ground material and agitating said slurry at a temperature of about 20° C. for a period of from about 6 to about 8 minutes to dissolve water-soluble products, filtering said slurry through a 325 mesh screen, suspending the solid material in water to form a 10% w/w second slurry, treating said second slurry with 100 ppm of hydrogen peroxide at a temperature of about 25° C. for a period of about 5 minutes, filtering said second slurry and drying the solid product to provide a fibrous product.
Claim 40
Dependent Claim 14 words
The process of claim 35 wherein the legume is yellow or green field peas.
Claim 41
Dependent Claim 25 words
The process of claim 35 wherein the fibrous product is ground to a powder having a particle size which passes through an 80 mesh screen.
Claim 42
Dependent Claim 13 words
A novel fibrous natural product, when prepared by the process of claim 1.
Claim 43
Dependent Claim 13 words
A novel fibrous natural product, when prepared by the process of claim 3.
Claim 44
Dependent Claim 110 words
A process for the preparation of a fibrous product which comprises grinding material from the outer seed coat of a legume to a particle size which passes through a 20 mesh screen but does not pass through a 150 mesh screen, forming an aqueous slurry of the ground material and agitating said slurry at a temperature of about 5°-40° C. for a period of from about 2 to about 10 minutes to dissolve water-soluble proteins and sugars present in the material while retaining pectins or gums present in the material, filtering said slurry to remove solid product from said slurry, and drying the solid product to provide a fibrous product.
Claim 45
Dependent Claim 110 words
A process for the preparation of a fibrous product which comprises grinding material from the outer seed coat of a legume to a particle size which passes through a 20 mesh screen but does not pass through a 150 mesh screen, forming an aqueous slurry of the ground material and agitating said slurry at a temperature of about 5°-40° C. for a period of from about 2 to about 10 minutes to dissolve water-soluble proteins and sugars present in the material while retaining pectins or gums present in the material, filtering said slurry to remove solid product from said slurry, and drying the solid product to provide a fibrous product.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1991-09-27 1992-03-28 1992-09-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1995-09-27 1996-03-28 1996-09-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1999-09-27 2000-03-28 2000-09-27 $7700.00 Window Closed / Lapsed

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