US4749667A
Expired / Lapsed
US
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Alumina - zirconia ceramics reinforced with silicon carbide whiskers and methods of making the same
Assignee: Carboloy Inc
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Filing: 1987-02-03
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Granted: 1988-06-07
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Expires: 2007-02-03
Abstract
Abstract Disclosed is a 35 to 45 volume percent silicon carbide whisker reinforced ceramic composite containing alumina and from about 5 to 21 volume percent zirconia which is used to make hard cutting tools having excellent toughness and hardness. Also disclosed are methods of producing the same.
Inventors
- 👤 Choll K. Jun
- 👤 Edward L. Exner
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 19:24
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/01; C04B35/10; C04B35/111; C04B35/117; C04B35/119; C04B35/622; C04B35/64; C04B35/645; C04B35/71; C04B35/78; C04B35/80
Claims Analysis
Total Claims: 22
Claim 1
Independent Claim
49 words
A silicon carbide reinforced ceramic composite comprising a matrix of alumina with at least about 5 volume percent zirconia in the monoclinic or tetragonal phase in an effective amount sufficient to increase hardness and fracture toughness and from about 35 to about 45 volume percent of silicon carbide whiskers.
Claim 2
Dependent Claim
49 words
A silicon carbide reinforced ceramic composite comprising a matrix of alumina with at least about 5 volume percent zirconia in the monoclinic or tetragonal phase in an effective amount sufficient to increase hardness and fracture toughness and from about 35 to about 45 volume percent of silicon carbide whiskers.
Claim 3
Dependent Claim
19 words
The composite of claim 1 wherein the amount of zirconia is from about 5 to about 21 volume percent.
Claim 4
Dependent Claim
19 words
The composite of claim 2 wherein the amount of zirconia is from about 8 to about 17 volume percent.
Claim 5
Dependent Claim
21 words
The composite of claim 1 wherein the amount of silicon carbide whiskers is from about 35 to about 40 volume percent.
Claim 6
Dependent Claim
21 words
The composite of claim 2 wherein the amount of silicon carbide whiskers is from about 35 to about 40 volume percent.
Claim 7
Dependent Claim
21 words
The composite of claim 3 wherein the amount of silicon carbide whiskers is from about 35 to about 40 volume percent.
Claim 8
Dependent Claim
31 words
The composite of claim 1 wherein the diameter of silicon carbide whiskers is from about 0.3 to about 2.0 μm and the length is from about 2 to about 40 μm.
Claim 9
Dependent Claim
21 words
The composite of claim 7 wherein the length of the silicon carbide whiskers is from about 5 to about 25 μm.
Claim 10
Dependent Claim
71 words
A silicon carbide whisker reinforced ceramic composite comprising a matrix of alumina with zirconia in a monoclinic or a tetragonal phase in an amount of about 8 to about 17 volume percent and from about 35 to about 45 volume percent of silicon carbide whiskers, said silicon carbide whiskers having a diameter of from about 0.3 to about 2.0 μm and a length of from about 2 to about 40 μm.
Claim 11
Dependent Claim
71 words
A silicon carbide whisker reinforced ceramic composite comprising a matrix of alumina with zirconia in a monoclinic or a tetragonal phase in an amount of about 8 to about 17 volume percent and from about 35 to about 45 volume percent of silicon carbide whiskers, said silicon carbide whiskers having a diameter of from about 0.3 to about 2.0 μm and a length of from about 2 to about 40 μm.
Claim 12
Dependent Claim
21 words
The composite of claim 9 wherein the amount of silicon carbide whiskers is from about 35 to about 40 volume percent.
Claim 13
Independent Claim
69 words
A method of forming a ceramic composite having excellent fracture toughness and hardness comprising combining alumina, from about 5 to 21 volume percent of monoclinic or tetragonal phase zirconia and from about 35 to 40 volume percent of silicon carbide whiskers to form a mixture, hot pressing said mixture at a temperature of from about 1700° to about 1800° C. at a pressure from about at least 2,000 psi.
Claim 14
Independent Claim
69 words
A method of forming a ceramic composite having excellent fracture toughness and hardness comprising combining alumina, from about 5 to 21 volume percent of monoclinic or tetragonal phase zirconia and from about 35 to 40 volume percent of silicon carbide whiskers to form a mixture, hot pressing said mixture at a temperature of from about 1700° to about 1800° C. at a pressure from about at least 2,000 psi.
Claim 15
Dependent Claim
15 words
The method of claim 11 wherein the pressure is from about 2,500 to 4,000 psi.
Claim 16
Dependent Claim
19 words
The method of claim 12 wherein the temperature is about 1750° C. and the pressure is about 3,000 psi.
Claim 17
Dependent Claim
19 words
The method of claim 11 wherein the amount of zirconia is from about 8 to about 17 volume percent.
Claim 18
Dependent Claim
21 words
The method of claim 14 wherein the amount of silicon carbide whisker is from about 35 to about 40 volume percent.
Claim 19
Dependent Claim
32 words
The method of claim 11 wherein the diameter of the silicon carbide whiskers is from about 0.3 to about 2.0 μm and the length is from about 2 to about 40 μm.
Claim 20
Dependent Claim
21 words
The method of claim 16 wherein the length of the silicon carbide whiskers is from about 5 to about 25 μm.
Claim 21
Dependent Claim
42 words
The method of claim 11 wherein the amount of zirconia is from about 8 to 17 volume percent, said silicon carbide whiskers having a diameter of from about 0.3 to 2.0 μm and a length of from about 2 to 40 μm.
Claim 22
Dependent Claim
20 words
The method of claim 18 wherein the amount of silicon carbide whiskers is from about 35 to 40 volume percent.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1991-06-07 | 1991-12-07 | 1992-06-07 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1995-06-07 | 1995-12-07 | 1996-06-07 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1999-06-07 | 1999-12-07 | 2000-06-07 | $7700.00 | Window Closed / Lapsed |