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US4626406A Expired / Lapsed US ⏱️ 0.0 years remaining

Activated sintering of metallic powders

Assignee: Huntington Alloys Corp
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Filing: 1985-10-28
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Granted: 1986-12-02
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Expires: 2005-10-28
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Abstract

Abstract A method for consolidating powder utilizing slurry extrusion or rolling techniques. A metallic powder, binder and boron containing activator are mixed together to form a slurry. The slurry is introduced into an active forming apparatus whereupon it is formed into an object of predetermined shape and sintered.

Inventors

  • 👤 Jon M. Poole

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 15:08
CPC Classifications
B; B22; B22F; B22F3/00; B22F3/22; B22F3/227; B22F3/10; B22F3/1003; C; C22; C22C; C22C1/00; C22C1/04; C22C1/0433; B22F2998/00

Claims Analysis

Total Claims: 21
Claim 1
Independent Claim 59 words
A method for consolidating a product from metallic powder, the method comprising: (a) blending the powder with a binder and a boron containing activator to form a slurry, (b) introducing the slurry into an active forming apparatus to cause the formation of an object of predetermined shape, (c) removing the binder from the object, and (d) sintering the object.
Claim 2
Independent Claim 59 words
A method for consolidating a product from metallic powder, the method comprising: (a) blending the powder with a binder and a boron containing activator to form a slurry, (b) introducing the slurry into an active forming apparatus to cause the formation of an object of predetermined shape, (c) removing the binder from the object, and (d) sintering the object.
Claim 3
Dependent Claim 25 words
The method according to claim 1 wherein the activator is selected from the group consisting of dilute boric acid-water solution, nickel boride and lithium tetraborate.
Claim 4
Dependent Claim 15 words
The method according to claim 2 wherein the nickel boride is -80 mesh and smaller.
Claim 5
Dependent Claim 11 words
The method according to claim 1 wherein the slurry is extruded.
Claim 6
Dependent Claim 12 words
The method according to claim 1 where the slurry is cold rolled.
Claim 7
Dependent Claim 21 words
The method according to claim 1 wherein the sintering temperature is 85% of the melting point of the alloy or greater.
Claim 8
Dependent Claim 21 words
The method according to claim 1 wherein the density of the object is in excess of 5 grams per cubic centimeter.
Claim 9
Dependent Claim 23 words
The method according to claim 2 wherein up to about 5% boric acid-water solution is used as the activator for water atomized powder.
Claim 10
Dependent Claim 24 words
The method according to claim 2 wherein up to about a 1% boric acid-water solution is used as the activator for gas atomized powder.
Claim 11
Dependent Claim 24 words
The method according to claim 2 wherein up to about a 1% boric acid-water solution is used as the activator for water atomized powder.
Claim 12
Dependent Claim 20 words
The method according to claim 1 wherein the activator content ranges up to about 1.2% by weight of the powder.
Claim 13
Dependent Claim 23 words
The method according to claim 1 wherein additional nickel powder is added to the metallic powder prior to the formation of the slurry.
Claim 14
Dependent Claim 11 words
The method according to claim 1 wherein the powder is atomized.
Claim 15
Dependent Claim 11 words
The method according claim 1 wherein the metal powder includes nickel.
Claim 16
Dependent Claim 13 words
The method according to claim 1 wherein the activator is a metal borate.
Claim 17
Dependent Claim 16 words
The method according to claim 1 wherein the density of the object is 90% or greater.
Claim 18
Dependent Claim 21 words
The method according to claim 1 where the binder content ranges from about 1 to 4% by weight of the powder.
Claim 19
Dependent Claim 12 words
The method according the claim 1 where the binder is water soluble.
Claim 20
Dependent Claim 14 words
The method according to claim 1 where water is added to form the slurry.
Claim 21
Dependent Claim 21 words
The method according to claim 19 wherein the water content ranges from about 5 to 20% by weight of the powder.

References Cited (Backward Citations)

US4011291A Cited
US4259112A Cited
US4298383A Cited
US4546047A Cited
US4562040A Cited
US4554130A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-12-01 1990-06-02 1990-12-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-12-01 1994-06-02 1994-12-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-12-01 1998-06-02 1998-12-02 $7700.00 Window Closed / Lapsed

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