Patent US4564378A successfully refreshed from Google Patents.
US4564378A
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Method for producing a preform for light waveguides
Assignee: Licentia Patent Verwaltungs GmbH
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Filing: 1984-02-09
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Granted: 1986-01-14
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Expires: 2004-02-09
Abstract
Abstract A method of producing a preform for light waveguides wherein glass-forming chlorides, e.g. SiCl 4 and/or GeCl 4 , are reacted with water vapor to form a glass forming layer, e.g. SiO 2 soot. This reaction advantageously takes place at relatively low temperatures, e.g. 20° C.-800° C. Surprisingly, almost no SiO 2 deposition takes place on higher heated surfaces, e.g. in the reaction chamber. Elimination of annoying OH - ions is possible.
Inventors
- 👤 Max Kuisl
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 08:47
CPC Classifications
C; C03; C03B; C03B37/00; C03B37/01; C03B37/012; C03B37/014; C03B37/018; C03B37/01807; C03B37/01413; C03B2207/00; C03B2207/30; C03B2207/34
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
141 words
In a method of producing a glasy preform for a light waveguide including depositing a glass forming layer on a tubular substrate disposed in a reaction chamber, and subsequently subjecting said glass forming layer to a heating process to convert said glass forming layer to a glassy layer; the improvement wherein said step of depositing comprises: providing a gaseous mixture of silicon tetrachloride (SiCl 4 ) gas and water vapor; cooling and maintaining said substrate at a temperature between 20° C. and 800° C. while heating said reaction chamber to a temperature of substantially greater than 800° C.; and flowing a stream of said gaseous mixture through the reaction chamber to react said silicon tetrachloride gas with said water vapor to precipitate a glass forming layer of silicon dioxide particles from the reacted gas and water vapor on the cooled substrate.
Claim 2
Dependent Claim
141 words
In a method of producing a glasy preform for a light waveguide including depositing a glass forming layer on a tubular substrate disposed in a reaction chamber, and subsequently subjecting said glass forming layer to a heating process to convert said glass forming layer to a glassy layer; the improvement wherein said step of depositing comprises: providing a gaseous mixture of silicon tetrachloride (SiCl 4 ) gas and water vapor; cooling and maintaining said substrate at a temperature between 20° C. and 800° C. while heating said reaction chamber to a temperature of substantially greater than 800° C.; and flowing a stream of said gaseous mixture through the reaction chamber to react said silicon tetrachloride gas with said water vapor to precipitate a glass forming layer of silicon dioxide particles from the reacted gas and water vapor on the cooled substrate.
Claim 3
Dependent Claim
19 words
A method as defined in claim 1 wherein said temperature of the substrate is maintained at approximately 20° C.
Claim 4
Dependent Claim
20 words
A method as defined in claim 1 wherein the reaction chamber is heated to a temperature of approximately 1000° C.
Claim 5
Dependent Claim
18 words
A method as defined in claim 1 wherein said mixture additionally contains germanium tetrachloride (GeCl 4 ) gas.
Claim 6
Dependent Claim
37 words
A method as defined in claim 1 wherein said glass-forming layer is precipitated on the exterior surface of the tubular substrate; and said step of cooling includes conducting a coolant through the interior of the tubular substrate.
Claim 7
Dependent Claim
17 words
A method as defined in claim 5 wherein the substrate contains graphite and the coolant is water.
Claim 8
Dependent Claim
28 words
A method as defined in claim 1 wherein said heating process is effected in a gas or vapor atmosphere which prevents development of hydroxyl (OH - ) ions.
Claim 9
Dependent Claim
35 words
A method as defined in claim 1 wherein the mixture further contains oxygen gas which reacts with the HCl gas produced in the reaction chamber to produce chlorine gas which acts as a dehydrating component.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1989-01-13 | 1989-07-15 | 1990-01-14 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1993-01-13 | 1993-07-15 | 1994-01-14 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1997-01-13 | 1997-07-15 | 1998-01-14 | $7700.00 | Window Closed / Lapsed |