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US4504601A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing pre-foamed particles of polypropylene resin

Assignee: JAPAN STYRENE PAPER Corp A CORP OF JAPAN
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Filing: 1983-09-29
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Granted: 1985-03-12
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Expires: 2003-09-29
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Abstract

Abstract A process for producing pre-foamed particles of a polypropylene resin which comprises expanding original pre-foamed particles of a polypropylene resin, said original pre-foamed particles having the following relation 2<E1/3xn1/2<45 wherein E is the expansion ratio of the original pre-foamed particles, and n is the number of cells per mm2 of the cross section of the original pre-foamed particles, by (1) imparting expanding ability to the original pre-foamed particles and then heating them with a heated gas to the heat distortion temperature of the base resin of the pre-foamed particles or a higher temperature or (2) heating the original pre-foamed particles with steam to the heat distortion temperature of the base resin of the particles or a higher temperature with or without imparting expanding ability thereto, whereby pre-foamed particles having an expansion ratio higher than the original expansion ratio E are obtained.

Inventors

  • 👤 Hideki Kuwabara
  • 👤 Shohei Yoshimura
  • 👤 Toru Yamaguchi
  • 👤 Yoshimi Sudo

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 07:25
CPC Classifications
B; B29; B29C; B29C44/00; B29C44/34; B29C44/3442; B29C44/3446; B29C44/3453; B29C44/3461; C; C08; C08J; C08J9/00; C08J9/22; C08J9/228; C08J9/232; C08J2323/00; C08J2323/02; C08J2323/10; Y; Y10; Y10S; Y10S264/00; Y10S264/09

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 257 words
A process for producing pre-foamed particles of a polypropylene resin which comprises expanding original pre-foamed particles of a polypropylene resin, said original pre-foamed particles having the following relation 2<E.sup.1/3 ×n.sup.1/2 <45 wherein E is the expansion ratio of the original pre-foamed particles, and n is the number of cells per mm 2 of the cross section of the original pre-foamed particles, by (1) including an inorganic gas, a volatile blowing agent, or a mixture of these into the original pre-foamed particles so that the internal pressure reaches 1.5 to 10 kg/cm 2 (abs), and expanding ability is imparted to the original pre-foamed particles and then heating them with a heated gas to a temperature of from the heat distortion temperature of the base resin of the pre-foamed particles, which is from 80° to 130° C., to a temperature 15° C. higher than the melting point of the base resin of the pre-foamed particles of (2) heating the original pre-foamed particles with steam to a temperature of from the heat distortion temperature of the base resin of the particles which is from 80° to 130° C. to a temperature 15° C. higher than the melting point of the base resin of the pre-foamed particles with or without imparting expanding ability thereto by including an inorganic gas, a volatile blowing agent, or a mixture of these into the original pre-foamed particles so that the internal pressure reaches 1.5 to 10 kg/cm 2 (abs), whereby pre-foamed particles having an expansion ratio higher than the original expansion ratio E are obtained.
Claim 2
Dependent Claim 257 words
A process for producing pre-foamed particles of a polypropylene resin which comprises expanding original pre-foamed particles of a polypropylene resin, said original pre-foamed particles having the following relation 2<E.sup.1/3 ×n.sup.1/2 <45 wherein E is the expansion ratio of the original pre-foamed particles, and n is the number of cells per mm 2 of the cross section of the original pre-foamed particles, by (1) including an inorganic gas, a volatile blowing agent, or a mixture of these into the original pre-foamed particles so that the internal pressure reaches 1.5 to 10 kg/cm 2 (abs), and expanding ability is imparted to the original pre-foamed particles and then heating them with a heated gas to a temperature of from the heat distortion temperature of the base resin of the pre-foamed particles, which is from 80° to 130° C., to a temperature 15° C. higher than the melting point of the base resin of the pre-foamed particles of (2) heating the original pre-foamed particles with steam to a temperature of from the heat distortion temperature of the base resin of the particles which is from 80° to 130° C. to a temperature 15° C. higher than the melting point of the base resin of the pre-foamed particles with or without imparting expanding ability thereto by including an inorganic gas, a volatile blowing agent, or a mixture of these into the original pre-foamed particles so that the internal pressure reaches 1.5 to 10 kg/cm 2 (abs), whereby pre-foamed particles having an expansion ratio higher than the original expansion ratio E are obtained.
Claim 3
Dependent Claim 27 words
The process of claim 1 wherein the polypropylene resin is a homopolymer of propylene, an ethylene-propylene random copolymer, and ethylene-propylene block copolymer, or a mixture of these.
Claim 4
Dependent Claim 23 words
The process of claim 1 wherein the gas is air, nitrogen, argon, helium, carbon dioxide, dichlorodifluoromethane, trichlorofluoromethane, dichlorotetrafluoroethane or a mixture of these.
Claim 5
Dependent Claim 10 words
The process of claim 3 wherein the gas is air.
Claim 6
Dependent Claim 26 words
The process of claim 1 wherein the operation 2 is carried out and the stream has a pressure of 0.5 to 3 kg cm 2 (G).
Claim 7
Dependent Claim 16 words
The process of claim 1 wherein the operation (1) or (2) is repeated at least twice.
Claim 8
Dependent Claim 19 words
The process of claim 5 which includes the step of imparting the expanding ability to the original pre-foamed particles.
Claim 9
Dependent Claim 22 words
The process of claim 5 wherein the time of heating the original pre-foamed particles with steam is not more than 1 minute.
Claim 10
Dependent Claim 12 words
The process of claim 1 wherein the operation (1) is carried out.

References Cited (Backward Citations)

US3823213A Cited
US3743611A Cited
US3709806A Cited
US3770663A Cited
US4168353A Cited
US4303756A Cited
US4399087A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1988-03-11 1988-09-10 1989-03-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1992-03-11 1992-09-10 1993-03-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1996-03-11 1996-09-10 1997-03-12 $7700.00 Window Closed / Lapsed

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