Patent US4468257A successfully refreshed from Google Patents.
US4468257A
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Washing and removal method of high molecular substances
Assignee: Mitsui Chemicals Inc
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Filing: 1982-06-18
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Granted: 1984-08-28
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Expires: 2002-06-18
Abstract
Abstract Method of adding water and a hydroxide of an alkali metal or alkaline earth metal to a washing solvent such as an alkylamide and/or alkylsulfoxide when washing and removing high molecular substances stuck on the interior of a production apparatus or molding machine for an aromatic vinyl-acrylonitrile copolymer. A method for regenerating and recovering the washing solvent used for the above-mentioned washing and removal by means of an evaporator and distillation tower.
Inventors
- 👤 Masahiro Kaneko
- 👤 Tadashi Asanuma
- 👤 Nobutaka Uchikawa
- 👤 Ichiro Fujio
- 👤 Tetsunosuke Shiomura
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 08:35
CPC Classifications
C; C08; C08J; C08J11/00; C08J11/02; B; B01; B01J; B01J19/00; B01J19/0053; C11; C11D; C11D7/00; C11D7/02; C11D7/04; C11D7/06; C11D7/50; C11D7/5004; C11D7/5009; C11D7/5013; B01J2219/00; B01J2219/00049; B01J2219/00051; B01J2219/00074; B01J2219/00087; B01J2219/00094; B01J2219/00105; B01J2219/0011; C11D7/22; C11D7/32; C11D7/34; Y; Y10; Y10S; Y10S422/00; Y10S422/901
Claims Analysis
Total Claims: 3
Claim 1
Independent Claim
146 words
Method for washing and removing high molecular substances stuck on the interior of a production apparatus upon producing an aromatic vinyl-acrylonitrile copolymer containing 5 to 33 weight percent acrylonitrile, comprising washing and removing said stuck high molecular substances from the interior of said production apparatus by using one or more solvents selected from the group consisting of an alkylamide and an alkylsulfoxide, which method comprises using, together with said one or more solvents, a mixture containing from 1.0×10 -4 to 1.0 gram equivalent of at least one hydroxide having the formula: M(OH).sub.n (I) wherein n is an integer of 1 or 2, and M is an alkali metal when n is 1 or an alkaline earth metal when n is 2, per liter of said one or more solvents, and 0.03 to 3.0 weight percent of water based on the amount of one or more solvents.
Claim 2
Dependent Claim
146 words
Method for washing and removing high molecular substances stuck on the interior of a production apparatus upon producing an aromatic vinyl-acrylonitrile copolymer containing 5 to 33 weight percent acrylonitrile, comprising washing and removing said stuck high molecular substances from the interior of said production apparatus by using one or more solvents selected from the group consisting of an alkylamide and an alkylsulfoxide, which method comprises using, together with said one or more solvents, a mixture containing from 1.0×10 -4 to 1.0 gram equivalent of at least one hydroxide having the formula: M(OH).sub.n (I) wherein n is an integer of 1 or 2, and M is an alkali metal when n is 1 or an alkaline earth metal when n is 2, per liter of said one or more solvents, and 0.03 to 3.0 weight percent of water based on the amount of one or more solvents.
Claim 3
Dependent Claim
32 words
Method as claimed in claim 1 wherein said at least one hydroxide is selected from the group consisting of lithium hydroxide, sodium hydroxide, potassium hydroxide, cesium hydroxide, calcium hydroxide and barium hydroxide.
References Cited (Backward Citations)
US2678304A
Cited
US3476656A
Cited
US3997360A
Cited
US3998655A
Cited
US4043874A
Cited
JPS558087A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-08-28 | 1988-02-27 | 1988-08-28 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-08-28 | 1992-02-27 | 1992-08-28 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-08-28 | 1996-02-27 | 1996-08-28 | $7700.00 | Window Closed / Lapsed |