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Apparatus and method for measuring optically active materials

Assignee: American Crystal Sugar Co
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Filing: 1982-02-25
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Granted: 1984-08-21
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Expires: 2002-02-25
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Abstract

Abstract A polarimeter system and method for sensing optical rotation caused by otically active materials in a solution are disclosed. The polarimeter system (10) includes a light source (11) for emitting infrared light, a polarizer (14) operatively connected to intercept the infrared light to produce a polarized beam therefrom and means for directing the beam through a sample of optically active material (15), which rotates the light beam. A beam splitting prism (16) splits the rotated polarized beam into its horizontal and vertical components. Infrared light detectors (17a) and (17b) convert the horizontal and vertical components into electrical signals representative of the optical rotation caused by the sample solution. Shaping circuitry (26) conditions the electrical signals for use by analog or digital (28) networks, that present the optical rotation or its physical correlative factor. Feedback circuitry (36) may be used to vary the light source (11) intensity in response to the detected light signals.

Inventors

  • 👤 James O. Kysilka
  • 👤 Charles A. Sawicki

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 22:00
CPC Classifications
H; H03; H03F; H03F3/00; H03F3/181; H03F3/183; H03F3/187; G; G01; G01J; G01J4/00; G01J4/04; G01N; G01N21/00; G01N21/17; G01N21/25; G01N21/31; G01N21/35; G01N21/3577; G01J1/00; G01J1/10; G01J1/20; G01J1/28; G01J1/30; G01N21/21

Claims Analysis

Total Claims: 25
Claim 1
Independent Claim 132 words
A polarimeter system for sensing optical rotation caused by optically active material in a dark sugar solution, said polarimeter system comprising: (a) means for containing a liquid sample of optically active material in the dark sugar solution; (b) an infrared light source for emitting infrared light; (c) polarizer means operatively connected to intercept at least a portion of said infrared light for producing a polarized light beam therefrom; (d) means for directing said polarized light beam through at least a portion of said liquid sample; and (e) infrared light detection means operatively connected to intercept said light beam after passing through said liquid sample, for producing a signal in response to the rotational condition of said polarized light beam, whereby the optical rotation caused by the dark sugar solution may be determined.
Claim 2
Dependent Claim 132 words
A polarimeter system for sensing optical rotation caused by optically active material in a dark sugar solution, said polarimeter system comprising: (a) means for containing a liquid sample of optically active material in the dark sugar solution; (b) an infrared light source for emitting infrared light; (c) polarizer means operatively connected to intercept at least a portion of said infrared light for producing a polarized light beam therefrom; (d) means for directing said polarized light beam through at least a portion of said liquid sample; and (e) infrared light detection means operatively connected to intercept said light beam after passing through said liquid sample, for producing a signal in response to the rotational condition of said polarized light beam, whereby the optical rotation caused by the dark sugar solution may be determined.
Claim 3
Dependent Claim 25 words
The polarimeter system of claim 1, wherein the light emitted from said infrared light source has a wavelength equal to or greater than 700 nanometers.
Claim 4
Dependent Claim 25 words
The polarimeter system of claim 1, wherein the light emitted from said infrared light source has a wavelength equal to or greater than 875 nanometers.
Claim 5
Dependent Claim 16 words
The polarimeter system of claim 1, wherein said infrared light souce comprises an infrared laser diode.
Claim 6
Dependent Claim 57 words
The polarimeter system of claim 1, wherein said detection means comprises: (a) means for splitting said polarized light beam after passing through said liquid sample into two components with orthogonal polarizations; (b) means for receiving and sensing said components; and (c) means for determining the ratio of one of said components to the other of said components.
Claim 7
Dependent Claim 36 words
The polarimeter system of claim 1, further comprising collimating optic means operatively connected between said light source and said containing means, for collimating at least a portion of said infrared light emitted by said light source.
Claim 8
Dependent Claim 46 words
The polarimeter system of claim 1, further comprising a band pass filter operatively connected between said light source and said polarizer means to intercept at least a portion of said infrared light, for passing, only a predetermined wavelength of said infrared light to said polarizing means.
Claim 9
Dependent Claim 33 words
The polarimeter system of claim 1, further comprising means for sensing the temperature of the optically active material and means for transmitting a signal responsive to the sensed temperature to said detection means.
Claim 10
Dependent Claim 29 words
The polarimeter system of claim 1, further comprising means for varying the intensity of said infrared light source in response to the light absorption property of said liquid sample.
Claim 11
Dependent Claim 214 words
A polarimeter system for sensing optical rotation caused by optically active material in a dark sugar solution, said polarimeter system comprising: (a) means for containing a liquid sample of optically active material in the dark sugar solution; (b) an infrared light source for emitting infrared light, the light emitted from said infrared light source having a wavelength equal to or greater that 700 nanometers; (c) polarizer means operatively connected to intercept at least a portion of said infrared light for polarizing said portion of said infrared light to produce a polarized beam of said light; (d) means for directing said polarized beam through at least a portion of said liquid sample; (e) collimating optics operatively connected to and positioned between said light source and said containing means; (f) a band pass filter operatively connected to and positioned between said light source and said polarizer means; (g) detection means operatively connected to intercept said beam passing through said liquid sample for producing a signal in response to the rotational condition of said polarized beam; and (h) means for varying the intensity of said infrared light source, in response to the amount of said polarized light beam being asorbed by said liquid sample, whereby the optical rotation caused by the dark sugar solution may be determined.
Claim 12
Dependent Claim 214 words
A polarimeter system for sensing optical rotation caused by optically active material in a dark sugar solution, said polarimeter system comprising: (a) means for containing a liquid sample of optically active material in the dark sugar solution; (b) an infrared light source for emitting infrared light, the light emitted from said infrared light source having a wavelength equal to or greater that 700 nanometers; (c) polarizer means operatively connected to intercept at least a portion of said infrared light for polarizing said portion of said infrared light to produce a polarized beam of said light; (d) means for directing said polarized beam through at least a portion of said liquid sample; (e) collimating optics operatively connected to and positioned between said light source and said containing means; (f) a band pass filter operatively connected to and positioned between said light source and said polarizer means; (g) detection means operatively connected to intercept said beam passing through said liquid sample for producing a signal in response to the rotational condition of said polarized beam; and (h) means for varying the intensity of said infrared light source, in response to the amount of said polarized light beam being asorbed by said liquid sample, whereby the optical rotation caused by the dark sugar solution may be determined.
Claim 13
Dependent Claim 184 words
A polarimeter system for sensing optical rotation caused by a dark sugar solution without the need to clarify the dark sugar solution, said polarimeter system comprising: (a) a sample container for holding a liquid sample of the dark sugar solution; (b) an infrared light source for emitting infrared light; (c) polarizer means operatively connected to intercept at least a portion of said infrared light for polarizing said portion of said infrared light to produce a polarized beam of said light; (d) collimating optics operatively connected to and positioned between said light source and said polarizing means, whereby said infrared light is collimated; (e) means for positioning said container in alignment with said infrared light source for intercepting said, polarized, collimated light beam wherein said polarized, collimated light beam passes through at least a portion of said sample container holding the dark sugar solution; and (f) detection means operatively connected to intercept said beam passing through said liquid sample, producing a signal in response to the rotational condition of said polarized beam, whereby the optical rotation caused by the dark sugar solution may be determined.
Claim 14
Dependent Claim 184 words
A polarimeter system for sensing optical rotation caused by a dark sugar solution without the need to clarify the dark sugar solution, said polarimeter system comprising: (a) a sample container for holding a liquid sample of the dark sugar solution; (b) an infrared light source for emitting infrared light; (c) polarizer means operatively connected to intercept at least a portion of said infrared light for polarizing said portion of said infrared light to produce a polarized beam of said light; (d) collimating optics operatively connected to and positioned between said light source and said polarizing means, whereby said infrared light is collimated; (e) means for positioning said container in alignment with said infrared light source for intercepting said, polarized, collimated light beam wherein said polarized, collimated light beam passes through at least a portion of said sample container holding the dark sugar solution; and (f) detection means operatively connected to intercept said beam passing through said liquid sample, producing a signal in response to the rotational condition of said polarized beam, whereby the optical rotation caused by the dark sugar solution may be determined.
Claim 15
Dependent Claim 25 words
The polarimeter system of claim 11, wherein the light emitted from said infrared light source has a wavelength equal to or greater than 700 nanometers.
Claim 16
Dependent Claim 60 words
The polarimeter system of claim 11, wherein said detection means comprises: (a) means for splitting said polarized beam after passing through said liquid sample into two components with orthogonal polarizations; (b) means for receiving and sensing said components and for producing sensed output signals in response thereto; and (c) means for conditioning said sensed signals for processing by electrical networks.
Claim 17
Dependent Claim 28 words
The polarimeter system of claim 13, wherein said conditioning means includes means for determining ratio of one of said orthogonal components to the other of said orthogonal components.
Claim 18
Dependent Claim 42 words
The polarimeter system of claim 11, further comprising a band pass filter operatively connected to and positioned between said light source and said polarizer means, whereby only a predetermined wavelength of said infrared light passes through said filter to said polarizer means.
Claim 19
Dependent Claim 29 words
The polarimeter system of claim 11, further comprising means for measuring the temperature of the optically active material and means for transmitting the temperature measurement to said detection means.
Claim 20
Independent Claim 82 words
A method for determining the optical rotation caused by optically active material in a liquid solution, such material in solution being characterized by being highly absorbent of visible light wavelengths, said method comprising: (a) polarizing light emitted from an infrared light source; (b) directing the polarized light through a sample of optically active material; and (c) detecting the polarized light after passing through the optically active material to determine the optical rotation caused by the optically active material in the liquid solution.
Claim 21
Independent Claim 82 words
A method for determining the optical rotation caused by optically active material in a liquid solution, such material in solution being characterized by being highly absorbent of visible light wavelengths, said method comprising: (a) polarizing light emitted from an infrared light source; (b) directing the polarized light through a sample of optically active material; and (c) detecting the polarized light after passing through the optically active material to determine the optical rotation caused by the optically active material in the liquid solution.
Claim 22
Independent Claim 88 words
A method for determining the optical rotation caused by a dark sugar solution of the type that is highly absorbent to visible light wavelengths, said method comprising: (a) producing infrared light waves; (b) transmitting at least portion of said infrared light waves through collimating optics; (c) polarizing said collimated light emitting from the collimating optics; (d) directing said polarized light through a dark sugar solution; and (e) analyzing the optical rotation of the polarized infrared light after passing through said sugar solution, and caused by the sugar solution.
Claim 23
Independent Claim 88 words
A method for determining the optical rotation caused by a dark sugar solution of the type that is highly absorbent to visible light wavelengths, said method comprising: (a) producing infrared light waves; (b) transmitting at least portion of said infrared light waves through collimating optics; (c) polarizing said collimated light emitting from the collimating optics; (d) directing said polarized light through a dark sugar solution; and (e) analyzing the optical rotation of the polarized infrared light after passing through said sugar solution, and caused by the sugar solution.
Claim 24
Dependent Claim 38 words
The method of claim 18, wherein the analyzing step includes detecting the polarized infrared light after passing through the sugar solution by splitting the polarized light into two components with orthogonal polarizations for use in determining optical rotation.
Claim 25
Dependent Claim 21 words
The method of claim 18, wherein the analyzing step includes the step of forming a ratio of the two orthogonal components.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-08-21 1988-02-20 1988-08-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-08-21 1992-02-20 1992-08-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-08-21 1996-02-20 1996-08-21 $7700.00 Window Closed / Lapsed

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