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US4464422A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preventing oxidation of copper film on ceramic body

Assignee: Murata Manufacturing Co Ltd
•
Filing: 1982-11-09
•
Granted: 1984-08-07
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Expires: 2002-11-09
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Abstract

Abstract A process for preventing the oxidation of a copper film formed on a ceramic body, which comprises the steps of forming a copper film on a ceramic body by a dry-plating process, treating the resultant copper film with a deactivating agent comprising at least one volatile hydrocarbon halide monomer by feeding the same into a vacuum chamber of a dry-plating apparatus.

Inventors

  • 👤 Atsuo Senda
  • 👤 Suehiro Kato
  • 👤 Toru Kasanami

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 12:01
CPC Classifications
B; B23; B23K; B23K35/00; B23K35/22; B23K35/226

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 60 words
A process for preventing oxidation of a copper film which has been formed on a ceramic body by a dry-plating process, which comprises contacting said copper film with a deactivating agent comprising at least one volatile hydrocarbon halide monomer in an evacuated vacuum chamber of the dry-plating apparatus before exposing the copper film on the ceramic body to the atmosphere.
Claim 2
Dependent Claim 60 words
A process for preventing oxidation of a copper film which has been formed on a ceramic body by a dry-plating process, which comprises contacting said copper film with a deactivating agent comprising at least one volatile hydrocarbon halide monomer in an evacuated vacuum chamber of the dry-plating apparatus before exposing the copper film on the ceramic body to the atmosphere.
Claim 3
Dependent Claim 28 words
The process according to claim 1 wherein said copper film is contacted with the deactivating agent by feeding the deactivating agent in a gaseous form into said chamber.
Claim 4
Dependent Claim 24 words
The process according to claim 1 wherein said copper film is contacted with the deactivating agent by spraying the deactivating agent into the chamber.
Claim 5
Dependent Claim 39 words
The process according to claim 1 wherein the copper film is contacted with the deactivating agent by feeding the deactivating agent into the chamber simultaneously with the surrounding atmosphere that is supplied for increasing the pressure in the chamber.
Claim 6
Dependent Claim 37 words
The process according to claim 1 wherein the deactivating agent is at least one volatile hydrocarbon halide monomer selected from the group consisting of trichloroethylene, tetrachloroethylene, trichlorofluoromethane, dichlorodifluoromethane, chlorodifluoromethane, 1,1,2-trichloro-1,2,2-trifluoroethane, carbon tetrachloride, methylchloride, methylene chloride, and chlorobenzene.
Claim 7
Dependent Claim 70 words
A process for producing copper-plated ceramic products for electronic ceramic components comprising the steps of forming a copper film on a ceramic body in an evacuated vacuum chamber by a dry-plating process, containing the resultant copper-plated ceramic body with a deactivating agent consisting essentially of at least one volatile hydrocarbon halide monomer to allow the copper to lose its catalytic activity before exposing said copper-plated caramic body to the atmosphere.
Claim 8
Dependent Claim 70 words
A process for producing copper-plated ceramic products for electronic ceramic components comprising the steps of forming a copper film on a ceramic body in an evacuated vacuum chamber by a dry-plating process, containing the resultant copper-plated ceramic body with a deactivating agent consisting essentially of at least one volatile hydrocarbon halide monomer to allow the copper to lose its catalytic activity before exposing said copper-plated caramic body to the atmosphere.
Claim 9
Dependent Claim 18 words
The process according to claim 6 wherein said copper film is formed by the vapor deposition of copper.
Claim 10
Dependent Claim 17 words
The process according to claim 6 wherein said copper film is formed by the sputtering of copper.
Claim 11
Dependent Claim 14 words
The process according to claim 6 wherein said copper film is formed by ion-plating.
Claim 12
Dependent Claim 27 words
The process according to claim 6 wherein said copper-plated ceramic body is contacted with the deactivating agent by introducing said agent in gaseous form into said chamber.
Claim 13
Dependent Claim 25 words
The process according to claim 6 wherein said copper-plated ceramic body is contacted with the deactivating agent by spraying the deactivating agent into said chamber.
Claim 14
Dependent Claim 36 words
The process according to claim 6 wherein the deactivating agent is at least one volatile hydrocarbon halide monomer selected from the group consisting of trichloroethylene, tetrachloroethylene, trichlorofluoromethane, dichlorodifluoromethane, chlorodifluoromethane, 1,1,2-trichloro-1,2,2-trifluoroethane, carbon tetrachloride, methylchloride, methylenechloride, and chlorobenzene.

References Cited (Backward Citations)

US2799600A Cited
US3227581A Cited
US3697342A Cited
JPS5420974A Cited
US4351695A Cited
US4325984A Cited
US4325984B1 Cited
US4325984B2 Cited
US4327131A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-08-07 1988-02-06 1988-08-07 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-08-07 1992-02-06 1992-08-07 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-08-07 1996-02-06 1996-08-07 $7700.00 Window Closed / Lapsed

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