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Production of magnetic powder

Assignee: Kanto Denka Kogyo Co Ltd
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Filing: 1981-02-11
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Granted: 1983-05-24
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Expires: 2001-02-11
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Abstract

Abstract The magnetic characteristics of magnetic powder consisting mainly of iron are improved by pre-treating the starting material from which the magnetic powder is prepared by reductions, with an aqueous solution and/or suspension of one member selected from the group consisting of zinc, chromium and copper compounds and mixtures thereof.

Inventors

  • 👤 Shintaro Suzuki
  • 👤 Sadao Iizuka
  • 👤 Yoshimi Moriya
  • 👤 Yuichi Omote

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 15:22
CPC Classifications
H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/032; H01F1/04; H01F1/06; H01F1/065; B; B22; B22F; B22F1/00; B22F1/17; Y; Y10; Y10T; Y10T428/00; Y10T428/12; Y10T428/12181

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 239 words
Acicular iron particles having improved properties for magnetic recording which contain at least one metal selected from the group consisting of zinc, chromium and copper, produced in accordance with the process comprising (a) treating a finely divided starting material in the form of acicular micro-particles selected from the group consisting of (i) iron oxyhydroxide, (ii) iron oxhydroxide containing a doping component selected from Co, Mn, Ni, Ti, Bi, Mo, Ag, Cr, Zn, Si, Al and mixtures thereof, (iii) iron oxides and (iv) iron oxides containing a doping component selected from Co, Mn, Ti, Bi, Mo, Ag, Cr, Zn, Si, Al and mixtures thereof, with an aqueous (1) solution or (2) suspension of an applied metal compound selected from the group consisting of zinc, chromium and copper compounds and mixtures thereof or a mixture of said aqueous solution and said aqueous suspension so that said applied metal compound is applied to said starting material, (b) filtering the thus treated material off the liquid medium to form a cake and drying said cake, and (c) reducing said dry cake in a reducing gas stream at a temperature up to about 600° C. whereby the individual particles are not sintered and the initial shape of the micro-particles of the starting material is retained and to form an acicular magnetic iron particle consisting essentially of iron and said applied metal selected from the group consisting of zinc, chromium and copper and mixtures thereof.
Claim 2
Dependent Claim 239 words
Acicular iron particles having improved properties for magnetic recording which contain at least one metal selected from the group consisting of zinc, chromium and copper, produced in accordance with the process comprising (a) treating a finely divided starting material in the form of acicular micro-particles selected from the group consisting of (i) iron oxyhydroxide, (ii) iron oxhydroxide containing a doping component selected from Co, Mn, Ni, Ti, Bi, Mo, Ag, Cr, Zn, Si, Al and mixtures thereof, (iii) iron oxides and (iv) iron oxides containing a doping component selected from Co, Mn, Ti, Bi, Mo, Ag, Cr, Zn, Si, Al and mixtures thereof, with an aqueous (1) solution or (2) suspension of an applied metal compound selected from the group consisting of zinc, chromium and copper compounds and mixtures thereof or a mixture of said aqueous solution and said aqueous suspension so that said applied metal compound is applied to said starting material, (b) filtering the thus treated material off the liquid medium to form a cake and drying said cake, and (c) reducing said dry cake in a reducing gas stream at a temperature up to about 600° C. whereby the individual particles are not sintered and the initial shape of the micro-particles of the starting material is retained and to form an acicular magnetic iron particle consisting essentially of iron and said applied metal selected from the group consisting of zinc, chromium and copper and mixtures thereof.
Claim 3
Dependent Claim 50 words
The acicular iron particles of claim 1 wherein after said iron particles has been prepared by reducing said dry cake in a reducing gas stream, the reduced material is contacted with a stream comprising an inert gas and a minor proportion of air whereby said acicular iron particles are stabilized.
Claim 4
Dependent Claim 42 words
The acicular iron particles of claim 1 or 2 wherein said applied metal compound is a metal compound used in an amount of about 1% to about 10% by weight of the weight of the iron in said finely divided starting material.
Claim 5
Dependent Claim 13 words
The acicular iron particles of claim 3 wherein said applied metal is copper.
Claim 6
Dependent Claim 13 words
The acicular iron particles of claim 3 wherein said applied metal is zinc.
Claim 7
Dependent Claim 13 words
The acicular iron particles of claim 3 wherein said applied metal is chromium.
Claim 8
Dependent Claim 35 words
The acicular iron particles of claim 1 or 2 wherein said acicular iron powders contain at least about 0.3 molar percent of said applied metal selected from the group consisting of zinc, chromium and copper.
Claim 9
Dependent Claim 13 words
The acicular iron particles of claim 7 wherein said applied metal is copper.
Claim 10
Dependent Claim 13 words
The acicular iron particles of claim 7 wherein said applied metal is zinc.
Claim 11
Dependent Claim 13 words
The acicular iron particles of claim 7 wherein said applied metal is chromium.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-05-23 1986-11-22 1987-05-24 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-05-23 1990-11-22 1991-05-24 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-05-23 1994-11-22 1995-05-24 $7700.00 Window Closed / Lapsed

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