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US4366008A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for hardening steel

Assignee: Nachi Fujikoshi Corp
•
Filing: 1981-03-20
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Granted: 1982-12-28
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Expires: 2001-03-20
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Abstract

Abstract A method of hardening steel so that it may have a surface layer with sufficient hardness to permit fabrication into machinery parts with a minimum of strain developed therein. The method comprises heating steel at a temperature in a range not lower than 100° C. below its A 1 transformation point (about 630° C.) and not higher than 50° C. thereabove (about 780° C.) in an atmosphere consisting solely of ammonia gas, or composed of ammonia gas and at least one of organic liquids, petroleum gases, endothermic gases and neutral gases, while ammonia gas is being supplied continuously at a lower flow rate, or at a higher flow rate followed by a diffusion treatment to austenitize a surface layer of the steel by penetration of nitrogen thereinto, and quenching the steel to transform the austenitized surface layer into a martensite layer.

Inventors

  • 👤 Jun Takeuchi
  • 👤 Kaishu Yamazumi
  • 👤 Takao Ishihara

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 05:23
CPC Classifications
C; C23; C23C; C23C8/00; C23C8/80; C21; C21D; C21D1/00; C21D1/78; C23C8/06; C23C8/08; C23C8/24; C23C8/26

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 96 words
A method of hardening steel, comprising: heating the steel at a temperature in a range not lower than 100° C. below the A 1 transformation point of the steel (about 630° C.) and not higher than 50° C. above said transformation point (about 780° C.) in an atmosphere composed solely of ammonia gas being supplied at a flow rate of from about 0.1 to 2 furnace volume per hour to austenitize a surface layer of the steel by penetration of nitrogen thereinto, and quenching the steel to transform said austenitized surface layer into a martensite layer.
Claim 2
Independent Claim 96 words
A method of hardening steel, comprising: heating the steel at a temperature in a range not lower than 100° C. below the A 1 transformation point of the steel (about 630° C.) and not higher than 50° C. above said transformation point (about 780° C.) in an atmosphere composed solely of ammonia gas being supplied at a flow rate of from about 0.1 to 2 furnace volume per hour to austenitize a surface layer of the steel by penetration of nitrogen thereinto, and quenching the steel to transform said austenitized surface layer into a martensite layer.
Claim 3
Independent Claim 120 words
A method of hardening steel, comprising: heating the steel at a temperature in a range not lower than 100° C. below the A 1 transformation point of the steel (about 630° C.) and not higher than 50° C. above said transformation point (about 780° C.) in an atmospere composed solely of ammonia gas being supplied at a flow rate of from about 2.1 to 7.5 furnace volume per hour to austenitize a surface layer of the steel by penetration of nitrogen thereinto, and discontinuing the supply of ammonia gas and heating at the same temperature for about half an hour to one hour for diffusion treatment, and quenching the steel to transform said austenitized surface layer into a martensite layer.
Claim 4
Independent Claim 120 words
A method of hardening steel, comprising: heating the steel at a temperature in a range not lower than 100° C. below the A 1 transformation point of the steel (about 630° C.) and not higher than 50° C. above said transformation point (about 780° C.) in an atmospere composed solely of ammonia gas being supplied at a flow rate of from about 2.1 to 7.5 furnace volume per hour to austenitize a surface layer of the steel by penetration of nitrogen thereinto, and discontinuing the supply of ammonia gas and heating at the same temperature for about half an hour to one hour for diffusion treatment, and quenching the steel to transform said austenitized surface layer into a martensite layer.
Claim 5
Independent Claim 147 words
A method of hardening steel, comprising: heating the steel at a temperature in a range not lower than 100° C. below the A 1 transformation point of the steel (about 630° C.) and not higher than 50° C. above said transformation point (about 780° C.) in an atmosphere composed of ammonia gas being supplied continuously at a partial pressure of from about 0.05 to 0.3, and at least one substance selected from the group consisting of (a) petroleum gas such as propane and butane, (b) endothermic gas generated by reforming petroleum gas, (c) a carburizing and reducing gas or liquid, including an organic liquid such as alcohols, esters and ketones, and (d) a neutral gas such as nitrogen and argon, to austenitize a surface layer of the steel by penetration of nitrogen thereinto, and quenching the steel to transform said austenitized surface layer into a martensite layer.
Claim 6
Independent Claim 147 words
A method of hardening steel, comprising: heating the steel at a temperature in a range not lower than 100° C. below the A 1 transformation point of the steel (about 630° C.) and not higher than 50° C. above said transformation point (about 780° C.) in an atmosphere composed of ammonia gas being supplied continuously at a partial pressure of from about 0.05 to 0.3, and at least one substance selected from the group consisting of (a) petroleum gas such as propane and butane, (b) endothermic gas generated by reforming petroleum gas, (c) a carburizing and reducing gas or liquid, including an organic liquid such as alcohols, esters and ketones, and (d) a neutral gas such as nitrogen and argon, to austenitize a surface layer of the steel by penetration of nitrogen thereinto, and quenching the steel to transform said austenitized surface layer into a martensite layer.
Claim 7
Independent Claim 170 words
A method of hardening steel, comprising: heating the steel at a temperature in a range not lower than 100° C. below the A 1 transformation point of the steel (about 630° C.) and not higher than 50° C. above said transformation point (about 780° C.) in an atmosphere composed of ammonia gas being supplied at a partial pressure of from about 0.31 to 0.95, and at least one substance selected from the group consisting of (a) petroleum gas such as propane and butane, (b) endothermic gas generated by reforming petroleum gas, (c) a carburizing and reducing gas or liquid, including an organic liquid such as alcohols, esters and ketones, and (d) a neutral gas such as nitrogen and argon, to austenitize a surface layer of the steel by penetration of nitrogen thereinto, and discontinuing the supply of ammonia gas and heating at the same temperature for about half an hour to one hour for diffusion treatment, and quenching the steel to transform said austenitized surface layer into a martensite layer.
Claim 8
Independent Claim 170 words
A method of hardening steel, comprising: heating the steel at a temperature in a range not lower than 100° C. below the A 1 transformation point of the steel (about 630° C.) and not higher than 50° C. above said transformation point (about 780° C.) in an atmosphere composed of ammonia gas being supplied at a partial pressure of from about 0.31 to 0.95, and at least one substance selected from the group consisting of (a) petroleum gas such as propane and butane, (b) endothermic gas generated by reforming petroleum gas, (c) a carburizing and reducing gas or liquid, including an organic liquid such as alcohols, esters and ketones, and (d) a neutral gas such as nitrogen and argon, to austenitize a surface layer of the steel by penetration of nitrogen thereinto, and discontinuing the supply of ammonia gas and heating at the same temperature for about half an hour to one hour for diffusion treatment, and quenching the steel to transform said austenitized surface layer into a martensite layer.

References Cited (Backward Citations)

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US3357869A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1985-12-27 1986-06-28 1986-12-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1989-12-27 1990-06-28 1990-12-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1993-12-27 1994-06-28 1994-12-28 $7700.00 Window Closed / Lapsed

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