Patent US4346014A successfully refreshed from Google Patents.
US4346014A
Expired / Lapsed
US
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Rolling oil compositions and method of inhibiting carbon smut on batch annealed steel
Assignee: Arkema Inc
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Filing: 1981-04-20
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Granted: 1982-08-24
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Expires: 2001-04-20
Abstract
Abstract Carbon smut on post-annealed cold rolled steel sheet and strip is inhibited by a process using a rolling oil containing from 0.5 to 5% by weight of specific organic nitro compounds in the cold rolling oil. The steel sheet and strip are substantially smut free after batch annealing. Rolling oils and their aqueous emulsions containing the organic nitro inhibitors are also disclosed and claimed.
Inventors
- 👤 Joseph A. Piucci
- 👤 Kurt Goltz
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-06 14:44
CPC Classifications
C; C10; C10M; C10M173/00; C10M173/02; C10M2201/00; C10M2201/02; C10M2207/00; C10M2207/02; C10M2207/023; C10M2207/026; C10M2207/10; C10M2207/12; C10M2207/125; C10M2207/129; C10M2207/18; C10M2207/28; C10M2207/281; C10M2207/282; C10M2207/283; C10M2207/286; C10M2207/40; C10M2207/404; C10M2209/00; C10M2209/10; C10M2209/103; C10M2209/104; C10M2215/00; C10M2215/02; C10M2215/04; C10M2215/042; C10M2215/06; C10M2215/064; C10M2215/20; C10M2215/202; C10M2215/22; C10M2215/221; C10M2215/225; C10M2215/226; C10M2215/24; C10M2215/26; C10M2215/30; C10M2219/00; C10M2219/10; C10M2219/102; C10M2219/104; C10M2219/106; C10M2229/00; C10M2229/02; C10M2229/04; C10M2229/05; C10N; C10N2050/00; C10N2050/01
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
109 words
In a process for producing steel sheet or strip substantially free of carbon smut deposits from cold rolled steel sheet or strip the improvement comprising cold rolling the steel sheet or strip in contact with a rolling oil containing about 0.5 to 5% by weight of one or more organic nitro-compounds selected from the group consisting of 2,4-dinitro benzoic acid, 2,5-dinitro benzoic acid, 3,4-dinitro benzoic acid, 3,5-dinitro benzoic acid, picric acid, 1,3-dinitro benzene, 2,4,6-trinitro toluene, 3,5-dinitro salicylic acid, 2-amino-6- nitrobenzothiazole, poly glycol ester of 3,5-dinitro benzoic acid, dimethyl octyne diol ester of 3,5-dinitro benzoic acid, 2,4,7-trinitro-9-fluorenone and 1,5-difluoro-2,4-dinitro benzene and thereafter without further treatment batch annealing the steel strip.
Claim 2
Dependent Claim
109 words
In a process for producing steel sheet or strip substantially free of carbon smut deposits from cold rolled steel sheet or strip the improvement comprising cold rolling the steel sheet or strip in contact with a rolling oil containing about 0.5 to 5% by weight of one or more organic nitro-compounds selected from the group consisting of 2,4-dinitro benzoic acid, 2,5-dinitro benzoic acid, 3,4-dinitro benzoic acid, 3,5-dinitro benzoic acid, picric acid, 1,3-dinitro benzene, 2,4,6-trinitro toluene, 3,5-dinitro salicylic acid, 2-amino-6- nitrobenzothiazole, poly glycol ester of 3,5-dinitro benzoic acid, dimethyl octyne diol ester of 3,5-dinitro benzoic acid, 2,4,7-trinitro-9-fluorenone and 1,5-difluoro-2,4-dinitro benzene and thereafter without further treatment batch annealing the steel strip.
Claim 3
Dependent Claim
40 words
The process of claim 1 in which the amount of the organic nitro compound carbon smut inhibitor in the rolling oil ranges from about 1 to 5% by weight based on the mixture of organic nitro compound and rolling oil.
Claim 4
Dependent Claim
22 words
The process of claim 1 in which the rolling oil containing the organic nitro compound carbon smut inhibitor is emulsified in water.
Claim 5
Dependent Claim
24 words
The process of claim 3 in which the rolling oil comprises 2 to 20% by weight of the mixture of rolling oil and water.
Claim 6
Dependent Claim
25 words
The process of claim 1 in which a pH modifier is present in the rolling oil at a concentration of 0 to 8% by weight.
Claim 7
Dependent Claim
35 words
The process of claim 1 in which an aliphatic amine of C 2 to C 12 content is present in the rolling oil at a concentration of 0 to 8% by weight to control acidity.
Claim 8
Dependent Claim
73 words
A rolling lubricant for cold rolling steel sheet or strip comprising a rolling oil containing from 0.5 to 5% by weight of one or more members selected from the group consisting of 2,4-dinitro benzoic acid, 2,5-dinitro benzoic acid, 3,4-dinitro benzoic acid, 3,5-dinitro benzoic acid, picric acid, 1,3-dinitro benzene, 2,4,6-trinitro toluene, 3,5-dinitro salicylic acid, 2-amino-6-nitrobenzothiazole, poly glycol ester of 3,5-dinitro benzoic acid, dimethyl octyne diol ester of 3,5-dinitro benzoic acid, 2,4,7-trinitro-9-fluorenone and 1,5-difluoro-2,4-dinitro benzene.
Claim 9
Dependent Claim
73 words
A rolling lubricant for cold rolling steel sheet or strip comprising a rolling oil containing from 0.5 to 5% by weight of one or more members selected from the group consisting of 2,4-dinitro benzoic acid, 2,5-dinitro benzoic acid, 3,4-dinitro benzoic acid, 3,5-dinitro benzoic acid, picric acid, 1,3-dinitro benzene, 2,4,6-trinitro toluene, 3,5-dinitro salicylic acid, 2-amino-6-nitrobenzothiazole, poly glycol ester of 3,5-dinitro benzoic acid, dimethyl octyne diol ester of 3,5-dinitro benzoic acid, 2,4,7-trinitro-9-fluorenone and 1,5-difluoro-2,4-dinitro benzene.
Claim 10
Dependent Claim
32 words
An aqueous emulsion of the rolling lubricant of claim 7 at a concentration of 0.5 to 15% by weight of rolling lubricant based on the combined weight of rolling lubricant and water.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1985-08-23 | 1986-02-22 | 1986-08-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1989-08-23 | 1990-02-22 | 1990-08-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1993-08-23 | 1994-02-22 | 1994-08-24 | $7700.00 | Window Closed / Lapsed |