Patent US4425281A successfully refreshed from Google Patents.
Patent US4256599A successfully refreshed from Google Patents.
US4256599A
Expired / Lapsed
US
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Denture cleansing tablet and process for making
Assignee: Kukident Richardson GmbH
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Filing: 1979-04-03
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Granted: 1981-03-17
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Expires: 1999-04-03
Abstract
Abstract A two layered cleansing tablet for the self-acting cleansing of dentures. The layers of the tablet disintegrate at controlled rates so that denture cleansing action is made more efficient and effective compared to single layered tablet structures. The present tablet employs sulfonic acid in the tablet layer which disintegrates in a first stage cleansing step and further employs ethylene diamine tetraacetate in both tablet layers. Improved denture cleansing action is achieved even with no increase in the total amount of active agents employed in a tablet.
Inventors
- 👤 Werner Krisp
- 👤 Rainer Malkowski
- 👤 Mira Reuss
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 13:37
CPC Classifications
A; A61; A61Q; A61Q11/00; A61Q11/02; A61K; A61K8/00; A61K8/02; A61K8/0216; A61K8/18; A61K8/30; A61K8/40; A61K8/44; A61K8/46; A61K2800/00; A61K2800/20; A61K2800/22; A61K2800/222
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
475 words
A two-layered cleansing tablet for the self-acting cleansing of dentures in an aqueous solution comprising (A) a first layer comprising on a total 100 weight percent dry weight first layer basis a mixture of (1) from about 35 to 50 weight percent sodium bicarbonate, (2) from about 20 to 30 weight percent sodium hexametaphosphate, (3) from about 15 to 20 weight percent of sulfamic acid, (4) from about 2 to 6 weight percent of ethylene diamine tetraacetate, (5) from about 1 to 4 weight percent of polyethylene glycol having a molecular weight ranging from about 18,000 to 24,000, (6) from about 0.5 to 2 weight percent of surfactant, (7) from about 0 to 2 weight percent bentonite, (8) from about 0 to 1 weight percent hardened triglyceride powder, (9) from about 0 to 2 weight percent 4-hydroxybenzoic acid alkyl ester, (B) a second layer comprising on a total 100 weight percent dry weight second layer basis a mixture of (1) from about 15 to 25 weight percent of sodium bicarbonate, (2) from about 8 to 15 weight percent sodium hexametaphosphate, (3) from about 1 to 8 weight percent ethylene diamine tetraacetate, (4) from about 10 to 15 weight percent acidic sodium pyrophosphate, (5) from about 25 to 35 weight percent of an alkali metal salt of peroxymonosulfuric acid, (6) from about 1 to 4 weight percent polyethylene glycol having a molecular weight ranging from about 18,000 to 24,000, (7) from about 3 to 6 weight percent water soluble starch, (8) from about 1 to 3 weight percent of polymeric dye carrier manifesting surface active cleansing properties and selected from the the group consisting of sodium polyacrylate and a water soluble cross linked polyvinyl pyrrolidone having a k-value of from about 24 to 27, (9) from about 1 to 3 percent dibasic calcium phosphate having a heavy metal content of less than about 0.1 percent by weight, (10) from about 1 to 3 weight percent surfactant, (11) from about 0 to 2 weight percent of sugar fatty acid esters wherein from about 30 to 70 weight percent thereof comprises stearate and 70 to 30 weight percent thereof comprises palmitate fatty acid components on a 100 weight percent total ester basis and with a monoester content of 40 to 70 weight percent and a di-and tri-ester content of 60 to 39 weight percent on a 100 weight percent total ester basis, (12) from about 0 to 2 weight percent 4-hydroxybenzoic acid alkyl ester, (13) from about 0 to 3 weight percent hardened triglyceride (C) the total quantity of said ethylene diamine tetraacetate in said tablet on a 100 weight percent total dry weight basis ranging from about 5 to 10 weight percent and the pH of the solution produced on dissolution in water being from about 6.5 to 7.0 during dissolution of the first and second layers.
Claim 2
Dependent Claim
475 words
A two-layered cleansing tablet for the self-acting cleansing of dentures in an aqueous solution comprising (A) a first layer comprising on a total 100 weight percent dry weight first layer basis a mixture of (1) from about 35 to 50 weight percent sodium bicarbonate, (2) from about 20 to 30 weight percent sodium hexametaphosphate, (3) from about 15 to 20 weight percent of sulfamic acid, (4) from about 2 to 6 weight percent of ethylene diamine tetraacetate, (5) from about 1 to 4 weight percent of polyethylene glycol having a molecular weight ranging from about 18,000 to 24,000, (6) from about 0.5 to 2 weight percent of surfactant, (7) from about 0 to 2 weight percent bentonite, (8) from about 0 to 1 weight percent hardened triglyceride powder, (9) from about 0 to 2 weight percent 4-hydroxybenzoic acid alkyl ester, (B) a second layer comprising on a total 100 weight percent dry weight second layer basis a mixture of (1) from about 15 to 25 weight percent of sodium bicarbonate, (2) from about 8 to 15 weight percent sodium hexametaphosphate, (3) from about 1 to 8 weight percent ethylene diamine tetraacetate, (4) from about 10 to 15 weight percent acidic sodium pyrophosphate, (5) from about 25 to 35 weight percent of an alkali metal salt of peroxymonosulfuric acid, (6) from about 1 to 4 weight percent polyethylene glycol having a molecular weight ranging from about 18,000 to 24,000, (7) from about 3 to 6 weight percent water soluble starch, (8) from about 1 to 3 weight percent of polymeric dye carrier manifesting surface active cleansing properties and selected from the the group consisting of sodium polyacrylate and a water soluble cross linked polyvinyl pyrrolidone having a k-value of from about 24 to 27, (9) from about 1 to 3 percent dibasic calcium phosphate having a heavy metal content of less than about 0.1 percent by weight, (10) from about 1 to 3 weight percent surfactant, (11) from about 0 to 2 weight percent of sugar fatty acid esters wherein from about 30 to 70 weight percent thereof comprises stearate and 70 to 30 weight percent thereof comprises palmitate fatty acid components on a 100 weight percent total ester basis and with a monoester content of 40 to 70 weight percent and a di-and tri-ester content of 60 to 39 weight percent on a 100 weight percent total ester basis, (12) from about 0 to 2 weight percent 4-hydroxybenzoic acid alkyl ester, (13) from about 0 to 3 weight percent hardened triglyceride (C) the total quantity of said ethylene diamine tetraacetate in said tablet on a 100 weight percent total dry weight basis ranging from about 5 to 10 weight percent and the pH of the solution produced on dissolution in water being from about 6.5 to 7.0 during dissolution of the first and second layers.
Claim 3
Dependent Claim
33 words
The two-layered tablet of claim 1 additionally having incorporated into said second layer thereof from about 0.1 to 1 weight percent silicic acid produced by hydrolysis of silicon tetrachloride in an oxy-hydrogen flame.
Claim 4
Dependent Claim
33 words
The two-layered tablet of claim 1 wherein said first layer contains from about 1 to 3 weight of a water soluble cross-linked polyvinyl pyrrolidone having a k-value of from about 24 to 27.
Claim 5
Dependent Claim
22 words
The two-layered tablet of claim 1 wherein said first layer contains from about 1 to 3 weight percent water soluble corn starch.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-03-16 | 1984-09-15 | 1985-03-17 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-03-16 | 1988-09-15 | 1989-03-17 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-03-16 | 1992-09-15 | 1993-03-17 | $7700.00 | Window Closed / Lapsed |