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Method of forming an insulating film on a grain-oriented silicon steel sheet

Assignee: JFE Steel Corp
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Filing: 1979-04-23
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Granted: 1980-12-30
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Expires: 1999-04-23
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Abstract

Abstract A highly adhesive and uniform insulating film can be formed on a grain-oriented silicon steel sheet without deteriorating the iron loss of the steel sheet by the use of a magnesia series annealing separator containing a strontium compound.

Inventors

  • 👤 Nobuyuki Morito
  • 👤 Toshitomo Sugiyama
  • 👤 Yasuo Yokoyama
  • 👤 Toshio Ichida

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 19:41
CPC Classifications
C; C21; C21D; C21D8/00; C21D8/12; C21D8/1277; C21D8/1283; C23; C23D; C23D5/00; C23D5/10

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 130 words
A method of forming a highly adhesive and uniform insulating film on a grain-oriented silicon steel sheet, without deteriorating the iron loss of the steel sheet, wherein a cold rolled silicon steel sheet having a final gauge is subjected to a decarburization annealing to form a silica-containing subscale on the surface, coated with an annealing separator consisting mainly of magnesia on the subscale and subjected to a final annealing to form an insulating film, an improvement comprising using a magnesia series annealing separator containing 0.1-10% by weight, calculated as strontium, of at least one strontium compound selected from the group consisting of SrSO 4 , Sr(OH) 2 .8H 2 O, SrCO 3 , and Sr(NO 3 ) 2 , and 0.5-5% by weight, calculated as titanium, of a titanium compound.
Claim 2
Independent Claim 130 words
A method of forming a highly adhesive and uniform insulating film on a grain-oriented silicon steel sheet, without deteriorating the iron loss of the steel sheet, wherein a cold rolled silicon steel sheet having a final gauge is subjected to a decarburization annealing to form a silica-containing subscale on the surface, coated with an annealing separator consisting mainly of magnesia on the subscale and subjected to a final annealing to form an insulating film, an improvement comprising using a magnesia series annealing separator containing 0.1-10% by weight, calculated as strontium, of at least one strontium compound selected from the group consisting of SrSO 4 , Sr(OH) 2 .8H 2 O, SrCO 3 , and Sr(NO 3 ) 2 , and 0.5-5% by weight, calculated as titanium, of a titanium compound.

References Cited (Backward Citations)

US2394047A Cited
US3477881A Cited
US3627594A Cited
US3582407A Cited
US3959034A Cited
US3930905A Cited
US4010050A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-12-30 1984-06-30 1984-12-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-12-30 1988-06-30 1988-12-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-12-30 1992-06-30 1992-12-30 $7700.00 Window Closed / Lapsed

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