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US4010050A Expired / Lapsed US ⏱️ 0.0 years remaining

Processing for aluminum nitride inhibited oriented silicon steel

Assignee: Allegheny Ludlum Corp
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Filing: 1975-09-08
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Granted: 1977-03-01
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Expires: 1995-09-08
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Abstract

Abstract A process for producing electromagnetic silicon steel having a cube-on-edge orientation and a permeability of at least 1850 (G/O e ) at 10 oersteds. The process includes the steps of: preparing an aluminum-bearing melt of silicon steel; casting the steel; hot rolling the steel; cold rolling the steel; decarburizing the steel; coating the steel with a base coating containing an amide and/or imide of an organic and/or inorganic acid; and final texture annealing the steel.

Inventors

  • 👤 Edward G. Choby, Jr.

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 17:27
CPC Classifications
C; C21; C21D; C21D8/00; C21D8/12; C21D8/1277; C21D8/1283; C23; C23D; C23D5/00; C23D5/10; H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/12; H01F1/14; H01F1/147; H01F1/14766; H01F1/14775; H01F1/14783

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 223 words
In a process for producing electromagnetic silicon steel having a cube-on-edge orientation and a permeability of at least 1850 (G/O e ) at 10 oersteds, which process includes the steps of: preparing a melt of silicon steel containing, by weight, up to 0.07% carbon, from 2.8 to 4.0% silicon, from 0.03 to 0.24% manganese, from 0.01 to 0.09% of material from the group consisting of sulfur and selenium, from 0.015 to 0.04% aluminum, up to 0.02% nitrogen, up to 0.5% copper and up to 0.0035% boron; casting said steel; hot rolling said steel; cold rolling said steel at a reduction of at least 75% decarburizing said steel; and final texturing said steel; the improvement comprising the steps of coating the surface of said steel with a base composition consisting essentially of: a. 100 parts, by weight, of at least one substance from the group consisting of boron, boron compounds, sulfur, sulfur compounds, selenium, selenium compounds, and oxides and hydroxides of magnesium, calcium, aluminum, titanium and manganese; and b. 4 to 120 parts, by weight, of at least one substance from the group consisting of amides and imides of organic and inorganic acids; and final texture annealing said steel with said coating thereon; said steel's texture and magnetic properties being, in part, attributable to said substance from the group consisting of amides and imides.
Claim 2
Dependent Claim 223 words
In a process for producing electromagnetic silicon steel having a cube-on-edge orientation and a permeability of at least 1850 (G/O e ) at 10 oersteds, which process includes the steps of: preparing a melt of silicon steel containing, by weight, up to 0.07% carbon, from 2.8 to 4.0% silicon, from 0.03 to 0.24% manganese, from 0.01 to 0.09% of material from the group consisting of sulfur and selenium, from 0.015 to 0.04% aluminum, up to 0.02% nitrogen, up to 0.5% copper and up to 0.0035% boron; casting said steel; hot rolling said steel; cold rolling said steel at a reduction of at least 75% decarburizing said steel; and final texturing said steel; the improvement comprising the steps of coating the surface of said steel with a base composition consisting essentially of: a. 100 parts, by weight, of at least one substance from the group consisting of boron, boron compounds, sulfur, sulfur compounds, selenium, selenium compounds, and oxides and hydroxides of magnesium, calcium, aluminum, titanium and manganese; and b. 4 to 120 parts, by weight, of at least one substance from the group consisting of amides and imides of organic and inorganic acids; and final texture annealing said steel with said coating thereon; said steel's texture and magnetic properties being, in part, attributable to said substance from the group consisting of amides and imides.
Claim 3
Dependent Claim 35 words
An improvement according to claim 1, wherein said composition has from 10 to 40 parts, by weight, of at least one substance from the group consisting of amides and imides of organic and inorganic acids.
Claim 4
Dependent Claim 32 words
An improvement according to claim 1, wherein said substance from the group consisting of amides and imides of organic and inorganic acids is from the group consisting of sulfamic acid and urea.
Claim 5
Dependent Claim 12 words
An improvement according to claim 3, wherein said composition contains sulfamic acid.
Claim 6
Dependent Claim 20 words
An improvement according to claim 1, wherein said composition has 100 parts, by weight, of oxides and hydroxides of magnesium.
Claim 7
Dependent Claim 35 words
An improvement according to claim 5, wherein said composition has from 10 to 40 parts, by weight, of at least one substance from the group consisting of amides and imides of organic and inorganic acids.
Claim 8
Dependent Claim 32 words
An improvement according to claim 5, wherein said substance from the group consisting of amides and imides of organic and inorganic acids is from the group consisting of sulfamic acid and urea.
Claim 9
Dependent Claim 12 words
An improvement according to claim 7, wherein said composition contains sulfamic acid.

References Cited (Backward Citations)

US1965798A Cited
US2801154A Cited
US3399085A Cited
US3676227A Cited
US3700506A Cited
US3855018A Cited
US3855018B1 Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-02-29 1980-08-30 1981-03-01 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-02-29 1984-08-30 1985-03-01 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-02-29 1988-08-30 1989-03-01 $7700.00 Window Closed / Lapsed

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