← Back to Patent Explorer
US4229492A Expired / Lapsed US ⏱️ 0.0 years remaining

Control of autodeposition baths

Assignee: Henkel Corp
•
Filing: 1977-12-30
•
Granted: 1980-10-21
•
Expires: 1997-12-30
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract An autodepositing coating process wherein a coating bath containing an acidic aqueous coating composition comprising as essential ingredients: (1) an acid; (2) an oxidizing agent; and (3) an aqueous dispersion of coating forming resin particles and surfactant, which surfactant is subject to being slowly altered by the acidic oxidizing environment in the metal coating bath resulting in the buildup of reaction products in the bath, which bath is maintained in continuous coating forming operability by replenishing in a manner which prevents the deterioration of the coating quality of the bath. The coating composition and replenishing composition may also contain as an optional ingredient an aqueous dispersion of pigment and surfactant and may also contain non-essential ingredients, which non-essential ingredients may increase in concentration as the bath is operated until a deleterious effect is asserted on the coating formation. The coating quality of the replenished bath is maintained by the addition of an aqueous surfactant composition and by operating the replenished bath at an elevated redox potential or by removal of the altered surfactant.

Inventors

  • 👤 Harry M. Leister
  • 👤 Joseph C. Donovan
  • 👤 Wilbur S. Hall

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 18:09
CPC Classifications
B; B05; B05D; B05D7/00; B05D7/14; B05D7/142; C; C09; C09D; C09D5/00; C09D5/08; C09D5/088

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 47 words
In an autodepositing coating process wherein an aqueous acidic coating composition having dispersed therein a coating forming resin and a surfactant, wherein said surfactant is modified in the course of the coating operation, the improvement which comprises extracting the modified surfactant with a water immiscible organic solvent.
Claim 2
Dependent Claim 47 words
In an autodepositing coating process wherein an aqueous acidic coating composition having dispersed therein a coating forming resin and a surfactant, wherein said surfactant is modified in the course of the coating operation, the improvement which comprises extracting the modified surfactant with a water immiscible organic solvent.
Claim 3
Dependent Claim 21 words
The improvement in an autodepositing process according to claim 1 wherein the surfactant is a salt of an alkyl aryl sulfonate.
Claim 4
Dependent Claim 17 words
The improvement in an autodepositing process according to claim 2 wherein the surfactant is sodium dodecylbenzene sulfonate.
Claim 5
Dependent Claim 18 words
The improvement in an autodepositing process according to claim 3 wherein the modified surfactant is extracted with 1,1,1-trichlorethane.

References Cited (Backward Citations)

US2658839A Cited
US2819188A Cited
US3261711A Cited
US3438926A Cited
US3585084A Cited
US3592699A Cited
US3472808A Cited
US3647567A Cited
US3709743A Cited
ZA721146B Cited
US3936546A Cited
US3876434A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-10-21 1984-04-21 1984-10-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-10-21 1988-04-21 1988-10-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-10-21 1992-04-21 1992-10-21 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag