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US4183738A Expired / Lapsed US ⏱️ 0.0 years remaining

Granulation process and products produced thereby

Assignee: International Fertilizer Development Center
•
Filing: 1977-05-09
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Granted: 1980-01-15
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Expires: 1997-05-09
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Abstract

Abstract A granulation process for the production of high purity granules of salt material comprising: (a) a wet blend formed by intensively mixing together (i) particles of soluble fine water-soluble salt having a relatively wide size distribution over the range of from about -30 to about +325 screen size (Tyler mesh), (ii) water insoluble particles of about -150 screen size (Tyler mesh) with surface area above 1 M 2 /gr, and (iii) sufficient water or saturated water solution to provide a moisture content of up to about 20% and preferably in the range of from about 5 to 15% by weight of the mixture, (b) granulating the wet blend from (a), preferably by pan granulation, and (c) drying and recovering the granular product. The product comprises a granular salt product which has the properties of high purity (up to 99% salt), uniform size distribution in the range of from about 2 to 4 mm, a crush strength of greater than about 3 lb/granule and generally in the range of from about 5 to 10 lbs. and a final moisture content of about 1.0% or less.

Inventors

  • 👤 Samuel Carmon

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 12:31
CPC Classifications
C; C05; C05D; C05D1/00; C05D1/005; B; B01; B01J; B01J2/00; B01J2/28; C05C; C05C1/00; C05C1/02; C05C3/00; C05C3/005

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 96 words
A granular salt product comprising free flowing granules containing from about 70 to 99% by weight of a water soluble salt selected from the group consisting of ammonium sulfate, ammonium nitrate, potassium chloride and potassium sulfate, from 1 to 30% by weight of an insoluble solid material and about 1% by weight or less of water based upon the combined weight of said salt and said insoluble solid material, said granules having a relatively uniform size distribution in the range of from about 2 to 4 mm and a crush strength of above about 3 lbs/granule.
Claim 2
Dependent Claim 96 words
A granular salt product comprising free flowing granules containing from about 70 to 99% by weight of a water soluble salt selected from the group consisting of ammonium sulfate, ammonium nitrate, potassium chloride and potassium sulfate, from 1 to 30% by weight of an insoluble solid material and about 1% by weight or less of water based upon the combined weight of said salt and said insoluble solid material, said granules having a relatively uniform size distribution in the range of from about 2 to 4 mm and a crush strength of above about 3 lbs/granule.
Claim 3
Dependent Claim 25 words
The product of claim 1 wherein said insoluble material is selected from the group consisting of phosphate rock, calcium carbonate, calcium sulfate and carbon black.
Claim 4
Dependent Claim 27 words
The product of claim 2 wherein said granules contain from about 95 to 99% of said salt and from about 1 to 5% of said insoluble material.
Claim 5
Dependent Claim 18 words
The product of claim 3 wherein the average crush strength of said granules is above about 5 lbs/granule.
Claim 6
Dependent Claim 18 words
The product of claim 1 wherein a mixture of soluble salts are used instead of a single salt.

References Cited (Backward Citations)

US3776713A Cited
US3660068A Cited
US3692511A Cited
US3725029A Cited
US3853490A Cited
US3923489A Cited
US4008065A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-01-14 1983-07-16 1984-01-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-01-14 1987-07-16 1988-01-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-01-14 1991-07-16 1992-01-15 $7700.00 Window Closed / Lapsed

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