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US4175055A Expired / Lapsed US ⏱️ 0.0 years remaining

Dry mix method for making an electrochemical cell electrode

Assignee: RTX Corp
•
Filing: 1978-06-28
•
Granted: 1979-11-20
•
Expires: 1998-06-28
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Abstract

Abstract A method for making an electrochemical cell electrode involves depositing a layer of mechanically blended dry catalyzed carbon powder and dry hydrophobic polymer powder on the surface of a substrate by dispersing the mixture of powders as a cloud in a chamber over the substrate and pulling the powder onto the substrate by drawing a vacuum under the substrate. The method is particularly adapted to the high speed manufacture of electrodes.

Inventors

  • 👤 Glen J. Goller
  • 👤 Vincent J. Petraglia
  • 👤 Joseph R. Salonia

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 23:19
CPC Classifications
H; H01; H01M; H01M4/00; H01M4/86; H01M4/88; H01M4/8825; H01M4/886; H01M4/8878; H01M4/8882; H01M4/8885; H01M4/8896; H01M4/96; Y; Y02; Y02E; Y02E60/00; Y02E60/30; Y02E60/50

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 102 words
A method for making an electrochemical cell electrode comprising the steps of: blending together, in dry form, dry carbon particles and dry hydrophobic polymer particles to form a dry mixture; applying a uniform layer of the dry mixture on the surface of a porous electrode substrate with virtually none of the mixture within the pores of the substrate by dispersing the mixture as a cloud of particles in a chamber over said surface of the substrate and pulling the carbon and polymer particles onto said surface by drawing a vacuum under the substrate; compacting the applied layer; and sintering the compacted layer.
Claim 2
Independent Claim 102 words
A method for making an electrochemical cell electrode comprising the steps of: blending together, in dry form, dry carbon particles and dry hydrophobic polymer particles to form a dry mixture; applying a uniform layer of the dry mixture on the surface of a porous electrode substrate with virtually none of the mixture within the pores of the substrate by dispersing the mixture as a cloud of particles in a chamber over said surface of the substrate and pulling the carbon and polymer particles onto said surface by drawing a vacuum under the substrate; compacting the applied layer; and sintering the compacted layer.
Claim 3
Dependent Claim 12 words
The method according to claim 1 wherein the hydrophobic polymer is PTFE.
Claim 4
Dependent Claim 45 words
The method according to claim 2 wherein the PTFE in the dry mixture has a molecular weight of at least 10 6 and, prior to its being applied to the substrate the dry mixture has a maximum particle size of less than about ten microns.
Claim 5
Dependent Claim 16 words
The method according to claim 2 wherein the carbon particles in the dry mixture are precatalyzed.
Claim 6
Dependent Claim 18 words
The method according to claim 2 wherein the carbon particles in the dry mixture are precatalyzed with platinum.
Claim 7
Dependent Claim 47 words
The method according to claim 1 wherein the hydrophobic polymer in the dry mixture has a molecular weight of at least 10 6 and a mean particle size, prior to application to the substrate, of one micron or less with no particles greater than about five microns.
Claim 8
Dependent Claim 27 words
The method according to claim 3 wherein the electrode substrate is graphitized carbon paper made from carbon fibers and has an open porosity of at least 80%.
Claim 9
Dependent Claim 20 words
The method according to claim 7 wherein the dry mixture has a mean particle size of one micron or less.
Claim 10
Dependent Claim 18 words
The method according to claim 7 wherein the carbon particles in the dry mixture are precatalyzed with platinum.

References Cited (Backward Citations)

US3900607A Cited
GB1163479A Cited
US3573991A Cited
US4044193A Cited
US4129633A Cited
US3829327A Cited
US3857737A Cited
US4017663A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-11-19 1983-05-21 1983-11-20 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-11-19 1987-05-21 1987-11-20 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-11-19 1991-05-21 1991-11-20 $7700.00 Window Closed / Lapsed

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