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US4171384A Expired / Lapsed US ⏱️ 0.0 years remaining

Combined dry-wet milling process for refining wheat

Assignee: Unilever Bestfoods North America
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Filing: 1978-05-11
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Granted: 1979-10-16
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Expires: 1998-05-11
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Abstract

Abstract There is disclosed a continuous process for refining whole grain wheat to obtain a prime wheat starch fraction and an animal feed product, the process comprising dry milling wheat kernels to provide an endosperm fraction, a germ fraction, a fiber (bran) fraction and a cleanings fraction, wet milling the endosperm fraction to provide a mill starch slurry, removing fine fiber tailings from the mill starch slurry, separating the slurry into a starch-rich fraction and protein-rich fraction, concentrating the protein-rich fraction, directly combining the fiber (bran), cleanings, fine fiber tailings and protein-rich concentrate, and the germ fraction to provide a wet animal feed product, and drying the feed product.

Inventors

  • 👤 Vincent P. Chwalek
  • 👤 Richard M. Olson

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 09:22
CPC Classifications
C; C08; C08B; C08B30/00; C08B30/04; C08B30/042; C08B30/046; A; A23; A23K; A23K10/00; A23K10/30; Y; Y02; Y02P; Y02P60/00; Y02P60/80; Y02P60/87

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 191 words
A continuous wheat refining process, which comprises: (A) dry milling whole grain wheat to provide (a) an endosperm fraction, (b) a germ fraction, (c) a fiber (bran) fraction, and (d) a cleanings fraction; (B) wet milling the single endosperm fraction of (A)(a) by sequentially (i) steeping the endosperm fraction, (ii) separating the larger wet endosperm particles from the smaller wet endosperm particles, (iii) milling the larger wet endosperm particles to reduce their particle size, (iv) recombining the wet endosperm particles of (ii) and (iii) into a single fraction, and (v) steeping the endosperm fraction again to provide a mill starch slurry; (C) separating fine fiber tailings from the mill starch slurry of (B)(v); (D) separating the defibered mill starch slurry of (C) into a starch-rich fraction and a protein-rich fraction; (E) concentrating the protein-rich fraction of (D); (f) directly combining each of the fiber (bran) fraction, the cleanings fraction and the germ fraction of (A), the fine fiber tailings fraction of (C) and the protein-rich concentrate of (E) to provide a wet animal feed product; and (G) drying the wet feed product of (F) to obtain a final animal feed product.
Claim 2
Dependent Claim 191 words
A continuous wheat refining process, which comprises: (A) dry milling whole grain wheat to provide (a) an endosperm fraction, (b) a germ fraction, (c) a fiber (bran) fraction, and (d) a cleanings fraction; (B) wet milling the single endosperm fraction of (A)(a) by sequentially (i) steeping the endosperm fraction, (ii) separating the larger wet endosperm particles from the smaller wet endosperm particles, (iii) milling the larger wet endosperm particles to reduce their particle size, (iv) recombining the wet endosperm particles of (ii) and (iii) into a single fraction, and (v) steeping the endosperm fraction again to provide a mill starch slurry; (C) separating fine fiber tailings from the mill starch slurry of (B)(v); (D) separating the defibered mill starch slurry of (C) into a starch-rich fraction and a protein-rich fraction; (E) concentrating the protein-rich fraction of (D); (f) directly combining each of the fiber (bran) fraction, the cleanings fraction and the germ fraction of (A), the fine fiber tailings fraction of (C) and the protein-rich concentrate of (E) to provide a wet animal feed product; and (G) drying the wet feed product of (F) to obtain a final animal feed product.
Claim 3
Dependent Claim 35 words
The process of claim 1 wherein in wet milling step (B), the initial weight ratio of the process (steep) water to the endosperm particles is in the range of from about 5:1 to about 6:1.
Claim 4
Dependent Claim 29 words
The process of claim 1 wherein the first steeping step (B)(i) and the second steeping step (B)(v) are conducted in an aqueous medium at an acid or alkaline pH.
Claim 5
Dependent Claim 11 words
The process of claim 3 wherein the steeping medium is acidic.
Claim 6
Dependent Claim 17 words
The process of claim 4 wherein the steeping medium comprises a solution of sulfur dioxide in water.
Claim 7
Dependent Claim 11 words
The process of claim 3 wherein the steeping medium is alkaline.
Claim 8
Dependent Claim 17 words
The process of claim 6 wherein the steeping medium comprises a solution of sodium hydroxide in water.
Claim 9
Dependent Claim 32 words
The process of claim 1 wherein the total residence time of the endosperm particles in steeping steps (B)(i) and (B)(v) is in the range of from about 2 to about 6 hours.
Claim 10
Dependent Claim 37 words
The process of claim 1 wherein in milling step (B)(iii) endosperm particles having a size of greater than about 50 to about 75 microns are reduced in size to about 50 to about 75 microns or less.
Claim 11
Dependent Claim 21 words
The process of claim 1 wherein step (D) is conducted by passing the mill starch slurry through a plurality of hydroclones.
Claim 12
Dependent Claim 22 words
The process of claim 10 wherein the mill starch slurry has a specific gravity of from about 7° to about 9° Baume.
Claim 13
Dependent Claim 301 words
A continuous wheat refining process, which comprises: (A) dry milling whole grain wheat to provide (a) an endosperm fraction, (b) a germ fraction, (c) a fiber (bran) fraction, and (d) a cleanings fraction; (B) wet milling the single endosperm fraction of (A)(a) by sequentially (i) steeping the endosperm fraction in a solution of sulfur dioxide in water, the initial weight ratio of the process (steep) water to the endosperm particles being in the range of from about 5:1 to about 6:1, (ii) separating the wet endosperm particles having a size of greater than about 50 microns from the smaller wet endosperm particles, (iii) impact milling the wet endosperm particles having a size of greater than about 50 microns to reduce their particle size to about 50 microns or less, (iv) recombining the wet endosperm particles of (ii) and (iii) into a single fraction, and (v) steeping the endosperm fraction again in a solution of sulfur dioxide in water to provide a mill starch slurry, the total residence time of steeping steps (i) and (v) combined being in the range from about 2 to about 6 hours; (C) separating fine fiber tailings from the mill starch slurry of (B)(v); (D) passing the defibered mill starch slurry of (C), having a specific gravity of from about 7° to about 9° Baume, through a plurality of hydroclones to provide an underflow stream comprising a starch-rich fraction and an overflow stream comprising a protein-rich fraction; (E) concentrating the protein-rich fraction of (D); (f) directly combining each of the fiber (bran) fraction, the cleanings fraction and the germ fraction of (A), the fine fiber tailings fraction of (C) and the protein-rich concentrate of (E) to provide a wet animal feed product; and (G) drying the wet feed product of (F) to obtain a final feed product.
Claim 14
Dependent Claim 301 words
A continuous wheat refining process, which comprises: (A) dry milling whole grain wheat to provide (a) an endosperm fraction, (b) a germ fraction, (c) a fiber (bran) fraction, and (d) a cleanings fraction; (B) wet milling the single endosperm fraction of (A)(a) by sequentially (i) steeping the endosperm fraction in a solution of sulfur dioxide in water, the initial weight ratio of the process (steep) water to the endosperm particles being in the range of from about 5:1 to about 6:1, (ii) separating the wet endosperm particles having a size of greater than about 50 microns from the smaller wet endosperm particles, (iii) impact milling the wet endosperm particles having a size of greater than about 50 microns to reduce their particle size to about 50 microns or less, (iv) recombining the wet endosperm particles of (ii) and (iii) into a single fraction, and (v) steeping the endosperm fraction again in a solution of sulfur dioxide in water to provide a mill starch slurry, the total residence time of steeping steps (i) and (v) combined being in the range from about 2 to about 6 hours; (C) separating fine fiber tailings from the mill starch slurry of (B)(v); (D) passing the defibered mill starch slurry of (C), having a specific gravity of from about 7° to about 9° Baume, through a plurality of hydroclones to provide an underflow stream comprising a starch-rich fraction and an overflow stream comprising a protein-rich fraction; (E) concentrating the protein-rich fraction of (D); (f) directly combining each of the fiber (bran) fraction, the cleanings fraction and the germ fraction of (A), the fine fiber tailings fraction of (C) and the protein-rich concentrate of (E) to provide a wet animal feed product; and (G) drying the wet feed product of (F) to obtain a final feed product.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-10-15 1983-04-16 1983-10-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-10-15 1987-04-16 1987-10-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-10-15 1991-04-16 1991-10-16 $7700.00 Window Closed / Lapsed

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