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US3909288A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for recovery of starch and corn oil from corn

Assignee: Cerestar USA Inc
•
Filing: 1973-11-05
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Granted: 1975-09-30
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Expires: 1993-11-05
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Abstract

Abstract A process for recovering starch and corn oil from corn kernels. The corn kernels are dry milled to separate the hulls and germ from the endosperm fractions. At least some of the endosperm fractions are steeped in separating the starch from the gluten. The gluten is dried and the separated germ and the dried corn gluten are subjected to solvent extraction to recover corn oil.

Inventors

  • 👤 Eugene L Powell
  • 👤 Gerald G Mcgeorge

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 18:45
CPC Classifications
A; A23; A23J; A23J1/00; A23J1/12; A23K; A23K10/00; A23K10/30; A23K10/37; C; C08; C08B; C08B30/00; C08B30/04; C08B30/042; C08B30/044; C11; C11B; C11B1/00; C11B1/02; C11B1/04; Y; Y02; Y02P; Y02P60/00; Y02P60/80; Y02P60/87

Claims Analysis

Total Claims: 23
Claim 1
Independent Claim 86 words
A PROCESS FOR RECOVERING STARCH AND CORN OIL FROM CORN COMPRISING: A. SUBJECTING CORN KERNALS TO A DRY SEPARATION PROCESS TO SEPATATE HULLS AND GERM FROM ENDOSPERM FRACTION, B. COMPINING AT LEAST SOME OF HE ENDOSPERM FRACTIONS WITH WATER AND SUBJECTING THE COMBINATION TO A WET STEERING STEP AND FURTHER PROCESS STEPS TO SEPARATE CORN STARCH FROM CORN GLUTEN, C. DRYING THE CORN GLUTEN, AND D. SUBJECTING AT LEAST THE SEPARATE GERM AND THE DRIED OIL GLUTEN TP A SOLVENT EXTRACTION STEP TO RECOVER CORN OIL.
Claim 2
Dependent Claim 86 words
A PROCESS FOR RECOVERING STARCH AND CORN OIL FROM CORN COMPRISING: A. SUBJECTING CORN KERNALS TO A DRY SEPARATION PROCESS TO SEPATATE HULLS AND GERM FROM ENDOSPERM FRACTION, B. COMPINING AT LEAST SOME OF HE ENDOSPERM FRACTIONS WITH WATER AND SUBJECTING THE COMBINATION TO A WET STEERING STEP AND FURTHER PROCESS STEPS TO SEPARATE CORN STARCH FROM CORN GLUTEN, C. DRYING THE CORN GLUTEN, AND D. SUBJECTING AT LEAST THE SEPARATE GERM AND THE DRIED OIL GLUTEN TP A SOLVENT EXTRACTION STEP TO RECOVER CORN OIL.
Claim 3
Dependent Claim 34 words
The process of claim 1 wherein step (a) is a corn dry milling process and the corN kernels are separated into a hull stream, a germ stream and a number of endosperm fraction streams.
Claim 4
Dependent Claim 22 words
The process of claim 1 wherein the oil meal resulting from the solvent extraction step is combined with heavy steepwater and hulls.
Claim 5
Dependent Claim 24 words
The process of claim 1 wherein fine fiber is recovered from the steeped endosperm fractions and the fine fiber is subjected to solvent extraction.
Claim 6
Dependent Claim 19 words
The process of claim 1 wherein the water-endosperm fraction admixture has a corn dry solids concentration of about 15-27%.
Claim 7
Dependent Claim 20 words
The process of claim 1 wherein the steeping is carried out for from about 1/2 hour to about 16 hours.
Claim 8
Dependent Claim 13 words
The process of claim 1 wherein the steeping temperature is from about 110*-130*F.
Claim 9
Dependent Claim 37 words
The process of claim 1 wherein step (a) is a short process dry milling procedure which separates the corn kernel into a hull stream, a germ stream and a corn flour stream and other endosperm fractions stream.
Claim 10
Dependent Claim 27 words
The process of claim 8 wherein the hull stream and the corn flour stream are also subjected to solvent extraction for the recovery of the corn oil.
Claim 11
Dependent Claim 17 words
The process of claim 1 wherein the endosperm fractions are maintained in suspension during the steeping step.
Claim 12
Dependent Claim 12 words
The process of claim 10 wherein the suspension is maintained by agitation.
Claim 13
Dependent Claim 30 words
The process of claim 1 wherein endosperm fractions are reduced in size so that they will pass through a 30 mesh/inch wire screen before they are combined with the water.
Claim 14
Dependent Claim 17 words
The process of claim 12 wherein the steep time is from about 1/2 to about 4 hours.
Claim 15
Dependent Claim 27 words
The process of claim 1 wherein the steeping is carried out in a sulfurous acid solution having a sulphur dioxide concentration of about 0.25 to about 0.01%.
Claim 16
Dependent Claim 20 words
The process of claim 14 wherein the pH of the steep is maintained at from about 3.5 to about 4.5.
Claim 17
Dependent Claim 17 words
The process of claim 15 wherein the pH is maintained at from about 3.9 to about 4.2.
Claim 18
Dependent Claim 27 words
The process of claim 1 wherein the crown starch suspended in water is separated from the palpable endosperm particles before the latter are subjected to wet milling.
Claim 19
Dependent Claim 28 words
The process of claim 17 wherein the crown starch slurry is separated from the steepwater with both starch and gluten being subsequently recovered from the crown starch fraction.
Claim 20
Dependent Claim 19 words
The process of claim 18 wherein the steepwater, after evaporation to form heavy steepwater, is combined with the hulls.
Claim 21
Dependent Claim 20 words
The process of claim 19 wherein the hull stream has been subjected to solvent extraction before combination with the steepwater.
Claim 22
Dependent Claim 182 words
A process for treating corn kernels comprising: a. subjecting the corn kernels to a dry separation process to separate hulls and germ from endosperm fractions by forming a hull stream, a germ stream and at leasst one endosperm stream; b. combining at least one of the endosperm streams with a sulfurous acid solution having a pH of from about 3.5 to about 4.5 and subjecting the combination to a wet dynamic steeping step for from about 1/2 hour to about 16 hours at temperatures ranging from about 110*-130*F; c. separating the steeped endosperm into two streams comprising (1) crown starch suspended in water and (2) palpable endosperm particles; d. milling the palpable endosperm particles and then recombining them with the crown starch slurry solids comprising starch and gluten which have been separated from the steepwater; e. separating the combined palpable endosperm particles and crown starch slurry solids into streams comprising corn gluten and corn starch; f. drying the corn gluten; and g. subjecting at least the dried corn gluten and the germ stream to an extraction process to remove corn oil therefrom.
Claim 23
Dependent Claim 182 words
A process for treating corn kernels comprising: a. subjecting the corn kernels to a dry separation process to separate hulls and germ from endosperm fractions by forming a hull stream, a germ stream and at leasst one endosperm stream; b. combining at least one of the endosperm streams with a sulfurous acid solution having a pH of from about 3.5 to about 4.5 and subjecting the combination to a wet dynamic steeping step for from about 1/2 hour to about 16 hours at temperatures ranging from about 110*-130*F; c. separating the steeped endosperm into two streams comprising (1) crown starch suspended in water and (2) palpable endosperm particles; d. milling the palpable endosperm particles and then recombining them with the crown starch slurry solids comprising starch and gluten which have been separated from the steepwater; e. separating the combined palpable endosperm particles and crown starch slurry solids into streams comprising corn gluten and corn starch; f. drying the corn gluten; and g. subjecting at least the dried corn gluten and the germ stream to an extraction process to remove corn oil therefrom.

References Cited (Backward Citations)

US2459548A Cited
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US2847282A Cited
US3029169A Cited
US3251717A Cited
US3597274A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-09-29 1979-03-31 1979-09-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-09-29 1983-03-31 1983-09-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-09-29 1987-03-31 1987-09-30 $7700.00 Window Closed / Lapsed

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