US4042414A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Processing of starch
Assignee: Research Corp
•
Filing: 1974-09-17
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Granted: 1977-08-16
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Expires: 1994-09-17
Abstract
Abstract Waxy, small granule starch of high spreadability, and waxy, large granule starch which is capable of forming an exceptionally clear and bright paste, are simultaneously produced by steeping waxy barley grain for a period of at least 12 hours in an aqueous solution containing sulfur dioxide at a temperature of 45°-55° C so as to swell the grain and extract soluble protein contained within said grain, water washing and milling said steeped grain, separating the starch from fibers and protein, suspending said starch in water to form a suspension containing less than 15% wt solids, permitting larger granules to settle for a period of at least 2 hours and recovering a larger granule fraction, said larger granules being characterized by an average particle size of greater than 10μ, and breaking the remaining suspension and recovering therefrom a smaller granule fraction, said small granules being characterized by an average particle size of from 2.5 to 10μ.
Inventors
- 👤 Kenneth Justin Goering
- 👤 Robert Freeman Eslick
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 22:54
CPC Classifications
C; C08; C08B; C08B30/00; C08B30/04; C08B30/042
Claims Analysis
Total Claims: 12
Claim 1
Independent Claim
172 words
A method for the simultaneous production of a waxy, small granule starch of high spreadability, and a large granule, waxy starch which is capable of forming an exceptionally clear and bright paste, which comprises: a. steeping waxy barley grain for a period of at least 12 hours in an aqueous solution containing sulfur dioxide at a temperature of 45°-55° C so to swell the grain and extract soluble protein contained within said grain, b. water washing and milling said steeped grain, c. separating fiber and protein from the starch granules in said grain, d. suspending said starch granules in water to form a suspension containing less than 15% wt solids, e. permitting larger granules to settle for a period of at least 2 hours and recovering a larger granule fraction, said larger granules being characterized by an average particle size of greater than 10μ, and f. breaking the remaining suspension and recovering therefrom a smaller granule fraction, said small granules being characterized by an average particle size of from 2.5 to 10μ.
Claim 2
Independent Claim
172 words
A method for the simultaneous production of a waxy, small granule starch of high spreadability, and a large granule, waxy starch which is capable of forming an exceptionally clear and bright paste, which comprises: a. steeping waxy barley grain for a period of at least 12 hours in an aqueous solution containing sulfur dioxide at a temperature of 45°-55° C so to swell the grain and extract soluble protein contained within said grain, b. water washing and milling said steeped grain, c. separating fiber and protein from the starch granules in said grain, d. suspending said starch granules in water to form a suspension containing less than 15% wt solids, e. permitting larger granules to settle for a period of at least 2 hours and recovering a larger granule fraction, said larger granules being characterized by an average particle size of greater than 10μ, and f. breaking the remaining suspension and recovering therefrom a smaller granule fraction, said small granules being characterized by an average particle size of from 2.5 to 10μ.
Claim 3
Dependent Claim
15 words
The process of claim 1, wherein said waxy barley being treated is Waxy Compana barley.
Claim 4
Dependent Claim
27 words
The process of claim 1, wherein said waxy barley grains are steeped in a slightly acidic solution of sodium meta-bisulfite which forms sulfur dioxide in said solution.
Claim 5
Dependent Claim
23 words
The process of claim 1, wherein said milled grains are screened to a mesh size of at least 150 prior to being suspended.
Claim 6
Dependent Claim
17 words
The process of claim 1, wherein said suspension is broken by subjecting said suspension to centrifugal action.
Claim 7
Independent Claim
185 words
A method for the simultaneous production of a waxy, small granule waxy starch of high spreadability, and a large granule, waxy starch which is capable of forming an exceptionally clear and bright paste which comprises: a. steeping Waxy Compana grain for a period of 12 to 50 hours in an aqueous solution containing sodium meta-bisulfite at a temperature of 45°-55° C so as to swell the grain and extract soluble protein contained within said grain, b. water washing and milling said steeped grain and screening said grain to a mesh size of 150, c. separating fiber and protein from the starch granules in said grain, d. supending said separated starch granules in water to form a suspension containing less than 15% wt solids, e. permitting larger granules to settle for a period of 2-20 hours and recovering a larger granule fraction being characterized by a particle size of greater than 10μ, and f. subjecting said suspension to centrifugal so as to break said suspension and recovering a smaller granule fraction, wherein small granules are characterized by an average particle size of from 2.5μ to 10μ.
Claim 8
Independent Claim
185 words
A method for the simultaneous production of a waxy, small granule waxy starch of high spreadability, and a large granule, waxy starch which is capable of forming an exceptionally clear and bright paste which comprises: a. steeping Waxy Compana grain for a period of 12 to 50 hours in an aqueous solution containing sodium meta-bisulfite at a temperature of 45°-55° C so as to swell the grain and extract soluble protein contained within said grain, b. water washing and milling said steeped grain and screening said grain to a mesh size of 150, c. separating fiber and protein from the starch granules in said grain, d. supending said separated starch granules in water to form a suspension containing less than 15% wt solids, e. permitting larger granules to settle for a period of 2-20 hours and recovering a larger granule fraction being characterized by a particle size of greater than 10μ, and f. subjecting said suspension to centrifugal so as to break said suspension and recovering a smaller granule fraction, wherein small granules are characterized by an average particle size of from 2.5μ to 10μ.
Claim 9
Dependent Claim
41 words
A small granule starch which is characterized by high spreadility and which can be used as a substitute for rice starch, which comprises small, waxy starch granules separated from Waxy Compana barley having an average particle size of 2.5μ to 10μ.
Claim 10
Dependent Claim
41 words
A small granule starch which is characterized by high spreadility and which can be used as a substitute for rice starch, which comprises small, waxy starch granules separated from Waxy Compana barley having an average particle size of 2.5μ to 10μ.
Claim 11
Dependent Claim
36 words
A large granule waxy starch which is capable of forming an exceptionally clear and bright paste, which comprises large waxy starch granules separated from Waxy Compana barley having an average particle size of 10μ to 40μ.
Claim 12
Dependent Claim
36 words
A large granule waxy starch which is capable of forming an exceptionally clear and bright paste, which comprises large waxy starch granules separated from Waxy Compana barley having an average particle size of 10μ to 40μ.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-08-15 | 1981-02-14 | 1981-08-16 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-08-15 | 1985-02-14 | 1985-08-16 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-08-15 | 1989-02-14 | 1989-08-16 | $7700.00 | Window Closed / Lapsed |