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US4140757A Expired / Lapsed US ⏱️ 0.0 years remaining

Extension of gum thickener with silicon dioxide and toothpaste containing the same

Assignee: JM Huber Corp
•
Filing: 1977-07-06
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Granted: 1979-02-20
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Expires: 1997-07-06
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Abstract

Abstract The extension of a gum thickener in a dentifrice composition of high water content is achieved by replacement of up to 50% of the gum thickener with a silica thickener which results in a dentifrice of improved cosmetic properties while reducing total raw material costs.

Inventors

  • 👤 Satish K. Wason
  • 👤 Robert K. Mays

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 01:08
CPC Classifications
A; A61; A61Q; A61Q11/00; A61K; A61K8/00; A61K8/18; A61K8/19; A61K8/25; A61K8/72; A61K8/73; A61K8/731

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 116 words
A dentifrice composition comprising the following essential components: ______________________________________ COMPONENT AMOUNT - WT. % ______________________________________ Abrasive 10-60 Humectant 15-40 Gum Thickener 0.4-0.9 Silica Thickener 1-20 Water 35-50 ______________________________________ wherein said silica thickener has a primary particle size of less than 40 millimicrons, a void volume of from 3.0 to 6.0 cc Hg/g, an oil absorption of 150-250 cc oil/100 g of silica, a surface area of from 100-400 m 2 /g, and a wet cake moisture in excess of 85%; and wherein said abrasive and said silica thickener are premixed prior to addition thereof to the other components of said dentifrice composition, said addition being at the conclusion of the mixing procedure for said other components.
Claim 2
Dependent Claim 116 words
A dentifrice composition comprising the following essential components: ______________________________________ COMPONENT AMOUNT - WT. % ______________________________________ Abrasive 10-60 Humectant 15-40 Gum Thickener 0.4-0.9 Silica Thickener 1-20 Water 35-50 ______________________________________ wherein said silica thickener has a primary particle size of less than 40 millimicrons, a void volume of from 3.0 to 6.0 cc Hg/g, an oil absorption of 150-250 cc oil/100 g of silica, a surface area of from 100-400 m 2 /g, and a wet cake moisture in excess of 85%; and wherein said abrasive and said silica thickener are premixed prior to addition thereof to the other components of said dentifrice composition, said addition being at the conclusion of the mixing procedure for said other components.
Claim 3
Dependent Claim 15 words
A composition according to claim 1 wherein said abrasive is a low structure silica abrasive.
Claim 4
Dependent Claim 12 words
A composition according to claim 1 wherein said abrasive is dicalcium phosphate.
Claim 5
Dependent Claim 21 words
A composition according to claim 1 wherein said humectant is selected from the group consisting of glycerine, sorbitol and mixtures thereof.
Claim 6
Dependent Claim 13 words
A composition according to claim 1 wherein said gum thickener is carboxymethy cellulose.
Claim 7
Dependent Claim 35 words
A composition according to claim 1 wherein said silica thickener has an oil absorption value from 200 to 250 cc oil/100 g of silica and a surface area from 250 to 400 m 2 /g.
Claim 8
Independent Claim 150 words
A method of using a silica thickener to extend the functional performance of a gum thickener in a dentifrice composition comprising about 10-60 weight percent of an abrasive, about 15-40 weight percent of a humectant, about 0.4 to 0.9 weight percent of a gum thickener, and about 35-50 weight percent of water, said method comprising (a) premixing about 1-20 weight percent of a high structure silica thickener with said abrasive, and (b) adding the resulting mixture to the remaining components of said dentifrice composition at the conclusion of the mixing procedure for said remaining components; wherein said thickener has a primary particle size of less than 40 millimicrons; a void volume of from 3.0 to 6.0 cc Hg/g; an oil absorption of 150 to 250 cc oil/100 g of silica; a surface area of from 100 to 400 m 2 /g; and a wet cake moisture in excess of 85%.
Claim 9
Independent Claim 150 words
A method of using a silica thickener to extend the functional performance of a gum thickener in a dentifrice composition comprising about 10-60 weight percent of an abrasive, about 15-40 weight percent of a humectant, about 0.4 to 0.9 weight percent of a gum thickener, and about 35-50 weight percent of water, said method comprising (a) premixing about 1-20 weight percent of a high structure silica thickener with said abrasive, and (b) adding the resulting mixture to the remaining components of said dentifrice composition at the conclusion of the mixing procedure for said remaining components; wherein said thickener has a primary particle size of less than 40 millimicrons; a void volume of from 3.0 to 6.0 cc Hg/g; an oil absorption of 150 to 250 cc oil/100 g of silica; a surface area of from 100 to 400 m 2 /g; and a wet cake moisture in excess of 85%.
Claim 10
Dependent Claim 15 words
A method according to claim 7 wherein said abrasive is a low structure silica abrasive.
Claim 11
Dependent Claim 12 words
A method according to claim 7 wherein said abrasive is decalcium phosphate.
Claim 12
Dependent Claim 21 words
A method according to claim 7 wherein said humectant is selected from the group consisting of glycerine, sorbitol and mixtures thereof.
Claim 13
Dependent Claim 13 words
A method according to claim 7 wherein said gum thickener is carboxymethyl cellulose.
Claim 14
Dependent Claim 34 words
A method according to claim 7 wherein said silica thickener has an oil absorption value from 200 to 250 cc/100 g of silica and a surface area from 250 to 400 m 2 /g.
Claim 15
Dependent Claim 19 words
a method according to claim 7 wherein the amount of gum thickener is about 0.5 to 0.8 weight percent.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-02-19 1982-08-21 1983-02-20 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-02-19 1986-08-21 1987-02-20 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-02-19 1990-08-21 1991-02-20 $7700.00 Window Closed / Lapsed

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