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US3935306A Expired / Lapsed US ⏱️ 0.0 years remaining

Toothpaste formulations

Assignee: Colgate Palmolive Co
•
Filing: 1974-02-08
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Granted: 1976-01-27
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Expires: 1994-02-08
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Abstract

Abstract Toothpaste formulations having dispersed therein a plurality of agglomerated particles of dental polishing agent that are visible, palpable and substantially insoluble in the toothpaste are disclosed. The agglomerates comprise individually impalpable particles of water insoluble dental polishing agent; can include an agglomerating agent and are reduced to smaller sized particles of dental polishing agent when subjected to mild mechanical agitation such as toothbrushing. Such agglomerates are particularly well suited for incorporation into transparent gel dental vehicles to provide special effects such as supplemental cleaning and polishing characteristics without adversely affecting the visual clarity of the finished toothpaste.

Inventors

  • 👤 Francis D. Roberts
  • 👤 John J. Steinke, III

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 14:25
CPC Classifications
A; A61; A61Q; A61Q11/00; A61K; A61K8/00; A61K8/02; A61K8/0241; A61K8/0275; A61K8/04; A61K8/042; A61K8/18; A61K8/19; A61K8/25; A61K8/26

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 235 words
A speckled toothpaste comprising a translucent or transparent gel toothpaste vehicle having a refractive index between 1.4 and 1.5 and having dispersed therein up to 75% by weight of macroscopically visible, substantially water-insoluble palpable agglomerates of impalpable dental polishing agent particles, said agglomerates having a particle size less than 840 microns and including an agglomerating agent having binding properties, said particles of dental polishing agent being so agglomerated that said agglomerates retain their visibility and palpability in the toothpaste but are reduced to invisible, impalpable particles when said toothpaste is subjected to toothbrushing, said toothpaste base including a polishing material having a refractive index substantially the same as said translucent or transparent toothpaste vehicle in order to maintain visual clarity so as to form a clear gel, the total amount of dental polishing agent and polishing material in said toothpaste being at least 5 percent by weight, said agglomerates being visible both on the surface and in the interior of said clear gel, giving a positive three dimensional sparkling appearance due to the unique light reflectance effects, said agglomerates being inherently white or, when colored, containing about 1 to 10% by weight of water insoluble dye, pigment or lake, said clear gel vehicle having a color different from, or contrasting with, said agglomerates, said gel vehicle containing water and having a total liquid content which is about 20 to 89.5% by weight of the toothpaste.
Claim 2
Dependent Claim 235 words
A speckled toothpaste comprising a translucent or transparent gel toothpaste vehicle having a refractive index between 1.4 and 1.5 and having dispersed therein up to 75% by weight of macroscopically visible, substantially water-insoluble palpable agglomerates of impalpable dental polishing agent particles, said agglomerates having a particle size less than 840 microns and including an agglomerating agent having binding properties, said particles of dental polishing agent being so agglomerated that said agglomerates retain their visibility and palpability in the toothpaste but are reduced to invisible, impalpable particles when said toothpaste is subjected to toothbrushing, said toothpaste base including a polishing material having a refractive index substantially the same as said translucent or transparent toothpaste vehicle in order to maintain visual clarity so as to form a clear gel, the total amount of dental polishing agent and polishing material in said toothpaste being at least 5 percent by weight, said agglomerates being visible both on the surface and in the interior of said clear gel, giving a positive three dimensional sparkling appearance due to the unique light reflectance effects, said agglomerates being inherently white or, when colored, containing about 1 to 10% by weight of water insoluble dye, pigment or lake, said clear gel vehicle having a color different from, or contrasting with, said agglomerates, said gel vehicle containing water and having a total liquid content which is about 20 to 89.5% by weight of the toothpaste.
Claim 3
Dependent Claim 17 words
A toothpaste as in claim 1 in which said gel is red and said agglomerates are white.
Claim 4
Dependent Claim 17 words
A toothpaste as in claim 1 in which said gel is blue and said agglomerates are white.
Claim 5
Dependent Claim 40 words
A toothpaste according to claim 1 wherein said particles of dental polishing agent are selected from the group consisting of insoluble phosphate salts, calcium carbonate, magnesium carbonate, hydrated alumina, silica, zirconium silicate, aluminum silicate, calcined aluminum silicate and polymethyl methacrylate.
Claim 6
Dependent Claim 15 words
A toothpaste according to claim 1 wherein said toothpaste base includes a siliceous polishing material.
Claim 7
Dependent Claim 18 words
A toothpaste according to claim 1 wherein said polishing material has a refractive index between 1.44 and 1.46.
Claim 8
Dependent Claim 16 words
A toothpaste according to claim 6 wherein said toothpaste base contains a silica xerogel polishing material.
Claim 9
Dependent Claim 32 words
A toothpaste according to claim 1 wherein said gel base includes a minor amount up to about 10 percent by weight of said agglomerates dispersed therein effective to form a speckled toothpaste.
Claim 10
Dependent Claim 23 words
A toothpaste according to claim 8 wherein said gel base further includes between 5 and 20 percent by weight of said polishing material.
Claim 11
Dependent Claim 20 words
A toothpaste according to claim 1 wherein said agglomerates have a mean particle size from about 200 and 500 microns.
Claim 12
Dependent Claim 260 words
A speckled toothpaste comprising a. a transparent or translucent clear gel vehicle having a refractive index between 1.4 and 1.5, b. said gel vehicle including between 5 and 20 percent by weight of a siliceous polishing material having a refractive index between 1.4 and 1.5, and c. between 1 and 10 percent by weight of agglomerates of impalpable dental polishing agent particles, d. said agglomerates including an agglomerating agent having binding or lubricating properties, e. said dental polishing agent particles comprising a major amount of said agglomerates, F. said combination of polishing materials in the vehicle and the agglomerates being effective in cleansing and polishing power during toothbrushing, g. said agglomerates being substantially stable and insoluble in said gel vehicle and being so agglomerated that they retain their visibility and palpability in the toothpaste but are reduced to invisible impalpable particles when the toothpaste is subjected to toothbrushing, h. said agglomerates being visible both on the surface and on the interior of said clear gel, giving a positive three dimensional sparkling appearance due to the unique light reflectance effects, said agglomerates being inherently white, or when colored, containing about 1 to 10% by weight water insoluble dye, pigment or lake, said clear gel vehicle having a color different from, or contrasting with, said agglomerates, said gel vehicle containing water and having a total liquid content which is about 20 to 89.5% by weight of the toothpaste, the refractive index of said siliceous polishing material being about the same as that of said gel vehicle in order to maintain visual clarity.
Claim 13
Dependent Claim 260 words
A speckled toothpaste comprising a. a transparent or translucent clear gel vehicle having a refractive index between 1.4 and 1.5, b. said gel vehicle including between 5 and 20 percent by weight of a siliceous polishing material having a refractive index between 1.4 and 1.5, and c. between 1 and 10 percent by weight of agglomerates of impalpable dental polishing agent particles, d. said agglomerates including an agglomerating agent having binding or lubricating properties, e. said dental polishing agent particles comprising a major amount of said agglomerates, F. said combination of polishing materials in the vehicle and the agglomerates being effective in cleansing and polishing power during toothbrushing, g. said agglomerates being substantially stable and insoluble in said gel vehicle and being so agglomerated that they retain their visibility and palpability in the toothpaste but are reduced to invisible impalpable particles when the toothpaste is subjected to toothbrushing, h. said agglomerates being visible both on the surface and on the interior of said clear gel, giving a positive three dimensional sparkling appearance due to the unique light reflectance effects, said agglomerates being inherently white, or when colored, containing about 1 to 10% by weight water insoluble dye, pigment or lake, said clear gel vehicle having a color different from, or contrasting with, said agglomerates, said gel vehicle containing water and having a total liquid content which is about 20 to 89.5% by weight of the toothpaste, the refractive index of said siliceous polishing material being about the same as that of said gel vehicle in order to maintain visual clarity.
Claim 14
Dependent Claim 17 words
A toothpaste as in claim 11 in which said gel is red and said agglomerates are white.
Claim 15
Dependent Claim 17 words
A toothpaste as in claim 11 in which said gel is blue and said agglomerates are white.

References Cited (Backward Citations)

US2196154A Cited
US3538230A Cited
US3574823A Cited
DE2031676A1 Cited
US3767791A Cited
US3803301A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-01-26 1979-07-28 1980-01-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-01-26 1983-07-28 1984-01-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-01-26 1987-07-28 1988-01-27 $7700.00 Window Closed / Lapsed

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